Scanning Probe Microscope Surface Charge Compensation

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Solution Overview

Problem

Scanning electron microscopes and scanning probe microscopes face challenges in accurately examining specimens with electrical charge distributions, leading to image distortion, probe damage, and measurement errors due to surface charging, which is particularly problematic in nanotechnology and microstructured component production.

Innovation Solution

A method involving the determination and modification of electrical potential distributions on the specimen surface using scanning probe microscopes, where the potential of the probe is adjusted to match the specimen's surface, and the use of charged particle beams or plasma discharges to compensate for surface charges, allowing for precise scanning and image correction.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If a charged particle beam is used to scan a specimen surface with electrical charge, then imaging capability is achieved, but image distortion and measurement errors occur due to surface charging effects

Engineering Contradiction:
Improveimaging accuracyVSAvoidsurface charging
Core Design Contradiction:
Measurement precisionVSObject-affected harmful factors

Solution Approach 1:

The electrical potential distribution is determined before scanning the specimen surface with the charged particle beam. This preliminary measurement allows the system to adjust scan parameters or apply compensating fields in advance, preventing image distortion caused by surface charging effects during the actual imaging process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system uses the determined electrical potential distribution as feedback to adjust scanning parameters, beam energy, or apply compensating electrical fields during the imaging process. This closed-loop control eliminates image distortion by continuously counteracting surface charging effects based on real-time potential measurements.

Inventive Principle:
Principle #23Feedback

2Measurement precision

If the probe of a scanning probe microscope is brought close to a charged specimen surface, then high-resolution scanning is achieved, but probe damage or specimen destruction occurs due to electrical flashovers

Engineering Contradiction:
Improvescanning resolutionVSAvoidprobe integrity
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The electrical potential distribution of the specimen surface is determined before bringing the probe close for high-resolution scanning. This advance knowledge allows the system to adjust the probe's electrical potential or apply compensating fields, preventing electrical flashovers that would damage the probe or specimen during close-probe scanning.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The system adjusts the electrical potential of the probe or applies compensating fields to match the specimen surface potential, creating an equipotential condition between probe and specimen. This eliminates potential differences that would cause electrical flashovers, enabling safe high-resolution scanning without probe damage or specimen destruction.

Inventive Principle:
Principle #12Equipotentiality

3Reliability

If the electrical potential of the probe is adjusted to match the specimen surface, then electrical flashovers are prevented, but additional measurement and adjustment steps are required

Engineering Contradiction:
Improveelectrical safetyVSAvoidmeasurement procedure
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The system integrates multiple functions into a single coordinated process: determining electrical potential distribution, adjusting probe potential, and performing the actual scanning/examining operation. This multi-functionality consolidates what would otherwise be separate complex steps into an integrated workflow, reducing overall procedural complexity while maintaining electrical safety.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach prevents damage to probes and specimens, reduces measurement errors, and enables accurate scanning and imaging of charged specimens by neutralizing surface charges, thereby improving the precision and reliability of nanoscale measurements.

Implementation Method 1

Scanning probe microscopes (SPM) are likewise powerful analytical tools in nanotechnology. SPMs scan a specimen or its surface with a probe tip and thus produce a realistic topography of the specimen surface.

Methodology Applied
Scientific EffectScanning probe microscopy: Scanning Probe Microscopy

Implementation Method 2

A powerful tool for locally analyzing a specimen is a scanning electron microscope (SEM), the electron beam of which can be focused very finely, so that the beam diameter at the focal point is in the single-digit nanometer range. This measuring instrument scans the electron beam over the surface of a specimen. Among the effects of the interaction of the electrons with the specimen are that secondary electrons (SE) and back-scattered electrons (BSE) are generated.

Methodology Applied
Scientific EffectElectron beam interaction: Electron Beam

Implementation Method 3

modifying the electrical potential distribution in the at least one first partial region of the specimen surface and/or modifying an electrical potential of the probe of the scanning probe microscope before scanning at least one second partial region of the specimen surface

Methodology Applied
Scientific EffectPlasma discharge: Plasma

Implementation Method 4

If the specimen is a wafer to be processed, coating processes and/or etching processes may also result in an electrical charging of the specimen.

Methodology Applied
Scientific EffectElectrostatic discharge: Electrostatic Discharge

Data Source

PatentUS11170970B2Methods and devices for examining an electrically charged specimen surface
Publication Date: 2021.11.09 CARL ZEISS SMT GMBH
  • US11170970B2 patent drawing
  • US11170970B2 patent drawing
  • US11170970B2 patent drawing

AI summary

A method for examining a specimen surface with a probe of a scanning probe microscope, the specimen surface having an electrical potential distribution. The method includes (a) determining the electrical potential distribution of at least one first partial region of the specimen surface; and (b) modifying the electrical potential distribution in the at least one first partial region of the specimen surface and/or modifying an electrical potential of the probe of the scanning probe microscope before scanning at least one second partial region of the specimen surface.