Lithium Primary Cell with pH-Modified Electrolyte for Void Volume Management

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Solution Overview

Problem

Existing primary electrochemical cells face challenges in balancing improved discharge performance with the need for increased void volume to accommodate reaction products, while also ensuring reliability against physical abuse and partial discharge.

Innovation Solution

The use of an iron disulfide cathode material and a non-aqueous electrolyte comprising specific solvents, salts, and pH-modifiers, along with a Positive Temperature Coefficient (PTC) device and optimized cell dimensions, including a gasket material and separator, enhances discharge performance and physical abuse resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If the cathode material composition is refined to increase discharge performance, then discharge performance is improved, but the volume of reaction products increases requiring more void volume

Engineering Contradiction:
Improvedischarge performanceVSAvoidvoid volume
Core Design Contradiction:
ProductivityVSVolume of stationary object

Solution Approach 1:

The patent modifies the chemical composition parameters of the electrolyte by incorporating specific pH-modifiers (ammonium carbonate, ammonium bicarbonate, or lithium carbonate) to control the chemical environment during discharge. This allows the cell to achieve improved discharge performance while managing the volume expansion of reaction products through controlled chemical reactions that produce smaller volume byproducts or facilitate better packing of discharge products.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If internal cell volume is maximized for active material by reducing housing, seal, and separator thickness, then discharge performance is improved, but physical abuse resistance deteriorates

Engineering Contradiction:
Improvedischarge performanceVSAvoidphysical abuse resistance
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent employs composite material strategies by combining multiple electrolyte components (solvents, salts, and pH-modifiers) to create an electrolyte system that provides both high ionic conductivity for performance and adequate buffering capacity for physical stress. The specific combination of dioxolane, sulfolane, and 3,5-dimethylisoxazole creates a composite electrolyte system that maintains cell integrity under physical abuse while enabling high discharge performance.

Inventive Principle:
Principle #40Composite materials

3Use of energy by moving object

If discharge depth is increased to improve performance, then more energy is delivered, but volume of reaction products increases requiring more void volume

Engineering Contradiction:
Improveenergy deliveryVSAvoidvoid volume
Core Design Contradiction:
Use of energy by moving objectVSVolume of stationary object

Solution Approach 1:

The patent converts the potentially harmful volume expansion from deep discharge into a beneficial effect by using pH-modifiers that control the formation of reaction products. The ammonium carbonate, ammonium bicarbonate, or lithium carbonate additives manage the chemical reactions during deep discharge to produce reaction products with smaller volume or better packing characteristics, thereby enabling high energy delivery without proportionally increasing void volume requirements.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration improves discharge performance, stability, and physical abuse resistance, maintaining performance even after high-temperature storage and passing conventional physical abuse tests by ensuring adequate void volume and minimizing the risk of failure.

Implementation Method 1

the composition of the electrolyte is modified by the inclusion of a pH-modifier, which is an inorganic additive selected from the group consisting of ammonium carbonate, ammonium bicarbonate, and combinations thereof

Methodology Applied
Scientific EffectpH-modification:

Implementation Method 2

a non-aqueous electrolyte in fluid communication with the anode, cathode and separator, wherein said electrolyte comprises a solvent, a salt dissolved therein

Methodology Applied
Scientific EffectIonic conduction: Conduction (electrical)

Implementation Method 3

the electrochemical processes or reactions that occur within the cell result in an increase of cathode thickness upon discharge, and an accompanying formation of reaction products

Methodology Applied
Scientific EffectElectrochemical reactions: Redox Reactions

Data Source

PatentEP2549568B1Improved lithium primary cell
Publication Date: 2016.03.09 SPECTRUM BRANDS INC
  • EP2549568B1 patent drawingFigure 1
  • EP2549568B1 patent drawingFigure 2
  • EP2549568B1 patent drawingFigure 3

AI summary

The present disclosure is directed to a primary electrochemical cell having an improved discharge performance, and/or improved reliability under physical abuse and/or partial discharge. More particularly, the present disclosure is directed to such a primary cell that comprises an improved cathode material (8) comprising a mixture of iron disulfide and a selected pH-modifier and an improved non-aqueous electrolyte that comprises a solvent, a salt, pH-modifiers, and selected organic or inorganic additives, which improve cell stability and discharge performance.