Multi-Channel Gas Injection System for Focused Beam Processing

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Solution Overview

Problem

Existing Gas Injection Systems (GIS) face issues with gas shadowing effects on uneven surfaces, limited tilt capabilities, and uneven distances between nozzles and the sample, which affect gas coverage and pressure in the vacuum chamber during focused-beam processing.

Innovation Solution

The implementation of a multi-channel GIS with concentric nozzles, where one channel is connected to a positioning unit and another is detachably mounted, allowing for improved nozzle placement and mixing of gases after exit, reducing shadowing and tilt limitations, and enabling the delivery of gases with significantly different fluxes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If a single nozzle is used and positioned close to the sample, then gas coverage is concentrated and background pressure is low, but gas shadowing effects occur on uneven surfaces and tilt capability is limited

Engineering Contradiction:
Improvegas coverage concentrationVSAvoidgas shadowing effects
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The single nozzle is segmented into multiple nozzles (typically three nozzles arranged in a triangular pattern) that are detachably mounted on the first channel. This segmentation allows gas to be delivered from multiple directions, eliminating shadowing effects on uneven surfaces while maintaining concentrated gas coverage at the sample location.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The nozzles are positioned in a three-dimensional arrangement around the beam path rather than in a single plane. By distributing nozzles in multiple spatial dimensions (e.g., triangular arrangement with vertices at different positions), the system achieves omnidirectional gas coverage that accommodates sample tilt in multiple axes without creating shadowing zones.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Object-affected harmful factors

If two opposing nozzles are used, then gas shadowing is avoided, but the distance between nozzles must be large enough to let the beam pass, reducing nozzle proximity to sample

Engineering Contradiction:
Improvegas shadowing effectsVSAvoiddistance from nozzle to sample
Core Design Contradiction:
Object-affected harmful factorsVSLength of moving object

Solution Approach 1:

Each nozzle is positioned locally optimized for its specific function, with individual positioning units that allow independent adjustment of each nozzle's location and orientation. This enables each nozzle to be placed as close as possible to the sample while maintaining the overall geometric arrangement that prevents shadowing, as each nozzle contributes to gas coverage from its specific local position.

Inventive Principle:
Principle #3Local quality

3Stability of the object's composition

If multiple nozzles are used for gas delivery, then gas coverage uniformity is improved, but device complexity increases

Engineering Contradiction:
Improvegas coverage uniformityVSAvoidnumber of nozzles and mounting mechanisms
Core Design Contradiction:
Stability of the object's compositionVSDevice complexity

Solution Approach 1:

The first channel with positioning unit serves as a universal platform that can accommodate different nozzle configurations and types. The positioning unit can adjust any nozzle to any required position and orientation, making the system universally adaptable to various experimental requirements without requiring separate dedicated mechanisms for each nozzle, thereby reducing overall complexity.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The nozzles are nested on the first channel in a hierarchical structure where multiple nozzles are mounted on a single positioning platform. This nesting allows all nozzles to be controlled by a single positioning unit, reducing the number of independent control systems needed and simplifying the overall device architecture while maintaining the ability to deliver uniform gas coverage.

Inventive Principle:
Principle #7Nested doll (Nesting)

4Productivity

If nozzles are positioned close to the sample, then gas delivery efficiency is high, but tilt capability is limited by nozzle-sample distance changes

Engineering Contradiction:
Improvegas delivery efficiencyVSAvoidtilt capability
Core Design Contradiction:
ProductivityVSAdaptability or versatility

Solution Approach 1:

The positioning unit is designed with dynamic adjustment capabilities that allow real-time modification of nozzle positions and orientations in response to sample tilt. The nozzles can be dynamically repositioned to maintain optimal spacing and angles relative to the tilted sample surface, preserving gas delivery efficiency across the full range of tilt angles without requiring large fixed distances.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration minimizes gas shadowing, enhances gas coverage uniformity, allows for closer nozzle placement to the sample, and facilitates the production of high-purity, dense metal structures with reduced processing time by ensuring consistent gas delivery and efficient removal of contaminants like carbon.

Implementation Method 1

allowing mixing of gases after exit, reducing shadowing and tilt limitations, and enabling the delivery of gases with significantly different fluxes

Methodology Applied
Scientific EffectGas flow:

Implementation Method 2

one channel is connected to a positioning unit for positioning the GIS, allowing for improved nozzle placement

Methodology Applied
Scientific EffectPositioning:

Implementation Method 3

another channel is detachably mounted on the first channel, allowing for improved nozzle placement and mixing of gases after exit

Methodology Applied
Scientific EffectGas mixing: Diffusion

Data Source

PatentEP3062329B1Multi-source GIS for particle-optical apparatus
Publication Date: 2016.12.14 FEI CO
  • EP3062329B1 patent drawingFigure 1~2
  • EP3062329B1 patent drawingFigure 3
  • EP3062329B1 patent drawingFigure 4~500c

AI summary

The invention relates to a Gas Injection System (GIS) for applying at least two fluids in the vacuum chamber of a particle-optical apparatus, the gas injection system having two or more channels(102, 110), each channel connected to an associated reservoir holding a fluid at a first side and having an associated exit opening at the other side, the exit sides individually exiting to the outside of the GIS via a nozzle with a nozzle opening, characterized in that at least two exit openings (106, 108) are separated by less than the diameter of the channels near the exit openings, preferably concentric to each other. The invention further relates to the use of said GIS in which the central nozzle directs a high flux of, for example, oxygen while the outer concentric nozzle directs a metal precursor, for example MeCpPtMe3, to the sample with a flux that is less than two orders of magnitude less. By the high flux of oxygen a purified metal is deposited in a one-step deposition method. The nozzle can be formed as an add-on nozzle so that an existing GIS can be upgraded. The nozzle is preferably manufactured by a 3-D printing technique using for example titanium.