Microwave Reactor Gas-Solids Separation with Cyclone and Back-Pulse Filter

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Solution Overview

Problem

Microwave chemical processing systems face challenges in effectively filtering small carbon-containing particles from hydrogen gas streams, as these particles are difficult to separate due to their small size and low density, leading to inefficiencies in gas-solids separation and increased costs.

Innovation Solution

A multi-stage gas-solid separator system is implemented, comprising a cyclone separator and a back-pulse filter system, which filters carbon particles from the hydrogen gas stream, allowing for efficient separation of carbon particles and maintaining high collection efficiency even at high gas flows.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional single-stage filtration systems are used, then device complexity is reduced, but particle separation efficiency deteriorates due to inability to effectively filter small carbon particles

Engineering Contradiction:
Improveparticle separation efficiencyVSAvoidfiltration system complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The filtration system is divided into multiple stages: a cyclone separator for coarse particle removal followed by a back-pulse filter for fine particle filtration. This segmentation allows each stage to be optimized for its specific particle size range, achieving high overall separation efficiency while managing system complexity through modular design

Inventive Principle:
Principle #1Segmentation

2Productivity

If high gas flow rates are used, then productivity is improved, but particle collection efficiency deteriorates due to reduced residence time for separation

Engineering Contradiction:
Improvegas flow rateVSAvoidparticle collection efficiency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The two-stage filtration system allows the first stage (cyclone) to handle high gas flows for bulk particle removal, while the second stage (back-pulse filter) operates at optimized flow rates for fine particle capture. This segmentation enables the system to maintain high productivity while achieving efficient particle collection across different flow conditions

Inventive Principle:
Principle #1Segmentation

3Manufacturing precision

If heated filters are used, then particle filtration is improved by preventing particle adhesion, but energy consumption increases due to heating requirements

Engineering Contradiction:
Improveparticle filtration efficiencyVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The back-pulse filter uses periodic reverse flow pulses to clear accumulated particles from the filter element instead of continuous heating. This periodic mechanical cleaning action prevents particle adhesion and maintains filtration efficiency without the continuous energy input required by heated filters, significantly reducing energy consumption

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The system achieves high collection efficiencies (>99%) of carbon particles, reducing operational costs and improving the purity of hydrogen gas, while being compatible with hot separated components and integrated with microwave plasma reactors without disrupting gas flows or oxygen levels.

Implementation Method 1

The gas-solids separation systems can contain cyclone filters

Methodology Applied
Scientific EffectCyclone separation: Cyclone Separation

Implementation Method 2

a first cyclone separator having an output, where the first cyclone separator filters the carbon particles from the separated components

Methodology Applied
Scientific EffectCentrifugal force: Centrifugal Force

Implementation Method 3

the back-pulse filters are periodically cleared by blowing gas through the filter candles to dislodge carbon-containing particles

Methodology Applied
Scientific EffectBack-pulse filtration:

Implementation Method 4

blowing gas through the filter candles

Methodology Applied
Scientific EffectGas flow:

Implementation Method 5

Microwave plasmas are used in the industrial chemical processing of gases. This is typically accomplished by flowing the gases to be reacted through an elongated vessel while microwave energy is coupled into the vessel to generate a plasma. The plasma cracks the gas molecules into component species

Methodology Applied
Scientific EffectMicrowave plasma: Plasma

Implementation Method 6

microwave energy is coupled into the vessel to generate a plasma

Methodology Applied
Scientific EffectMicrowave energy coupling: Microwave Radiation

Data Source

PatentUS10781103B2Microwave reactor system with gas-solids separation
Publication Date: 2020.09.22 LYTEN INC
  • US10781103B2 patent drawing
  • US10781103B2 patent drawing
  • US10781103B2 patent drawing

AI summary

Microwave chemical processing system having a microwave plasma reactor, and a multi-stage gas-solid separation system are disclosed. The microwave energy source has a waveguide, a reaction zone, and an inlet configured to receive the input material, and the input material is converted into separated components. The separated components include hydrogen gas and carbon particles. The multi-stage gas-solid separation system has a first cyclone separator to filter the carbon particles from the separated components, and a back-pulse filter system coupled to the output of the first cycle separator to filter the carbon particles from the output from the first cyclone separator.