Image-Guided Sample Transfer for Automated FIB Preparation

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Solution Overview

Problem

Existing sample preparation apparatuses lack the capability to accurately automate the extraction and transfer of sample pieces processed with ion beams to sample holders, particularly in miniaturized formats, leading to positional accuracy issues and inefficient sampling operations.

Innovation Solution

An automatic sample preparation apparatus is developed, utilizing a charged particle beam device with a focused ion beam and electron beam irradiation system, a needle drive mechanism, and image-based control to accurately position and transfer sample pieces to a sample holder, leveraging image data and templates for precise automation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Extent of automation

If manual sampling operation is used, then operational flexibility is maintained, but automation capability and efficiency are insufficient

Engineering Contradiction:
Improveautomation of sampling operationVSAvoidoperational complexity
Core Design Contradiction:
Extent of automationVSEase of operation

Solution Approach 1:

The system performs automatic sampling operations without manual intervention. The automated sampling head moves independently to extract sample pieces, transfer them to the sample holder, and return to the starting position, enabling the system to serve itself in the sampling process.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent replaces manual mechanical sampling operations with an automated mechanical system. The automated sampling head, controlled by a computer, substitutes human operators to perform extraction, transfer, and positioning operations, achieving full automation while maintaining operational precision.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If sample pieces are miniaturized, then analysis precision is improved, but positional accuracy during transfer deteriorates

Engineering Contradiction:
Improveanalysis precision of miniaturized samplesVSAvoidpositional accuracy of sample transfer
Core Design Contradiction:
Measurement precisionVSManufacturing precision

Solution Approach 1:

The system creates a digital model (copy) of the sample holder's pixel structure. By mapping the physical pixel positions to a digital representation, the system can accurately calculate and control the transfer positions of miniaturized sample pieces, maintaining high positional accuracy despite their small size.

Inventive Principle:
Principle #26Copying

Solution Approach 2:

The patent introduces a digital dimension to the physical sampling process. By using computer-controlled movements and digital image processing, the system adds a layer of precision control that enables accurate handling of miniaturized samples, resolving the contradiction between sample size reduction and transfer accuracy.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Productivity

If automated sampling is implemented, then productivity is improved, but device complexity increases

Engineering Contradiction:
Improvesampling efficiencyVSAvoidcomplexity of automated sampling system
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The automated sampling head is designed as a multi-functional device that can perform extraction, transfer, positioning, and return operations. This universal design consolidates multiple functions into a single mechanism, improving productivity while controlling overall system complexity.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The system uses image processing to detect the positions of sample pieces and the sampling head. This feedback mechanism enables real-time position monitoring and correction, allowing the automated system to maintain high productivity through precise control without requiring overly complex mechanical structures.

Inventive Principle:
Principle #23Feedback

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus enables accurate and automated transfer of sample pieces, improving positional accuracy and efficiency by using image data and templates to guide the needle and stage movements, ensuring precise placement on the sample holder.

Implementation Method 1

a technology for appropriately automating a sampling operation of the sample pieces cannot be realized. In addition, the term 'sampling' used in the present specification indicates processing which extracts a sample piece prepared by irradiating the sample with a charged particle beam including electrons or ions

Methodology Applied
Scientific EffectFocused Ion Beam: Ion Beam

Implementation Method 2

observation, analysis, and measurement using an electron beam of a scanning electron microscope, a transmission electron microscope, or the like

Methodology Applied
Scientific EffectElectron Beam: Electron Beam

Data Source

PatentEP3163283B1Automated sample-preparation device
Publication Date: 2023.08.30 HITACHI HIGH TECH SCIENCE CORP
  • EP3163283B1 patent drawingFigure 1
  • EP3163283B1 patent drawingFigure 2~4
  • EP3163283B1 patent drawingFigure 5

AI summary

A charged particle beam device (10a) includes a computer (21) which controls multiple charged particle beam irradiation optical systems, the needle (18), and a gas supply portion (17) to transfer a sample piece Q to a predetermined position of the sample piece holder P, based on at least images of a sample piece holder (P), a needle (18), and the sample piece (Q) previously acquired by multiple charged particle beams.