Laser-Heated Crystal Growth for Compositionally Stable Single Crystals

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Solution Overview

Problem

Existing methods for growing single crystals face challenges in maintaining a desired composition due to changes in the melt's composition or impurity concentration during crystal growth, leading to compositional supercooling and difficulties in achieving uniform crystal composition.

Innovation Solution

A crystal growing apparatus that employs a laser mechanism to heat and irradiate the melt near the boundary region between the growing crystal and the melt, allowing for a controlled temperature gradient to be maintained despite changes in the melt's composition or impurity concentration, ensuring the growth of a crystal with a desired composition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional heating methods are used to grow crystals, then the crystal growth process can proceed, but compositional supercooling occurs due to changes in melt composition, making it difficult to grow crystals with desired composition

Engineering Contradiction:
Improvecrystal composition uniformityVSAvoidmelt composition stability
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent applies local quality by using a laser to selectively heat only the solid-liquid interface region rather than the entire melt. This localized heating creates a controlled temperature gradient at the interface, preventing compositional supercooling while allowing the bulk melt composition to change during crystal growth. The laser energy is focused on the boundary region where crystal formation occurs, maintaining precise thermal control at the critical interface zone.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent implements parameter changes by dynamically adjusting the laser heating parameters (power, focal position, scanning speed) to compensate for changes in melt composition during crystal growth. As the crystal grows and melt composition changes, the laser parameters are modified to maintain the optimal temperature gradient at the solid-liquid interface, ensuring continuous prevention of compositional supercooling throughout the growth process.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If the melt composition changes during crystal growth, then crystal growth can proceed, but the intended composition of the crystal differs from the intended composition of the melt

Engineering Contradiction:
Improvecrystal growth rateVSAvoidcrystal composition accuracy
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent employs feedback control by monitoring the crystal growth process and adjusting the laser heating parameters in response to detected changes in melt composition or crystal growth conditions. This feedback mechanism allows real-time compensation for composition changes, ensuring that the crystal maintains the desired composition even as the melt evolves during the growth process.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent applies dynamics by making the heating system adaptive and adjustable during the crystal growth process. The laser heating parameters are dynamically modified based on the changing conditions, allowing the system to respond to and compensate for melt composition changes, thereby maintaining precise control over crystal composition throughout the growth process.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus effectively grows crystals with a desired composition by increasing the temperature gradient at the solid-liquid interface, preventing compositional supercooling and enabling the growth of high-quality single crystals even when the melt's composition changes during crystal growth.

Implementation Method 1

a laser mechanism that irradiates and heats, with laser light, the portion in which the raw material body is melted near a boundary region between the portion in which the raw material body is melted and the crystal

Methodology Applied
Scientific EffectLaser heating: Laser

Implementation Method 2

heating and melting one end side of a raw material body with a heating mechanism, the raw material body being formed with the raw material that is solid

Methodology Applied
Scientific EffectMelting: Melting

Data Source

PatentUS20240263340A1Method of growing crystal
Publication Date: 2024.08.08 NIPPON TELEGRAPH & TELEPHONE CORP
  • US20240263340A1 patent drawing
  • US20240263340A1 patent drawing
  • US20240263340A1 patent drawing

AI summary

An embodiment crystal growing apparatus is an apparatus that grows a crystal of a raw material by heating and melting, with a heating mechanism, one end side of a raw material body formed with a solid raw material with which a seed crystal is in contact, and further includes a laser mechanism. In crystal growth using this crystal growing apparatus, the portion to be heated for forming a melt is moved in the direction toward the other end side of the raw material body, and the melt is irradiated and heated with laser light emitted from the laser mechanism while the melt is moved from the one end side to the other end side.