Polishing Composition Reducing Surface Defects via Dispersibility Control

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Solution Overview

Problem

Conventional polishing compositions, including cellulose derivatives, struggle to achieve a surface with low haze and few surface defects, particularly in the final polishing step of semiconductor substrates like silicon wafers, due to micro aggregation and quality variability of cellulose derivatives.

Innovation Solution

A polishing composition comprising an abrasive, a basic compound, and a surface protective agent with a cellulose derivative and a vinyl alcohol-based dispersant, where the dispersibility parameter is less than 100, effectively reduces surface defects by improving dispersibility and wettability, and includes an oxyalkylene-based additive to enhance surface quality.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional polishing compositions including cellulose derivatives are used, then the polishing process can be performed, but micro aggregation occurs causing surface defects

Engineering Contradiction:
Improvesurface qualityVSAvoidmicro aggregation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent extracts and removes the harmful micro aggregation component from the polishing composition by optimizing the cellulose derivative selection and adding specific dispersants, thereby eliminating the source of surface defects while maintaining the beneficial protective functions

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent introduces dispersants as intermediary substances that mediate between the cellulose derivative and the polishing slurry components, preventing micro aggregation formation and ensuring uniform distribution of particles for defect-free polishing surfaces

Inventive Principle:
Principle #24Intermediary (Mediator)

2Ease of manufacture

If cellulose derivatives with varied quality are used, then the polishing composition can be formulated, but surface defects cannot be accurately prevented

Engineering Contradiction:
Improveformulation flexibilityVSAvoidsurface defect prevention
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent applies parameter changes by specifying precise molecular weight ranges for cellulose derivatives (5×10^4 to 500×10^4) and optimizing dispersant concentrations, thereby transforming the formulation from a flexible but imprecise process to a controlled precision process that prevents surface defects

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite material system combining cellulose derivatives with specific dispersants and polishing particles, where the composite exhibits superior properties that prevent micro aggregation and surface defects while maintaining formulation flexibility

Inventive Principle:
Principle #40Composite materials

3Reliability

If general-purpose water-soluble polymers like HEC are used, then the surface protective function is provided, but surface defects still occur

Engineering Contradiction:
Improvesurface protectionVSAvoidsurface defects
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent applies local quality by selecting cellulose derivatives with specific molecular weight characteristics and combining them with dispersants that locally address the micro aggregation problem at the molecular level, while maintaining the overall surface protective function of the polishing composition

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The composition significantly reduces Light Point Defect Non-cleanable (LPD-N) defects and achieves a higher quality surface with reduced haze, improving the overall polishing outcome.

Implementation Method 1

a vinyl alcohol-based dispersant... the surface protective agent has a dispersibility parameter α of less than 100

Methodology Applied
Scientific EffectDispersion: Dispersion (of waves)

Implementation Method 2

improving wettability... a vinyl alcohol-based dispersant... dispersibility parameter α of less than 100

Methodology Applied
Scientific EffectWetting: Wetting

Data Source

PatentUS11130883B2Polishing composition
Publication Date: 2021.09.28 FUJIMI INCORPORATED

AI summary

Provided is a polishing composition that includes a cellulose derivative and is effective for reducing surface defects after polishing. According to the present application, a polishing composition comprising an abrasive, a basic compound and a surface protective agent is provided. The surface protective agent contains a cellulose derivative and a vinyl alcohol-based dispersant. The surface protective agent has a dispersibility parameter α of less than 100.