Microbubble Integrated Structure Manufacturing via Microfluidics

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Solution Overview

Problem

Current methods for manufacturing three-dimensional graphene structures face limitations in controlling size and shape, leading to low structural stability and limited applications in electronic materials, while methods for producing non-spherical bubbles are complex and inefficient.

Innovation Solution

A method involving the formation of microbubbles using a microfluidic system, followed by self-assembly and drying to create two-dimensional or three-dimensional integrated structures with controlled sizes and shapes, utilizing alkylated two-dimensional nanosheets to achieve lightweight and high-stiffness materials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional methods (hydrothermal, freeze-drying, sol-gel) are used to manufacture three-dimensional graphene structures, then the structures can be formed, but the size and shape control is limited and structural stability is insufficient

Engineering Contradiction:
Improvesize and shape controlVSAvoidstructural stability
Core Design Contradiction:
Manufacturing precisionVSStability of the object's composition

Solution Approach 1:

The patent changes the fundamental parameter of bubble formation from conventional mixing methods to microfluidic-based controlled gas injection. By controlling flow rates, pressure, and channel dimensions in the microfluidic system, the patent achieves precise control over microbubble size (diameter) and shape, while the resulting structures exhibit enhanced stability

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces conventional mechanical mixing methods (stirring, ultrasonic decomposition, high-speed shear mixing) with a microfluidic system that uses controlled fluid flow and pressure to generate microbubbles. This substitution enables precise control over bubble formation, size, and shape, resolving the contradiction between manufacturing precision and structural stability

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Ease of manufacture

If simple bubble formation methods are used, then spherical microbubbles are easily produced, but uniform distribution size control is difficult and structural stability is low

Engineering Contradiction:
Improvebubble formation simplicityVSAvoiduniform distribution size control
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent introduces a microfluidic system as an intermediary device between the gas source and the liquid phase. This intermediary provides controlled interfaces (channels, membranes) that mediate the gas-liquid interaction, enabling uniform microbubble formation with precise size control while maintaining ease of manufacture through a standardized platform

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent changes the formation mechanism from spontaneous bubble generation to controlled microfluidic injection. By adjusting parameters such as flow rate ratios, pressure differential, and channel geometry, the system achieves uniform microbubble sizes while keeping the manufacturing process simple and scalable

Inventive Principle:
Principle #35Parameter changes

3Manufacturing precision

If sacrificial template method is used to manufacture hollow particles, then hollow structures can be formed, but manufacturing time is long and productivity is low

Engineering Contradiction:
Improvehollow structure formationVSAvoidmanufacturing time and productivity
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The patent extracts and eliminates the sacrificial template step entirely. Instead of forming hollow particles through template removal, the microfluidic system directly generates hollow microbubbles by controlling gas-liquid interface formation. This direct formation approach maintains hollow structure precision while dramatically reducing manufacturing time and increasing productivity

Inventive Principle:
Principle #2Taking out (Extraction)

4Adaptability or versatility

If non-spherical bubble formation is attempted, then different characteristics (filling, optical, electrical) can be achieved, but manufacturing complexity increases

Engineering Contradiction:
Improveshape characteristicsVSAvoidmanufacturing complexity
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent uses parameter changes in the microfluidic system (channel geometry, flow rate ratios, pressure control) to generate non-spherical microbubbles. By modifying these parameters, the system can produce various shapes (spherical, ellipsoidal, cylindrical) without increasing manufacturing complexity, as all shapes are achieved through the same microfluidic platform with adjustable parameters

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method enables the production of ultra-lightweight, high-stiffness integrated structures with controlled structural characteristics, overcoming the limitations of existing techniques and providing enhanced stability and versatility for various applications.

Implementation Method 1

a gas phase is injected into a liquid phase using a fine single/multichannel or porous multi-channel (membrane) including a microfluidic system

Methodology Applied
Scientific EffectGas injection through microfluidic system:

Implementation Method 2

a process in which bubbles are generated using ultrasonic waves (20 kHz or more)

Methodology Applied
Scientific EffectUltrasonic cavitation: Acoustic Cavitation

Implementation Method 3

inducing self-assembly of the microbubbles by buoyancy to form a structure under a condition of a height difference of a liquid level

Methodology Applied
Scientific EffectBuoyancy: Archimedes' Principle (Buoyancy)

Implementation Method 4

a third step of drying the structure

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS11123696B2Microbubble integrated structure and method of manufacturing the same
Publication Date: 2021.09.21 RES & BUSINESS FOUND SUNGKYUNKWAN UNIV
  • US11123696B2 patent drawing
  • US11123696B2 patent drawing
  • US11123696B2 patent drawing

AI summary

The present invention relates to a method of manufacturing an integrated structure using microbubbles, and an integrated structure manufactured by the method.