Polymeric Decoupling Layer for OLED Encapsulation

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Solution Overview

Problem

Existing encapsulation methods for environmentally sensitive devices, such as OLEDs, face challenges due to plasma damage during the deposition of barrier and decoupling layers, leading to degradation and reduced performance, with conventional decoupling layers failing to provide adequate barrier performance and compatibility with deposition technologies.

Innovation Solution

A method involving the use of polymeric decoupling layers made from blends of 60-90 wt% dimethacrylate, 0-20 wt% monoacrylate, 5-20 wt% triacrylate, and 1-10 wt% photoinitiator, which are designed to minimize plasma damage, mechanical stress, and water permeability, enhancing the overall barrier performance and compatibility with various deposition processes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If plasma-based deposition processes are used to deposit barrier and decoupling layers, then barrier performance is improved, but plasma damage occurs to the environmentally sensitive device

Engineering Contradiction:
Improvebarrier performanceVSAvoidplasma damage
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

A plasma-resistant decoupling layer is introduced as an intermediary between the plasma deposition process and the environmentally sensitive device. This decoupling layer acts as a protective mediator that allows plasma-based barrier layer deposition while preventing direct plasma damage to the device, thereby maintaining barrier performance without compromising device integrity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The decoupling layer is designed with specific local properties (plasma resistance, appropriate thickness, material composition) that differ from both the barrier layer and the device structure. This localized quality enhancement at the interface region protects the device from plasma damage while maintaining overall barrier stack functionality

Inventive Principle:
Principle #3Local quality

2Reliability

If conventional decoupling layers are used, then device encapsulation is achieved, but adequate barrier performance and compatibility with deposition technologies are not provided

Engineering Contradiction:
Improvebarrier performanceVSAvoidcompatibility with deposition technologies
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The decoupling layer is designed to perform multiple functions simultaneously: it serves as a protective barrier during plasma deposition, provides mechanical stress relief, maintains structural integrity, and ensures compatibility with various deposition technologies. This multi-functionality enables the encapsulation system to achieve both adequate barrier performance and broad deposition technology compatibility

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Reliability

If barrier stacks with multiple layers are deposited to improve barrier performance, then water vapor and oxygen permeation resistance is enhanced, but mechanical stress and plasma damage increase

Engineering Contradiction:
Improvewater vapor and oxygen permeation resistanceVSAvoidmechanical stress
Core Design Contradiction:
ReliabilityVSStress or pressure

Solution Approach 1:

The barrier stack is segmented into distinct functional layers: a plasma-resistant decoupling layer and a barrier layer. This segmentation allows each layer to be optimized for its specific function while reducing overall mechanical stress and plasma damage exposure, as the decoupling layer absorbs stress and protects the device during deposition of subsequent barrier layers

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed solution significantly reduces plasma damage and mechanical stress, improves barrier performance, and maintains the electroluminescence and appearance of encapsulated devices, while also addressing issues of water permeability and structural stability, resulting in enhanced longevity and reliability of encapsulated devices.

Implementation Method 1

a blend of polymer precursors comprising 60 to 90 wt% of a dimethacrylate, 0 to 20 wt% of a monoacrylate, 5 to 20 wt% of a triacrylate, and 1 to 10 wt% of a photoinitiator

Methodology Applied
Scientific EffectPhotopolymerization: Photopolymerisation

Implementation Method 2

The barrier stacks typically include at least one barrier layer and at least one decoupling layer... preventing environmental oxygen and water vapor from degrading the display device

Methodology Applied
Scientific EffectPermeation barrier: Permeation

Data Source

PatentEP1925043B1Encapsulated devices and method of making
Publication Date: 2011.05.11 SAMSUNG MOBILE DISPLAY CO LTD
  • EP1925043B1 patent drawingFigure 1~2B
  • EP1925043B1 patent drawingFigure 3A~3D
  • EP1925043B1 patent drawingFigure 4A~4C

AI summary

A method of encapsulating an environmentally sensitive device. The method includes providing a substrate; placing at least one environmentally sensitive device adjacent to the substrate; and depositing at least one barrier stack adjacent to the environmentally sensitive device, the at least one barrier stack comprising at least one barrier layer and at least one polymeric decoupling layer, wherein the at least one polymeric decoupling layer is made from at least one polymer precursor, and wherein the polymeric decoupling layer has at least one of: a reduced number of polar regions; a high packing density; a reduced number of regions that have bond energies weaker than a C-C covalent bond; a reduced number of ester moieties; increased Mw of the at least one polymer precursor; increased chain length of the at least one polymer precursor; or reduced conversion of C=C bonds. An encapsulated environmentally sensitive device is also described.