Pitch Hydrocracking Reactor for Residuum Upgrading

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Solution Overview

Problem

The existing hydrocracking processes for upgrading petroleum feedstocks, such as asphaltenic pitch, face challenges in converting pitch into valuable products due to high production costs, seasonal demand, and quality issues, leading to pitch being considered a low-value or undesirable byproduct.

Innovation Solution

A process involving hydrocracking a heavy oil feedstock in an ebullated bed hydrocracking reactor, followed by solvent deasphalting and feeding the pitch, hydrogen, and spent catalyst to a pitch hydrocracking reactor under specific temperature and pressure conditions to convert pitch into distillate hydrocarbons, thereby reducing pitch production and increasing conversion efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If reaction severity is increased to increase residuum conversion, then conversion efficiency improves, but pitch production increases

Engineering Contradiction:
Improveresiduum conversionVSAvoidpitch production
Core Design Contradiction:
ProductivityVSQuantity of substance

Solution Approach 1:

The patent converts the harmful byproduct pitch into a valuable feedstock by introducing a pitch hydrocracking reactor that processes pitch alongside spent catalyst and hydrogen to produce distillate hydrocarbons. This transforms the waste disposal problem into an additional revenue stream and improves overall process efficiency.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent changes the operational parameters by introducing a dedicated pitch hydrocracking reactor with specific temperature and pressure conditions optimized for pitch conversion. This allows the system to handle pitch as a separate stream with appropriate processing conditions, preventing pitch accumulation while maintaining high residuum conversion.

Inventive Principle:
Principle #35Parameter changes

2Adaptability or versatility

If pitch is converted to fuel oil using lighter cutter stock, then pitch utilization improves, but the process requires very high volume of lighter cutter stock

Engineering Contradiction:
Improvepitch utilizationVSAvoidlighter cutter stock volume
Core Design Contradiction:
Adaptability or versatilityVSQuantity of substance

Solution Approach 1:

The pitch hydrocracking reactor uses spent catalyst from the ebullated bed reactor to catalyze pitch conversion, eliminating the need for external catalyst inputs. The system essentially uses its own spent catalyst to process its own byproduct, creating a self-sufficient loop that reduces external material requirements.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent changes the conversion approach from blending with lighter cutter stock to hydrocracking with hydrogen and spent catalyst. This fundamental parameter change transforms pitch into distillate hydrocarbons directly, eliminating the need for large volumes of lighter cutter stock while producing higher value products.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If spent catalyst is discarded after ebullated bed hydrocracking, then catalyst management simplifies, but catalyst resources are wasted

Engineering Contradiction:
Improvecatalyst managementVSAvoidcatalyst activity
Core Design Contradiction:
Ease of manufactureVSLoss of substance

Solution Approach 1:

The patent extends the useful life of the spent catalyst by continuously utilizing it in the pitch hydrocracking reactor. Instead of discarding the catalyst after single-use in the ebullated bed reactor, the system maintains continuous catalytic activity by deploying the spent catalyst to convert pitch, thereby eliminating waste and maximizing resource utilization.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The patent changes the catalyst application from single-use to multi-use by adjusting the operational parameters to suit pitch hydrocracking conditions. The spent catalyst from ebullated bed hydrocracking is repurposed for pitch conversion with appropriate temperature and pressure adjustments, extending its functional lifecycle.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces pitch production, enhances residuum hydrocarbon conversion rates, and eliminates the need for external units, achieving high conversion efficiencies with minimal additional catalyst requirements, thus addressing the value and quality issues of pitch in existing processes.

Implementation Method 1

hydrocracking a heavy oil feedstock in a hydrocracking reaction system comprising one or more hydrocracking reaction stages comprising an ebullated bed hydrocracking reactor

Methodology Applied
Scientific EffectHydrocracking: Chemical Bonding

Implementation Method 2

solvent deasphalting at least one of the two or more hydrocarbon fractions to produce a deasphalted oil fraction and a pitch

Methodology Applied
Scientific EffectSolvent extraction: Liquid-Liquid Extraction

Implementation Method 3

contacting the pitch, hydrogen, and the spent or partially spent catalyst stream in the pitch hydrocracking reactor at reaction conditions of temperature and pressure sufficient to convert at least a portion of the pitch to distillate hydrocarbons

Methodology Applied
Scientific EffectCatalytic hydrocracking: Catalysis

Implementation Method 4

contacting the pitch, hydrogen, and the spent or partially spent catalyst stream in the pitch hydrocracking reactor

Methodology Applied
Scientific EffectHydrogenation: Hydrogenation

Data Source

PatentEP2946000B1Conversion of asphaltenic pitch within an ebullated bed residuum hydrocracking process
Publication Date: 2019.07.24 LUMMUS TECHNOLOGY INC
  • EP2946000B1 patent drawingFigure 1
  • EP2946000B1 patent drawingFigure 2
  • EP2946000B1 patent drawingFigure 3

AI summary

A process for upgrading residuum hydrocarbons including: feeding pitch, hydrogen, and a partially spent catalyst recovered from a hydrocracking reactor to an ebullated bed pitch hydrocracking reactor; contacting the pitch, hydrogen, and the catalyst in the ebullated bed pitch hydrocracking reactor at reaction conditions of temperature and pressure sufficient to convert at least a portion of the pitch to distillate hydrocarbons; and separating the distillate hydrocarbons from the catalyst. In some embodiments, the process may include selecting the ebullated bed pitch hydrocracking reactor reaction conditions to be at or below the level where sediment formation would otherwise become excessive and prevent continuity of operations.