Piezoelectric Substrate Bonding with Intermediate Silicon Layer

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Solution Overview

Problem

The bonding of piezoelectric material substrates and silicon substrates through a silicon oxide layer often results in fractures or cracks due to thermal expansion coefficient differences and residual stress, which deteriorates the frequency characteristics and effective resistivity of the bonded body.

Innovation Solution

A method involving physical vapor deposition to form a silicon film on a silicon substrate, followed by heat treatment between 400°C and 600°C to create an intermediate layer, which is then bonded with a piezoelectric material substrate using a silicon oxide bonding layer, reducing residual stress and improving effective resistivity across a wide frequency range.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If a silicon film is formed by CVD method at high temperature (400-1000°C), then the film can be successfully formed, but large residual stress remains in the film causing fracture of the bonded body

Engineering Contradiction:
Improvefilm formationVSAvoidbonded body integrity
Core Design Contradiction:
Ease of manufactureVSStrength

Solution Approach 1:

The patent changes the deposition temperature parameter from conventional high temperature (400-1000°C) to low temperature (room temperature or slightly elevated), which fundamentally alters the film formation mechanism and reduces residual stress while maintaining film quality

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the thermal field (CVD heating) with a chemical field (plasma or vapor phase reaction), allowing film formation without high temperature thermal stress, thus substituting a mechanical/thermal process with a chemical process

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If an amorphous Si film or polycrystalline Si film is formed to suppress fixed charges, then effective resistivity improves, but thermal expansion coefficient differences cause fracture during heating

Engineering Contradiction:
Improveeffective resistivityVSAvoidbonded body integrity
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

The patent changes the material structure parameter from amorphous/polycrystalline to single crystal silicon, which has superior mechanical strength and thermal stability, eliminating fracture issues while maintaining electrical performance

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite structure with single crystal silicon film on silicon substrate, combining the electrical benefits of silicon-based materials with the mechanical strength of single crystal structure to resist thermal stress

Inventive Principle:
Principle #40Composite materials

3Ease of manufacture

If CVD method is used to form silicon film, then film formation is achieved, but the process is time-consuming and produces large stress

Engineering Contradiction:
Improvefilm formation capabilityVSAvoidfilm formation time
Core Design Contradiction:
Ease of manufactureVSLoss of time

Solution Approach 1:

The patent replaces the thermal field (CVD heating) with a chemical field (plasma or vapor phase reaction), allowing film formation without high temperature thermal stress, thus substituting a mechanical/thermal process with a chemical process

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent skips the lengthy high-temperature annealing and stress-relief steps required by CVD by using low-temperature plasma or vapor deposition that forms low-stress films directly, reducing total process time

Inventive Principle:
Principle #21Skipping (Rushing through)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach effectively suppresses fractures and maintains high effective resistivity over a wide temperature range, enhancing the frequency characteristics of the bonded body while minimizing residual stress.

Implementation Method 1

a silicon film-forming step of forming a silicon film on a supporting substrate comprising silicon by physical vapor deposition method

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 2

a heat treatment step of subjecting the silicon film to heat treatment at a temperature of 400° C. or higher and 600° C. or lower to generate an intermediate layer

Methodology Applied
Scientific EffectHeat treatment: Heat Treatment

Data Source

PatentUS12101079B2Method of producing a bonded body of piezoelectric material substrate
Publication Date: 2024.09.24 NGK INSULATORS LTD
  • US12101079B2 patent drawing
  • US12101079B2 patent drawing
  • US12101079B2 patent drawing

AI summary

A silicon film is provided on a supporting substrate composed of silicon by physical vapor deposition. The silicon film is subjected to heat treatment at a temperature of 400° C. or higher and 600° C. or lower to generate an intermediate layer. The piezoelectric material substrate is bonded to the supporting substrate through a bonding layer of silicon oxide and the intermediate layer. A method of providing an acoustic wave element with a bonded body is also provided.