High Purity SiC Powder from Waste via Chemical Etching

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Solution Overview

Problem

The existing processes for producing silicon carbide (SiC) powders are costly and environmentally unfriendly due to high-temperature heat treatment requirements and generate waste that ends up in landfills, leading to environmental issues and high disposal costs.

Innovation Solution

A process involving the pulverization, classification, removal of iron components, and cleaning of silicon carbide waste to produce high-purity SiC powders, which includes cutting and removing graphite before pulverization to enhance efficiency and purity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If high-temperature heat treatment (1,800°C to 2,100°C) under vacuum or inert gas conditions is used to prepare silicon carbide, then the purity and quality of SiC powder is improved, but the manufacturing cost increases significantly

Engineering Contradiction:
Improvepurity of SiC powderVSAvoidmanufacturing cost
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The patent changes the temperature parameter from high-temperature (1,800-2,100°C) to low-temperature (room temperature or slightly elevated) processing. Instead of heat treatment, the invention uses chemical etching with selective reagents to remove impurities, thereby achieving high purity SiC powder without the energy-intensive high-temperature process

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the thermal/chemical high-temperature synthesis mechanism with a chemical etching mechanism. By using selective chemical reagents that dissolve impurities while leaving SiC intact, the process achieves purification through chemical selectivity rather than thermal energy input

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If high-temperature heat treatment under vacuum or inert gas conditions is used, then the quality of SiC powder is improved, but the processing time and energy consumption increase

Engineering Contradiction:
Improvequality of SiC powderVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The patent fundamentally changes the processing temperature parameter from high-temperature to low-temperature operation. The chemical etching process occurs at or near room temperature, dramatically reducing processing time and energy consumption while maintaining product quality through selective impurity removal

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent skips the lengthy high-temperature heat treatment step entirely by using direct chemical etching. This allows the process to rapidly remove impurities in a short time frame without requiring prolonged exposure to extreme temperatures

Inventive Principle:
Principle #21Skipping (Rushing through)

3Ease of manufacture

If silicon carbide waste is landfilled, then disposal is simple, but environmental problems occur and disposal costs increase

Engineering Contradiction:
Improvedisposal simplicityVSAvoidenvironmental impact
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The patent converts the harmful waste material into a beneficial resource by recovering valuable SiC powder from waste. The chemical etching process selectively removes impurities from waste SiC, transforming discarded material into high-purity reusable powder, thereby eliminating environmental harm and disposal costs

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The patent implements a recovery process that extracts valuable SiC from waste materials. Instead of discarding SiC waste to landfills, the process recovers and purifies the SiC powder through chemical etching, enabling reuse in manufacturing applications

Inventive Principle:
Principle #34Discarding and recovering

4Quantity of substance

If conventional SiC production processes are used, then SiC powder can be produced, but the yield and productivity are low

Engineering Contradiction:
ImproveSiC powder productionVSAvoidproduction efficiency
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent enables the waste SiC material to self-purify through selective chemical etching. The process exploits the different chemical reactivities between SiC and impurities, allowing the SiC to remain intact while impurities are automatically removed by the etching reagent, achieving high yield without complex processing

Inventive Principle:
Principle #25Self-service

Data Source

PatentUS20230322562A1Preparation method of high purity sic powder
Publication Date: 2023.10.12 KC IND CO LTD

AI summary

The process for preparing high purity SiC powders according to embodiments not only solves the environmental problems by using waste SiC, but also reduces the manufacturing cost with high yield, high productivity, and high uniformity.