Oxidized Cellulose Multi-Encapsulated Formulations

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Solution Overview

Problem

Current cellulose dissolution processes are cumbersome, expensive, and require harsh conditions, leading to degradation and limited solubility, which hinders the full exploitation of cellulose potential.

Innovation Solution

A process involving the use of a polar aprotic solvent and a salt under an inert atmosphere, with controlled temperature and salt concentration to minimize degradation and enhance solubility, allowing for the formation of modified cellulose solutions with preserved molecular weight and degree of oxidation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If conventional methods (co-suspension, co-emulsion, co-precipitation) are used to prepare multi-encapsulated formulations, then multiple active ingredients can be delivered simultaneously, but the formulations suffer from poor flow properties, caking, and lack of freedom of formulation design

Engineering Contradiction:
Improvefreedom of formulation designVSAvoidflow properties and caking
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The patent uses oxidized cellulose as a composite material that combines the properties of a disintegrant and a binder into one component. This composite approach allows simultaneous delivery of multiple active ingredients while maintaining good flow properties and preventing caking, resolving the contradiction between formulation versatility and manufacturing ease.

Inventive Principle:
Principle #40Composite materials

2Adaptability or versatility

If multiple excipients are used in conventional formulations, then various functions can be achieved, but the number of manufacturing steps and potential for interaction increases

Engineering Contradiction:
Improvefunctional capabilitiesVSAvoidnumber of manufacturing steps
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent merges the functions of multiple excipients (disintegrant, binder, flow agent) into a single oxidized cellulose component. This consolidation reduces the number of manufacturing steps and potential interactions while maintaining all necessary functional capabilities, directly addressing the contradiction between versatility and complexity.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

Oxidized cellulose serves multiple functions simultaneously as a disintegrant, binder, and flow agent. This multi-functionality allows the formulation to achieve various excipient functions with a single component, reducing manufacturing complexity while preserving functional versatility.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Device complexity

If oxidized cellulose is used as a multi-functional excipient, then the number of manufacturing steps is reduced and formulation design freedom increases, but questions remain about its ability to simultaneously provide disintegration, binding, and flow properties

Engineering Contradiction:
Improvenumber of manufacturing stepsVSAvoidsimultaneous provision of multiple functions
Core Design Contradiction:
Device complexityVSReliability

Solution Approach 1:

The patent utilizes the specific chemical parameters of oxidized cellulose (oxidation degree, molecular weight, surface area) to optimize its multi-functional performance. By controlling these parameters, the formulation reliably provides disintegration, binding, and flow properties simultaneously, ensuring reliability while maintaining simplicity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process effectively dissolves cellulose with minimal degradation, maintaining a high degree of oxidation and molecular weight, facilitating the formation of stable modified cellulose solutions suitable for various applications.

Implementation Method 1

The disintegrant is effective in promoting disintegration of the compressed core upon contact with liquid

Methodology Applied
Scientific EffectAbsorption: Absorption (physical)

Implementation Method 2

The binder is effective in binding particles together

Methodology Applied
Scientific EffectAdhesion: Adhesive

Data Source

PatentEP2895151B1Multi-encapsulated formulations made with oxidized cellulose
Publication Date: 2020.02.19 COVIDIEN LP
  • EP2895151B1 patent drawingFigure 1~5
  • EP2895151B1 patent drawingFigure 6~10
  • EP2895151B1 patent drawingFigure 11~12

AI summary

A microsphere and method for forming the same are disclosed. The microsphere includes modified cellulose and at least one of a visualization agent, a magnetic material, or a radioactive material.