Photoactive Tuning Fork Probe for AFM Frequency Control

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Solution Overview

Problem

Atomic force microscopes, particularly frequency modulation AFMs, face challenges in achieving high resolution when probing samples with varying properties like liquids and solids due to increased vibration frequencies caused by surface interactions, requiring frequent tip modifications and complex control systems for piezoelectric elements.

Innovation Solution

An optomechanical transducer with a tuning fork made from piezoelectric material and partially coated with photoactive films containing photo-switchable molecules, allowing for precise modulation of resonance frequency through light-induced stiffness changes, enabling closer proximity to surfaces without additional equipment complexity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the probe is brought into very close proximity with the surface to improve resolution, then measurement precision is improved, but the vibration frequency increases undesirably causing reduction in resolution

Engineering Contradiction:
ImproveresolutionVSAvoidvibration frequency
Core Design Contradiction:
Measurement precisionVSSpeed

Solution Approach 1:

The patent changes the physical-chemical state of the tuning fork by depositing photoactive film material that can switch between different molecular configurations. This allows dynamic modification of the stiffness coefficient, thereby adjusting the resonance frequency to compensate for frequency increases caused by proximity to the surface.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a composite structure combining piezoelectric material with photoactive film (containing photo-switchable molecules). This composite allows the tuning fork to respond to both electrical actuation and optical control, enabling precise frequency modulation through light-induced stiffness changes.

Inventive Principle:
Principle #40Composite materials

2Speed

If piezoelectric elements are used to control vibration frequency, then frequency control is achieved, but device complexity and manufacturing cost increase

Engineering Contradiction:
Improvevibration frequency controlVSAvoidcontrol system complexity
Core Design Contradiction:
SpeedVSDevice complexity

Solution Approach 1:

The patent replaces the need for additional piezoelectric control elements with a photoactive film that responds to light. This substitutes a complex electrical control system with a simpler optical control mechanism, reducing device complexity while maintaining frequency control capability.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The photoactive film acts as an intermediary between light and the mechanical structure of the tuning fork. It translates optical energy into mechanical stiffness changes, providing a direct control mechanism that eliminates the need for additional piezoelectric control elements and complex control systems.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Adaptability or versatility

If tips are modified to measure heterogeneous samples (liquid and solid phases), then adaptability is improved, but ease of manufacture deteriorates

Engineering Contradiction:
Improvesample type adaptabilityVSAvoidtip modification difficulty
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The patent makes the tuning fork universally adaptable to different sample types (liquid, solid, viscous, rigid, flexible) by equipping it with photoactive film that allows real-time frequency adjustment. This single probe design replaces the need for multiple specialized tips, improving ease of manufacture while maintaining versatility.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent introduces dynamic adjustability to the probe through photoactive film that can change stiffness in real-time based on illumination. This allows the same probe to adapt its mechanical properties for different sample types during operation, eliminating the need for physical tip modifications and improving manufacturing simplicity.

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This solution enhances the resolution of frequency modulation AFMs by allowing real-time adjustment of vibration frequency, facilitating high-resolution imaging of diverse samples, including liquids and solids, without the need for frequent tip changes or additional control systems.

Implementation Method 1

the at least one photoactive film comprising photo-switchable molecules, suitable for a molecular switching between a first molecular configuration and a second molecular configuration in reaction to the absorption of light of a defined wavelength, called photo-isomerization wavelength, such that the photoactive film is subjected to a shape change

Methodology Applied
Scientific EffectPhoto-isomerization: Photochromism

Implementation Method 2

a tuning fork made from piezoelectric material comprising two arms

Methodology Applied
Scientific EffectPiezoelectric effect: Piezoelectric Effect

Implementation Method 3

A tuning fork has a resonance vibration frequency that is characteristic of its geometrical and mechanical properties, and in particular its stiffness

Methodology Applied
Scientific EffectResonance: Resonance

Data Source

PatentUS20240094240A1Optomechanical transducer
Publication Date: 2024.03.21 ECOLE NAT SUPERIEURE DINGS DE CAEN
  • US20240094240A1 patent drawing
  • US20240094240A1 patent drawing

AI summary

An optomechanical transducer, including a tuning fork made of piezoelectric material including two arms, at least one photoactive film partially deposited on at least one part of at least one of the arms of the tuning fork, the at least one photoactive film including photo-switchable molecules, suitable for molecular switching between a first molecular configuration and a second molecular configuration in response to the absorption of light at a defined, so-called photo-isomerisation wavelength, so that the photoactive film undergoes a shape change that induces a change in the stiffness coefficient of the tuning fork is disclosed. A probe is also provided for a frequency modulation atomic force microscope and to such a microscope.