Probiotic Beadlets via Spray Drying and Powder Coating

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Solution Overview

Problem

Current methods for formulating probiotics, such as freeze-drying and spray-drying, are time-consuming, expensive, and can negatively affect the viability of bacteria, while existing beadlet formulations for fat-soluble substances have low active content and require emulsification steps, making them unsuitable for high-probiotic formulations with good storage stability and handling properties.

Innovation Solution

The production of beadlets comprising probiotic compounds and starch/starch derivatives using a powder coating process, where an aqueous solution of probiotics and starch is spray-dried to create beadlets with a high probiotic content and improved storage stability, coated with a powder catch medium like starch or silicate compounds.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If freeze-drying is used for probiotic formulation, then storage stability is improved, but production time and cost increase significantly

Engineering Contradiction:
Improvestorage stabilityVSAvoidproduction time
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The patent uses spray-drying process which involves phase transition from liquid to solid particles through rapid evaporation of solvent, creating stable probiotic formulations without the extended time requirements of freeze-drying. The aqueous probiotic suspension is atomized into droplets that rapidly dry in the spray-dryer chamber, achieving storage stability through controlled phase change rather than slow freeze-drying.

Inventive Principle:
Principle #36Phase transitions

2Productivity

If spray-drying is used for probiotic formulation, then production cost is reduced, but bacterial viability decreases due to high temperatures

Engineering Contradiction:
Improveproduction efficiencyVSAvoidthermal damage to probiotics
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The patent modifies the spray-drying parameters to use lower inlet temperatures and optimized atomization conditions, changing the thermal parameters from conventional high-temperature spray-drying to a gentler process that preserves probiotic viability while maintaining production efficiency. The process parameters are specifically adjusted to keep product temperature below harmful thresholds.

Inventive Principle:
Principle #35Parameter changes

3Ease of operation

If existing beadlet formulations for fat-soluble substances are used, then handling properties are improved, but probiotic content is limited to low concentrations

Engineering Contradiction:
Improvehandling propertiesVSAvoidprobiotic content
Core Design Contradiction:
Ease of operationVSQuantity of substance

Solution Approach 1:

The patent creates homogeneous aqueous probiotic-starch suspensions that are uniformly distributed throughout the beadlet matrix, allowing high probiotic loading (30-80 wt%) without aggregation or phase separation. The homogeneity of the aqueous phase enables high concentrations of water-soluble probiotics to be incorporated while maintaining the beadlet form's superior handling properties.

Inventive Principle:
Principle #33Homogeneity

4Adaptability or versatility

If emulsification is used in beadlet production, then fat-soluble substances can be incorporated, but process complexity increases

Engineering Contradiction:
Improvesubstance incorporation capabilityVSAvoidprocess steps
Core Design Contradiction:
Adaptability or versatilityVSDevice complexity

Solution Approach 1:

The patent extracts the emulsification step from the beadlet production process, eliminating the need for emulsifiers and emulsification equipment. By focusing on water-soluble probiotics and using a straightforward spray-drying approach, the process removes the complex emulsion formation and stabilization steps while still achieving effective probiotic delivery.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This process allows for the creation of beadlets with high probiotic content (30-80 wt-%) and excellent storage stability, handling properties, and simplified production, overcoming the limitations of existing methods by maintaining bacterial viability and avoiding the need for emulsification.

Implementation Method 1

converting the solution into a dry powder by spray drying

Methodology Applied
Scientific EffectEvaporation: Evaporation

Implementation Method 2

These beadlets are coated with a layer of the powder catch medium

Methodology Applied
Scientific EffectAdhesion: Adhesive

Data Source

PatentEP2320749B1Production of beadlets comprising probiotic compounds
Publication Date: 2015.09.16 DSM IP ASSETS BV

AI summary

The present invention relates a process of production of beadlets comprising probiotic compounds in a matrix comprising at least one starch and/or starch derivative, to such beadlets and to the use of such specific beadlets in food (for humans and animals) as well as in premixes.