Nitrided Steel Component with Thin Compound Layer for Bending

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Solution Overview

Problem

Nitrided steel parts face challenges with low toughness and deformability due to a thick compound layer, which affects their bending straightening ability and fatigue characteristics, and existing methods to reduce the compound layer thickness either compromise fatigue strength or increase production costs.

Innovation Solution

A two-stage gas nitriding process is employed, initially forming a compound layer with a high nitriding potential (high K N value) followed by a low nitriding potential treatment to break down the compound layer, promoting a deeper nitrogen diffused layer while maintaining surface hardness and reducing voids, using a specific steel composition and controlled nitriding conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If gas nitriding is performed to form a compound layer, then wear resistance and pitting resistance are improved, but toughness and deformability decrease

Engineering Contradiction:
Improvewear resistanceVSAvoidtoughness
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent applies parameter changes by controlling the nitriding potential (K N value) within a specific range (0.05 to 0.40) to optimize the compound layer thickness. By adjusting this parameter, the patent achieves a balance between wear resistance (improved by compound layer) and toughness (maintained by limiting compound layer thickness to 5 μm or less).

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates local quality differences by forming a compound layer with specific phase composition (γ' phase content of 30-70%) and thickness (5 μm or less) only in the surface region. This allows the surface to have high wear resistance while the underlying material maintains its toughness and deformability.

Inventive Principle:
Principle #3Local quality

2Stability of the object's composition

If the thickness of the compound layer is reduced to improve toughness, then bending straightening ability improves, but wear resistance may decrease

Engineering Contradiction:
Improvebending straightening abilityVSAvoidwear resistance
Core Design Contradiction:
Stability of the object's compositionVSStrength

Solution Approach 1:

The patent uses parameter changes by precisely controlling the nitriding potential (K N = 0.05 to 0.40) and treating temperature (500-600°C) to achieve optimal compound layer thickness (≤5 μm). This parameter optimization ensures both adequate wear resistance and sufficient bending straightening ability.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure with a thin compound layer (≤5 μm) containing specific phases (γ' and ε) overlying a nitrogen-diffused hardened layer. This composite configuration provides wear resistance from the compound layer while maintaining ductility and bending straightening ability through the controlled thickness and phase composition.

Inventive Principle:
Principle #40Composite materials

3Length of stationary object

If the nitriding potential K N is lowered to reduce compound layer thickness, then compound layer thickness decreases, but nitrogen diffusion into steel becomes difficult

Engineering Contradiction:
Improvecompound layer thicknessVSAvoidnitrogen diffusion
Core Design Contradiction:
Length of stationary objectVSQuantity of substance

Solution Approach 1:

The patent applies parameter changes by optimizing the nitriding potential to a specific range (K N = 0.05 to 0.40) that simultaneously achieves two goals: limiting compound layer thickness to 5 μm or less while ensuring adequate nitrogen diffusion to form a hardened layer with effective depth of 100 μm or more. This precise parameter control resolves the contradiction between thin compound layer and sufficient nitrogen diffusion.

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If mechanical polishing or shot blasting is used to remove the compound layer, then bending straightening ability improves, but production costs increase

Engineering Contradiction:
Improvebending straightening abilityVSAvoidproduction cost
Core Design Contradiction:
Stability of the object's compositionVSEase of manufacture

Solution Approach 1:

The patent applies preliminary action by controlling the nitriding process parameters (K N value and temperature) in advance to directly produce a compound layer with optimal thickness (≤5 μm) and phase composition. This preliminary control eliminates the need for subsequent mechanical polishing or shot blasting operations, thereby reducing production costs while achieving the desired bending straightening ability.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in a nitrided steel part with a thin compound layer, high surface hardness, deep hardened layer, and improved bending straightening ability and fatigue characteristics, while minimizing voids and production costs.

Implementation Method 1

Nitriding is a method of treatment diffusing nitrogen into the surface of a steel material

Methodology Applied
Scientific EffectNitriding: Nitriding

Implementation Method 2

diffusing nitrogen into the surface of a steel material

Methodology Applied
Scientific EffectDiffusion: Diffusion

Data Source

PatentEP3348664B1Nitrided steel component and manufacturing method thereof
Publication Date: 2020.06.24 NIPPON STEEL CORPORATION
  • EP3348664B1 patent drawingFigure 1(a)~1(b)
  • EP3348664B1 patent drawingFigure 2
  • EP3348664B1 patent drawingFigure 3

AI summary

A nitrided steel part excellent in bending straightening ability and bending fatigue characteristic enabling reduction of size and decrease of weight of parts or enabling demand for high load capacities to be met, using as a material a steel material containing, by mass%, C: 0.2 to 0.6%, Si: 0.05 to 1.5%, Mn: 0.2 to 2.5%, P: 0.025% or less, S: 0.003 to 0.05%, Cr: 0.05 to 0.5%, Al: 0.01 to 0.05%, and N: 0.003 to 0.025%, and having a balance of Fe and impurities, having formed on the steel surface a compound layer of a thickness 3 µm or less comprising iron, nitrogen, and carbon and a hardened layer formed below the compound layer, and having an effective hardened layer depth of 160 to 410 µm.