Sodium Ibuprofen Tablet Hardness and Dissolution via Binder Optimization

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Solution Overview

Problem

Commercially available sodium ibuprofen tablets have high sodium content, poor stability, and friability issues, leading to uncertainty in dosage and increased waste during handling, while also having slow dissolution profiles.

Innovation Solution

The development of sodium ibuprofen cores with low sodium content, using microcrystalline cellulose and mannitol as binders, and a dihydrate form, which are compressed into tablets with a coating to achieve high hardness, low friability, and rapid dissolution, along with a manufacturing process that includes roller compaction to ensure stability and bioavailability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If tablets are compressed under low compression force, then dissolution rate is improved, but tablet hardness and strength deteriorate

Engineering Contradiction:
Improvedissolution rateVSAvoidtablet hardness
Core Design Contradiction:
SpeedVSStrength

Solution Approach 1:

The patent changes the physical-chemical parameters of the active ingredient by using sodium ibuprofen dihydrate instead of anhydrous form, and optimizes binder composition ratios to achieve both low compression force (improved dissolution) and adequate tablet hardness. The dihydrate form allows compression at lower forces while maintaining structural integrity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses a composite binder system containing both microcrystalline cellulose and mannitol in specific ratios, creating a synergistic effect where the combination provides both adequate binding strength for tablet formation and porosity for rapid dissolution, resolving the contradiction between hardness and dissolution rate.

Inventive Principle:
Principle #40Composite materials

2Strength

If tablets are compressed under high compression force, then tablet hardness is improved, but dissolution rate deteriorates and friability increases

Engineering Contradiction:
Improvetablet hardnessVSAvoiddissolution rate
Core Design Contradiction:
StrengthVSSpeed

Solution Approach 1:

By changing the compression force parameter to low levels and using sodium ibuprofen dihydrate with optimized binder composition, the patent achieves tablet hardness sufficient for handling while maintaining a porous structure that enables rapid dissolution, avoiding the compaction that would slow dissolution.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If sodium ibuprofen tablets are formulated with conventional binders, then manufacturing is simplified, but sodium content becomes excessive

Engineering Contradiction:
Improvemanufacturing simplicityVSAvoidsodium content
Core Design Contradiction:
Ease of manufactureVSQuantity of substance

Solution Approach 1:

The patent changes the chemical form of the active ingredient to sodium ibuprofen dihydrate and optimizes the binder system to require lower quantities, thereby reducing total sodium content below 140 mg/day while maintaining manufacturability through standard compression processes.

Inventive Principle:
Principle #35Parameter changes

4Ease of manufacture

If tablets have high friability, then manufacturing cost is reduced, but dosage accuracy deteriorates and waste increases

Engineering Contradiction:
Improvemanufacturing costVSAvoiddosage accuracy
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

The patent optimizes compression parameters and binder composition to achieve the minimum acceptable friability level that prevents crumbling and breakage during handling, thereby ensuring dosage accuracy and reducing waste while maintaining cost-effective manufacturing.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentEP2445486B1Sodium ibuprofen tablets and methods of manufacturing pharmaceutical compositions including sodium ibuprofen
Publication Date: 2017.11.08 WYETH LLC
  • EP2445486B1 patent drawingFigure 1
  • EP2445486B1 patent drawingFigure 2
  • EP2445486B1 patent drawingFigure 3

AI summary

Sodium ibuprofen compositions and methods of manufacturing tablets and caplets comprising sodium ibuprofen are described. The formulation is advantageous because it allows for the formation of tablets having low sodium content and further provides tablets exhibiting improved physical stability, high tablet hardness and high strength, coupled with excellent dissolution and bioavailability characteristics. The formulations and processes are further advantageous because they can be produced in large quantities without an unacceptable number of defective tablets.