Silicon CMP Slurry pH Control to Reduce Surface Defects

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Solution Overview

Problem

The existing Chemical Mechanical Polishing (CMP) techniques for semiconductor substrates are inadequate in reducing defects on the surface of silicon materials, as described in JP 2002-114967 A.

Innovation Solution

A polishing method using a composition containing abrasive grains, a tri- or more polyvalent hydroxy compound, and a dispersing medium with a pH of less than 6.0, which reduces adhesion of organic residues and thereby minimizes surface defects during the polishing process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional CMP techniques are used, then polishing can be performed on semiconductor substrates, but surface defects such as scratches and residue adhesion are not sufficiently reduced

Engineering Contradiction:
Improvesurface qualityVSAvoidsurface defects
Core Design Contradiction:
Manufacturing precisionVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical parameters of the polishing composition by specifying a pH range of 2.0 to 6.0 and incorporating tri- or more polyvalent hydroxy compounds with specific molecular weights (90 or more). These parameter changes transform the chemical environment to reduce organic residue adhesion and minimize surface defects during polishing of silicon materials

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite polishing composition that integrates multiple functional components: abrasive grains for mechanical removal, tri- or more polyvalent hydroxy compounds for chemical etching and surface modification, and dispersing media for stable suspension. This composite formulation synergistically reduces surface defects while maintaining polishing effectiveness

Inventive Principle:
Principle #40Composite materials

2Productivity

If polishing composition is used to remove material, then planarization is achieved, but organic residues adhere to the surface causing defects

Engineering Contradiction:
Improvepolishing rateVSAvoidorganic residue adhesion
Core Design Contradiction:
ProductivityVSObject-generated harmful factors

Solution Approach 1:

The invention converts the harmful adhesion of organic residues into a beneficial effect by using tri- or more polyvalent hydroxy compounds that chemically interact with and modify the residue molecules. The hydroxy groups form hydrogen bonds or chemical complexes with organic residues, preventing their adhesion to the silicon surface and transforming them into removable byproducts

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

By controlling the pH within 2.0 to 6.0 and selecting hydroxy compounds with molecular weights of 90 or more, the invention optimizes the chemical environment to prevent organic residue adhesion while maintaining efficient material removal, thus achieving both high productivity and clean surfaces

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed method effectively reduces surface defects on silicon materials by utilizing the hydrophilizing properties of the polyvalent hydroxy compound, improving the polishing efficiency and reducing scratches and residue adhesion.

Implementation Method 1

it was found that the above effect was obtained by a polishing method, including polishing a polishing object containing a silicon material by using a polishing composition containing abrasive grains, a tri- or more polyvalent hydroxy compound and a dispersing medium and having pH of less than 6.0

Methodology Applied
Scientific EffectHydrophilization: Hydrophile

Data Source

PatentUS11749531B2Polishing method, and polishing composition and method for producing the same
Publication Date: 2023.09.05 FUJIMI INCORPORATED

AI summary

A polishing method according to the present invention, includes polishing a polishing object containing a silicon material by using a polishing composition containing abrasive grains, a tri- or more polyvalent hydroxy compound and a dispersing medium and having pH of less than 6.0.