Metal Strip Pickling Control Using LIBS Oxide Measurement

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Solution Overview

Problem

Conventional cleaning methods for hot-rolled metal strips are inefficient in removing the oxide layer, leading to material loss, environmental hazards, and suboptimal cleaning processes due to unknown initial scale thickness and excessive acid usage.

Innovation Solution

A cleaning plant equipped with laser-induced breakdown spectroscopy (LIBS) systems for precise measurement of oxide layer thickness and composition, allowing for automatic adjustment of pickling parameters and reduced acid consumption.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of substance

If conventional chemical pickling is used to remove oxide layers, then the oxide layer is removed, but excessive acid consumption and material loss occur

Engineering Contradiction:
Improvematerial lossVSAvoidacid consumption
Core Design Contradiction:
Loss of substanceVSQuantity of substance

Solution Approach 1:

The system performs preliminary measurement of oxide layer thickness using LIBS technology before the pickling process. This allows the pickling parameters (acid concentration, exposure time, temperature) to be pre-calculated and optimized based on the actual oxide thickness, preventing both over-pickling (excessive material removal) and under-pickling (insufficient cleaning).

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system implements a feedback control loop where oxide layer thickness is measured in real-time, process parameters are automatically adjusted based on measurement results, and the cleaning effectiveness is continuously monitored. This closed-loop control ensures optimal acid usage and minimal material loss while maintaining consistent cleaning quality.

Inventive Principle:
Principle #23Feedback

2Manufacturing precision

If conventional chemical pickling is used without precise measurement, then cleaning is performed, but process optimization is impossible due to unknown initial scale thickness

Engineering Contradiction:
Improvecleaning precisionVSAvoidoxide thickness information
Core Design Contradiction:
Manufacturing precisionVSLoss of information

Solution Approach 1:

The system replaces conventional mechanical or visual inspection methods with LIBS (Laser-Induced Breakdown Spectroscopy) technology. A laser pulse is directed at the oxide layer, creating a plasma whose spectral emission lines provide precise information about oxide thickness and composition. This optical spectroscopy method enables non-contact, rapid, and highly accurate measurement of oxide layer characteristics.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The system utilizes changes in spectral parameters (intensity, wavelength, duration of emission lines) to determine oxide layer thickness and composition. By analyzing how these spectral parameters vary with oxide thickness, the system can precisely quantify the oxide layer and adjust pickling parameters accordingly to achieve optimal cleaning precision.

Inventive Principle:
Principle #35Parameter changes

3Reliability

If excessive acid is used to ensure complete cleaning, then cleaning reliability is improved, but environmental harm and disposal costs increase

Engineering Contradiction:
Improvecleaning reliabilityVSAvoidenvironmental impact
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The system performs preliminary measurement and calculation of exact pickling parameters based on actual oxide thickness. This allows the minimum necessary amount of acid to be used while ensuring complete and reliable cleaning, eliminating the need for excessive acid application that would compromise environmental safety.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system dynamically adjusts pickling parameters (acid concentration, flow rate, exposure time, temperature) based on real-time oxide thickness measurements. This parameter optimization ensures that cleaning reliability is maintained at the required level while minimizing acid consumption and environmental impact.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enables precise and safe cleaning with reduced material loss, environmental impact, and optimized acid usage, improving the quality and efficiency of the cleaning process.

Implementation Method 1

at least one laser source (4), arranged upstream of the pickling means (5), for ablation of the superficial layer of oxide

Methodology Applied
Scientific EffectLaser ablation: Laser Ablation

Implementation Method 2

The measuring means (4) consist of at least one laser source (4) cooperating with a fiber optic spectrometer, defining a LIBS system (Laser Induced Breakdown Spectroscopy)

Methodology Applied
Scientific EffectLaser-induced breakdown spectroscopy:

Data Source

PatentEP3631049B1Cleaning plant for metal products
Publication Date: 2021.10.27 DANIELI & C OFFICINE MECCANICHE SPA
  • EP3631049B1 patent drawingFigure 1
  • EP3631049B1 patent drawingFigure 2
  • EP3631049B1 patent drawingFigure 3

AI summary

A plant for cleaning rolled metal strips provided with a superficial layer of oxide, the plant comprising unwinding means for unwinding at least one coil of rolled strip and pickling means for pickling said rolled strip; wherein there are provided measuring means for measuring the thickness of the superficial layer of oxide, arranged between said unwinding means and said pickling means. A relating cleaning method is also claimed.