Particle Sizing via Interferometric Light Recombination

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Solution Overview

Problem

Existing particle sizing instruments face difficulties in distinguishing small particles near the Rayleigh limit due to nearly isotropic scattering patterns, making it challenging to accurately determine particle size or distribution.

Innovation Solution

The instrument employs an optical path adjuster to vary the interference signal by splitting and recombining scattered light using optical fibres and lenses, generating an interference pattern that improves the differentiation of particle sizes near the Rayleigh limit, enhancing the signal-to-noise ratio and allowing for more precise particle size analysis.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional non-interferometric light scattering is used for particle sizing, then the measurement method is simple and straightforward, but the ability to distinguish small particles near the Rayleigh limit is severely limited due to nearly isotropic scattering patterns

Engineering Contradiction:
Improveparticle size differentiation capabilityVSAvoidoptical system complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The scattered light is segmented into multiple portions using optical elements (lenses, mirrors, beam splitters) that direct different angular ranges of scattered light to separate detection zones. This segmentation allows the interferometric system to capture and analyze subtle differences in scattering patterns that would be indistinguishable in conventional isotropic detection, thereby improving particle size differentiation capability near the Rayleigh limit.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

An interferometric optical system acts as an intermediary between the particle sample and the detector. By introducing reference beams and creating interference patterns, the system transforms the nearly isotropic scattering signals into distinguishable interferometric patterns that encode particle size information, effectively mediating the detection process to overcome the limitations of direct conventional scattering measurement.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Measurement precision

If the detection system uses interferometric patterns to improve particle size resolution, then the signal-to-noise ratio is enhanced, but the optical path complexity and alignment requirements increase

Engineering Contradiction:
Improvesignal-to-noise ratioVSAvoidoptical path complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

Multiple scattered light portions carrying different angular information are merged through interferometric recombination. The optical system combines these segmented light paths with precise phase control, creating constructive and destructive interference patterns that amplify the signal-to-noise ratio for particle size detection while integrating multiple measurement channels into a unified detection scheme.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The detection approach transitions from measuring only light intensity (one dimension) to measuring interferometric phase and intensity distributions (multiple dimensions). By capturing the spatial and phase information of scattered light across different optical paths, the system adds dimensional complexity to the measurement space, enabling superior particle size resolution that compensates for the increased optical path complexity.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables improved resolution and accuracy in particle sizing, particularly for smaller particles, and extends the range of characterizable particle sizes by distinguishing similar interference patterns more effectively than non-interferometric methods.

Implementation Method 1

The second optical system recombines the first and second portions of scattered light to produce an interference pattern at a detection location

Methodology Applied
Scientific EffectInterference: Interference

Implementation Method 2

The optical path adjuster may be configured to adjust an optical path length for the first portion of scattered light (e.g. to the second optical system), relative to an optical path length for the second portion of scattered light

Methodology Applied
Scientific EffectOptical path length adjustment:

Implementation Method 3

The first element of the first optical system may be configured to receive a first portion of the scattered light and to modify the convergence of the first portion of scattered light communicated to the second optical system

Methodology Applied
Scientific EffectRefraction: Refraction

Data Source

PatentEP3762703B1Improved particle sizing by optical diffraction
Publication Date: 2023.02.22 MALVERN INSTRUMENTS
  • EP3762703B1 patent drawingFigure 1~2
  • EP3762703B1 patent drawingFigure 3
  • EP3762703B1 patent drawingFigure 4~5A

AI summary

A particle-sizing instrument is provided, comprising: a sample cell (10) for receiving a sample (12) comprising a plurality of particles; a light source (4) configured to illuminate the sample (12) with a light beam (8) to produce scattered light by the interaction of the light beam (8) with the particles; a first optical system (30) comprising a first and second optical element (31, 32) respectively configured to split a portion of the scattered light into a first and second portion of scattered light: a second optical system (40) configured to receive the first and second portion of scattered light from the first optical system (30), and to recombine the first and second portion of scattered light to produce an interference signal (25) at a detection location, and a detector (14) configured to detect the interference signal (25) at the detection location.