Microfluidic Phase Behavior Analysis Using Optical Detection

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Solution Overview

Problem

Conventional PVT measurements of reservoir fluids are time-consuming and require large volumes of fluid, posing logistical and safety challenges due to high pressures, and existing microfluidic solutions have limitations in efficiently analyzing phase behavior properties.

Innovation Solution

A microfluidic device with a serpentine microchannel and deformable membranes for pressure measurement, combined with optical sensing and image processing to distinguish gas and liquid phases, allowing for rapid estimation of phase states and properties at multiple locations along the channel.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional PVT measurements are performed using a cylinder and piston, then accurate phase behavior analysis is achieved, but the measurement process takes up to a few weeks to complete

Engineering Contradiction:
Improvephase behavior analysis accuracyVSAvoidmeasurement time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent replaces the mechanical cylinder-piston system with a microfluidic device that uses capillary forces and surface tension to control fluid phases. This substitution enables rapid phase behavior analysis by eliminating the need for slow mechanical compression and expansion cycles, reducing measurement time from weeks to hours while maintaining accuracy through optical detection of phase transitions.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention changes the measurement parameters by using small volume samples (microliters instead of liters) and operating at reduced pressures compared to conventional methods. This allows rapid equilibrium to be reached in the microchannel, enabling quick phase behavior characterization without the time-consuming high-pressure maintenance required by traditional PVT cells.

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If conventional PVT measurements are performed, then comprehensive fluid properties are obtained, but substantial volumes of reservoir fluid (up to 4 liters) must be maintained at high pressures

Engineering Contradiction:
Improvefluid properties characterizationVSAvoidfluid sample volume
Core Design Contradiction:
Measurement precisionVSQuantity of substance

Solution Approach 1:

The patent replaces bulk mechanical PVT measurement with microfluidic capillary-based measurement, requiring only microliter-scale samples. The microchannel geometry and surface properties enable phase behavior analysis of small fluid volumes, eliminating the need to transport and maintain large high-pressure samples while achieving comparable characterization accuracy through optical phase detection.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The invention transitions from three-dimensional bulk fluid measurement to two-dimensional interfacial measurement in the microchannel. By measuring phase behavior at the liquid-gas interface in the microchannel rather than in bulk, the system achieves accurate phase characterization with minimal fluid volume, as the measurement is based on interfacial phenomena visible through the channel walls.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Measurement precision

If conventional PVT measurements are performed with large fluid volumes at high pressures, then accurate phase behavior data is obtained, but shipping and handling becomes costly and poses safety issues

Engineering Contradiction:
Improvephase behavior data accuracyVSAvoidsafety risks and handling costs
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The patent replaces high-pressure bulk fluid handling with low-pressure microfluidic flow, eliminating safety hazards associated with transporting liters of high-pressure reservoir fluid. The microdevice operates at atmospheric or near-atmospheric pressures, allowing safe handling and shipping of minimal fluid volumes while maintaining measurement accuracy through precise optical detection of phase states in the microchannel.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables rapid and efficient analysis of phase behavior properties, reducing the need for large fluid samples and minimizing safety risks, while providing accurate measurements comparable to conventional methods.

Implementation Method 1

an optical sensing system arranged to generate a plurality of digital images of the fluid in the microchannel

Methodology Applied
Scientific EffectOptical sensing: Absorption (EM radiation)

Implementation Method 2

A processing system then distinguished gas from liquid phases In the digital images

Methodology Applied
Scientific EffectImage processing: Image Processing

Data Source

PatentEP2460004B1Phase behavior analysis using a microfluidic platform
Publication Date: 2014.09.03 SERVICES PETROLIERS SCHLUMBERGER SA
  • EP2460004B1 patent drawingFigure 1~2
  • EP2460004B1 patent drawingFigure 3~4
  • EP2460004B1 patent drawingFigure 5

AI summary

Methods and related systems are described for analyzing phase properties in a microfluidic device. A fluid is introduced under pressure into microchannel, and phase states of the fluid are optically detected at a number of locations along the microchannel. Gas and liquid phases of the fluid are distinguished based on a plurality of digital images of the fluid in the microchannel. Bi-level images can be generated based on the digital images, and the fraction of liquid or gas in the fluid can be estimated versus pressure based on the bi-level images. Properties such as bubble point values and/or a phase volume distribution ratio versus pressure for the fluid are can be estimated based on the detected phase states of the fluid.