Simultaneous Distillation and Alloying Device

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Solution Overview

Problem

Current methods for producing high-purity metals and alloys, such as magnesium-based alloys, face challenges including low distillation speeds, material incompatibility issues, and energy-intensive processes, particularly when distilling multiple metals simultaneously, which complicates the production of alloys like Magnesium-Zinc-Calcium due to corrosion concerns and the need for high-purity alloying elements.

Innovation Solution

A device comprising a chamber with a trough, a heating element, a collecting vessel, and a condensation device, which allows for independent optimization of heating and condensation processes, enabling continuous distillation and reducing the dependency on filling state, and can operate under vacuum or inert gas conditions to enhance distillation speed and purity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If vacuum distillation is used to purify magnesium, then high-purity metal is obtained, but distillation speed decreases as liquid level increases

Engineering Contradiction:
ImprovepurityVSAvoiddistillation speed
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The condensation function is segmented from the crucible and assigned to a separate condensation device with dedicated condensation surfaces. This segmentation allows the crucible to maintain constant heating power while the condensation device independently manages condensation efficiency, preventing the coupling effect that causes speed degradation as liquid level rises.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

A separate condensation device is introduced as an intermediary component between the crucible and the collection system. This mediator provides dedicated condensation surfaces that are thermally optimized for condensation efficiency, decoupling the condensation process from the crucible's liquid level and maintaining consistent distillation speed throughout the process.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Use of energy by stationary object

If graphite crucible is used for magnesium distillation, then good thermal conductivity is achieved, but it reacts with calcium to form calcium carbide

Engineering Contradiction:
Improvethermal conductivityVSAvoidchemical reaction
Core Design Contradiction:
Use of energy by stationary objectVSObject-generated harmful factors

Solution Approach 1:

The condensation function is extracted from the graphite crucible and transferred to a separate condensation device made of calcium-compatible materials. This extraction eliminates the harmful chemical reaction between graphite and calcium while preserving the thermal conductivity requirements for the heating process in the crucible.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

Different parts of the system are assigned different material qualities: the crucible uses graphite for optimal thermal conductivity during heating, while the condensation device uses calcium-compatible materials (such as stainless steel or ceramic) to prevent chemical reactions. This local differentiation of material properties resolves the contradiction between thermal performance and chemical compatibility.

Inventive Principle:
Principle #3Local quality

3Manufacturing precision

If separate distillation and alloying processes are used, then high-purity alloying elements are obtained, but process time and energy consumption increase

Engineering Contradiction:
ImprovepurityVSAvoidprocess time
Core Design Contradiction:
Manufacturing precisionVSLoss of time

Solution Approach 1:

The distillation and alloying processes are merged into a single integrated operation. Multiple starting materials are simultaneously introduced into the crucible, where they undergo combined distillation and alloying in one continuous process. This eliminates the need for separate handling steps and reduces both process time and energy consumption while maintaining high purity through the constant-power heating and efficient condensation.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The system enables continuous operation where multiple materials are processed simultaneously in a single batch. The constant-power heating maintains steady-state distillation conditions throughout the process, and the condensed materials are collected together as a homogeneous alloy, eliminating interruptions and repeated heating cycles that would increase time and energy consumption.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The device facilitates high-speed and efficient production of target materials with reduced energy consumption and simplified processes, enabling the production of high-purity metals and alloys like Magnesium-Zinc-Calcium with improved mechanical properties and biocompatibility.

Implementation Method 1

The first heating element is configured to heat the chamber such that starting material being received in the trough is vaporized

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 2

The condensation device is configured to condensate the vaporized starting material, whereby the condensate is formed

Methodology Applied
Scientific EffectCondensation: Condensation

Data Source

PatentUS20230083353A1Simultaneous distillation and alloying
Publication Date: 2023.03.16 ETH ZURICH
  • US20230083353A1 patent drawing
  • US20230083353A1 patent drawing
  • US20230083353A1 patent drawing

AI summary

A device for producing a target material from starting material comprises a chamber, at least one trough, at least a first heating element being configured to heat the chamber such that starting material is vaporized, and at least one collecting vessel being configured to receive a condensate that will constitute the target material. The device optionally comprises at least a first source of negative pressure or at least a first supply device being in connection with the chamber being configured to evacuate the chamber or to supply an inert gas to the chamber. The device further comprises at least one condensation device, wherein said condensation device is configured to condensate the vaporized starting material, whereby the condensate is formed, and/or at least a first gate device being in connection with the chamber such, that the starting material is introducible into the chamber via said first gate device.