Laser-Assisted Micro-Mass Spectrometry for Low-Power Cryogenic Analysis

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Solution Overview

Problem

Current mass spectrometers are not suitable for low-power, high-performance chemical detection in hazardous and tactical situations, nor are they efficient for analyzing organic compounds in cryogenic planetary environments, due to high power consumption and complexity.

Innovation Solution

A laser-assisted micro-mass spectrometer with a pulsed inlet and a multi-wavelength laser system, utilizing dual ionization sources for efficient analysis of refractory organic compounds, capable of operating in low-power and cryogenic conditions, with a compact design suitable for planetary missions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Use of energy by moving object

If conventional mass spectrometers are used for chemical detection, then measurement precision is maintained, but power consumption is excessive and device complexity is high

Engineering Contradiction:
Improvepower consumptionVSAvoidchemical detection precision
Core Design Contradiction:
Use of energy by moving objectVSMeasurement precision

Solution Approach 1:

The mass spectrometer is divided into modular components: a pulsed inlet system, a multi-wavelength laser system, and a compact mass analyzer. This segmentation allows each component to be optimized for low power consumption while maintaining overall measurement precision through coordinated operation of the modules

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The inlet system operates in pulsed mode rather than continuously, synchronizing sample introduction with laser pulses. This periodic action significantly reduces power consumption of the inlet and vacuum systems while maintaining detection precision by concentrating analytical resources on actual measurement moments

Inventive Principle:
Principle #19Periodic action

2Device complexity

If conventional mass spectrometers are used for chemical detection, then measurement precision is maintained, but device complexity is high

Engineering Contradiction:
Improveinstrument complexityVSAvoidchemical detection precision
Core Design Contradiction:
Device complexityVSMeasurement precision

Solution Approach 1:

The multi-wavelength laser system serves multiple functions: it performs laser ablation of samples, ionizes neutral molecules, and can be tuned to different wavelengths for analyzing different types of compounds. This multi-functionality reduces the need for separate specialized instruments, lowering overall device complexity while maintaining precision

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The laser ablation and ionization functions are merged into a single laser system, and the pulsed inlet is integrated with the laser triggering mechanism. This consolidation reduces the number of separate components and simplifies the overall instrument architecture while preserving measurement precision

Inventive Principle:
Principle #5Merging (Combining)

3Measurement precision

If multi-wavelength laser system is used, then analysis sensitivity is improved, but power consumption increases

Engineering Contradiction:
Improveanalysis sensitivityVSAvoidlaser power consumption
Core Design Contradiction:
Measurement precisionVSUse of energy by moving object

Solution Approach 1:

The laser operates in pulsed mode with multiple wavelengths sequentially or simultaneously activated only during measurement periods. This periodic operation allows the system to achieve high sensitivity through multi-wavelength capability while minimizing power consumption by keeping the laser inactive during non-measurement intervals

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The laser wavelength is dynamically changed based on the specific analytical requirements for different compounds. This parameter adjustment allows the system to achieve optimal sensitivity for each analyte type while consuming only the necessary power for the specific measurement task, avoiding continuous high-power operation

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves high sensitivity and specificity in chemical analysis with reduced power consumption and complexity, enabling quick decision-making in hazardous situations and effective analysis of organic compounds in cryogenic environments.

Implementation Method 1

a multi-wavelength laser system configured to generate at least two laser beams... when directed to a target of analyte material, can be configured to generate a neutral sample of analyte material

Methodology Applied
Scientific EffectLaser ablation: Laser Ablation

Implementation Method 2

a first mass spectrometer module including a plurality of first ionization sources

Methodology Applied
Scientific EffectPhotoionisation: Photoionisation

Data Source

PatentUS12080532B2Devices and methods for laser-assisted micro mass spectroscopy
Publication Date: 2024.09.03 CHEMRING SENSORS & ELECTRONICS SYSTEMS INC
  • US12080532B2 patent drawing
  • US12080532B2 patent drawing
  • US12080532B2 patent drawing

AI summary

Systems and methods disclosed provide a laser-assisted micro-mass spectrometer, which can include a pulsed inlet, a multi-wavelength laser system, and a first mass spectrometer module including a plurality of first ionization sources. In an embodiment, the pulsed inlet can be configured to receive a neutral sample of analyte material and provide it to said first mass spectrometer module.