Nanoparticle Recognition via Scattered Light Dipole Rotation

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Solution Overview

Problem

Current nanoparticle recognition methods in vacuum optical tweezers are inefficient due to random particle trapping, high vacuum requirements, and incompatibility with existing scanning technologies, leading to complex and time-consuming processes for particle identification and measurement.

Innovation Solution

A nanoparticle recognition device and method utilizing detection of scattered light with electric dipole rotation, employing a combination of trapping and probe lasers, polarization adjustment, and photodetection to identify and calculate nanoparticle size and morphology based on light intensity changes, allowing for real-time detection at room pressure and improved resolution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If vacuum optical tweezers are used for nanoparticle recognition, then particles can be isolated from environment, but the process requires frequent vacuumization and recovery time

Engineering Contradiction:
Improveisolation from environmentVSAvoidvacuumization and recovery time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent changes the operating pressure parameter from vacuum to atmospheric pressure, eliminating the need for vacuumization while maintaining particle isolation through the optical trap itself. This allows continuous operation without vacuum cycle interruptions.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent extracts the particle isolation function from the vacuum environment and transfers it to the optical trap mechanism, allowing particles to be contained and manipulated independently at atmospheric pressure without requiring vacuum conditions.

Inventive Principle:
Principle #2Taking out (Extraction)

2Measurement precision

If direct imaging methods (electron beam scanning or atomic force microscopy) are used for nanoparticle detection, then imaging resolution is improved, but the scanning technologies are incompatible with optical trap platform

Engineering Contradiction:
Improveimaging resolutionVSAvoidcompatibility with optical trap
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent replaces mechanical scanning methods (electron beam or atomic force microscopy) with optical detection methods. By using light scattering and polarization changes, the system achieves high-resolution nanoparticle characterization without mechanical contact, maintaining compatibility with the optical trap platform.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent creates a universal detection system that uses optical methods to simultaneously achieve particle trapping, positioning, and characterization. The same optical infrastructure serves multiple functions, eliminating the need for separate incompatible scanning systems.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Measurement precision

If conventional vacuum measurement methods are used, then particle size can be calculated, but measurement accuracy depends on accurate measurement of molecular radius, vacuum degree and beam waist size

Engineering Contradiction:
Improveparticle size measurementVSAvoidmeasurement parameters required
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent extracts the particle size measurement from the complex vacuum thermodynamic method and creates a direct optical measurement approach. By measuring light scattering intensity and polarization changes, particle size is determined directly without needing to measure vacuum degree, molecular radius, or beam waist size separately.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent uses light scattering patterns as an optical copy or fingerprint of particle characteristics. By analyzing the scattered light properties, all particle parameters (size, shape, composition) are inferred from the optical signature rather than requiring multiple separate measurements.

Inventive Principle:
Principle #26Copying

4Productivity

If room pressure particle delivery is used, then delivery efficiency is improved, but vacuumization is required for measurement causing time consumption

Engineering Contradiction:
Improveparticle delivery efficiencyVSAvoidvacuumization time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent changes the pressure parameter from vacuum to atmospheric pressure for the entire measurement process. This allows particles to be delivered efficiently at room pressure and measured immediately without requiring vacuumization, eliminating the time loss associated with pressure transitions.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method simplifies particle recognition, reduces vacuumization needs, enhances detection resolution, and provides a cost-effective alternative to SEM and AFM for nanoparticle analysis, enabling real-time detection and accurate sizing of nanoparticles.

Implementation Method 1

a laser beam is used to suspend particles, and it can be understood by a harmonic oscillator model

Methodology Applied
Scientific EffectOptical radiation pressure: Radiation Pressure

Implementation Method 2

detection of scattered light with electric dipole rotation

Methodology Applied
Scientific EffectLight scattering: Scattering

Implementation Method 3

the polarization direction is changed, and a change rate of the light intensity of the scattered light of the particles is obtained

Methodology Applied
Scientific EffectElectric dipole rotation:

Data Source

PatentUS11774344B2Nanoparticle recognition device and method based on detection of scattered light with electric dipole rotation
Publication Date: 2023.10.03 ZHEJIANG LAB
  • US11774344B2 patent drawing
  • US11774344B2 patent drawing

AI summary

The present application discloses a nanoparticle recognition device and method based on detection of scattered light with electric dipole rotation. According to the scattering model of nanoparticles, the in situ detection of particle morphology in an optical trap is realized by the methods of particle suspension control and scattered light detection and separation. Specifically, two linearly polarized laser beams are used, wherein the first laser beam suspends nanoparticles and rotates nanoparticles by adjusting the polarization direction; the polarization direction of the second linearly polarized light is unchanged, and scattered light in a specific dipole direction is excited; the change of the polarizability of the nanoparticles is deduced by monitoring the change of the light intensity of the scattered light excited by the second laser beam at the fixed position, so that particle morphology recognition is realized.