Sb-Modified Sn-Ag-Cu Solder Paste for No-Clean PCBs

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Solution Overview

Problem

Lead-free solder pastes, particularly Sn-Ag-Cu based, exhibit high reactivity with flux components, leading to issues like increased viscosity and short pot life when using maleated rosin as the main flux resin, which results in tacky and dark flux residues, complicating the soldering process and inspection.

Innovation Solution

Adding 1-8 mass% of Sb to the Sn-Ag-Cu based solder powder suppresses the reaction with maleated rosin, maintaining a stable solder paste viscosity and extending its pot life, while ensuring a transparent and non-tacky flux residue.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-affected harmful factors

If lead-free solder powder (Sn-Ag-Cu based) is used to eliminate Pb pollution, then environmental safety is improved, but reactivity with flux components increases causing viscosity increase and short pot life

Engineering Contradiction:
ImprovePb pollutionVSAvoidsolder paste viscosity stability
Core Design Contradiction:
Object-affected harmful factorsVSStability of the object's composition

Solution Approach 1:

Sb is introduced as an intermediary element that forms a protective interface layer between the Sn-Ag-Cu solder powder and the flux components (particularly maleated rosin). This Sb-containing layer acts as a mediator that reduces the direct reactive interaction between the solder powder and flux, thereby suppressing viscosity increase and extending pot life while maintaining the lead-free environmental benefit

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The solder paste is formulated as a composite system containing Sn-Ag-Cu solder powder with added Sb element. This composite composition leverages the low reactivity of Sb with flux components to create a more stable paste system. The composite nature of the solder powder (multiple elements working together) provides both the lead-free advantage and the improved stability through synergistic interactions among Sn, Ag, Cu, and Sb

Inventive Principle:
Principle #40Composite materials

2Ease of manufacture

If maleated rosin is used as the main flux resin to achieve transparent and non-tacky residue, then residue quality is improved, but reactivity with solder powder increases causing short pot life

Engineering Contradiction:
Improveresidue transparency and non-tackinessVSAvoidpot life
Core Design Contradiction:
Ease of manufactureVSDuration of action of stationary object

Solution Approach 1:

Sb serves as an intermediary substance that intervenes in the reaction between maleated rosin and Sn-Ag-Cu solder powder. The Sb forms a protective layer on the solder powder surface that prevents direct contact and excessive reaction with the maleated rosin, thereby extending pot life while allowing the maleated rosin to perform its function of producing transparent, non-tacky residue

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The chemical composition parameters of the solder powder are modified by adding Sb element. This parameter change (compositional modification) alters the reactivity characteristics of the solder powder with maleated rosin, reducing the reaction rate and extending pot life while preserving the desirable residue properties that maleated rosin provides

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The addition of Sb to the Sn-Ag-Cu solder powder stabilizes the solder paste, preventing viscosity increase and maintaining a long pot life, along with achieving a transparent and non-tacky flux residue, enhancing the reliability and inspection quality of the soldering process.

Implementation Method 1

Adding 1-8 mass% of Sb to the Sn-Ag-Cu based solder powder suppresses the reaction with maleated rosin

Methodology Applied
Scientific EffectChemical reaction suppression: Chemical Bonding

Implementation Method 2

maintaining a stable solder paste viscosity and extending its pot life

Methodology Applied
Scientific EffectViscosity stabilization:

Implementation Method 3

ensuring a transparent and non-tacky flux residue

Methodology Applied
Scientific EffectTranslucency control:

Data Source

PatentEP2578350B1No-clean lead-free solder paste
Publication Date: 2018.10.03 SENJU METAL IND CO LTD

AI summary

As electronic equipment has become smaller in size, printed circuit boards which cannot be subjected to cleaning have been developed, and a no-clean lead-free solder paste is becoming necessary. In order for a solder paste not to require cleaning, it is necessary that the color of the residue be transparent and that the residue be non-tacky. A maleated rosin, which is a rosin suited for no-clean paste, has a high acid value so it is not suitable for a flux for lead-free solder. As a means of suppressing a reaction between a flux containing a maleated rosin and a Sn-Ag-Cu based solder alloy powder, a Sn-Ag-Cu-Sb based solder alloy powder is used which adds 1 - 8 mass % of Sb to a Sn-Ag-Cu based solder alloy. As a result, it is possible to provide a solder paste which has the excellent effect that the solder paste does not easily undergo changes over time and