Sugar Crystallization via Pressure Homogenization

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Existing methods for producing sugar crystal-containing liquids face challenges in maintaining adequate supersaturation and achieving consistent crystal size and number, often requiring seed crystals and high stirring speeds that can lead to temperature increases and crystal dissolution.

Innovation Solution

A method involving a pressure homogenizer that applies a shearing force by pressurizing the liquid to pass through a narrow space, generating crystal nuclei without the need for seed crystals, while controlling temperature and enhancing crystallization efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If high stirring speed is employed to promote crystallization, then crystallization efficiency is improved, but liquid temperature rises causing crystal dissolution

Engineering Contradiction:
Improvecrystallization efficiencyVSAvoidliquid temperature
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The patent replaces the conventional mechanical stirring system with a high-pressure homogenization system. The homogenizer applies intense shear stress and cavitation effects to induce crystallization without the continuous mechanical agitation that causes temperature rise. This substitution resolves the contradiction by achieving crystallization efficiency through pressure-induced nucleation rather than mechanical stirring.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent utilizes phase transition phenomena during high-pressure homogenization, where the sudden pressure drop and cavitation effects cause localized temperature changes that promote nucleation. The phase transition of sugar from dissolved to crystalline state is induced by the physical conditions in the homogenizer rather than by continuous stirring, thereby avoiding excessive temperature rise.

Inventive Principle:
Principle #36Phase transitions

2Productivity

If seed crystals are added to promote crystallization, then crystallization is enhanced, but the size, shape and number of crystals become difficult to control

Engineering Contradiction:
Improvecrystallization enhancementVSAvoidcrystal size and number control
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent employs self-nucleation where the sugar solution itself generates crystal nuclei through the homogenization process. The intense shear stress and cavitation in the homogenizer create numerous nucleation sites directly in the solution, eliminating the need for external seed crystals. This self-service approach provides better control over crystal characteristics as the nucleation conditions can be precisely controlled through pressure and flow rate parameters.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent controls crystal formation by changing physical parameters (pressure, temperature, flow rate) during homogenization rather than by adding seed crystals. By adjusting the homogenization pressure and other operational parameters, the number and size of crystal nuclei can be precisely controlled, achieving manufacturing precision without the variability introduced by seed crystal addition.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If stirring is applied to crystallize sugar, then crystal formation is promoted, but reproducibility of graining conditions becomes difficult to achieve

Engineering Contradiction:
Improvecrystal formationVSAvoidreproducibility of graining
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent replaces the stirring mechanism with high-pressure homogenization, which provides more consistent and controllable physical conditions for crystallization. The homogenizer delivers repeatable shear stress and cavitation effects through controlled pressure cycles, leading to better reproducibility of graining conditions compared to the variability inherent in manual or mechanical stirring operations.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method promotes consistent and efficient sugar crystallization, maintaining supersaturation, reducing temperature rise, and allowing for regulation of crystal size and number, applicable to various sugars and solutions, with improved reproducibility and reduced risk of crystal dissolution.

Implementation Method 1

applying a shearing force to a liquid supersaturated with sugar

Methodology Applied
Scientific EffectShearing force: Shear Stress

Implementation Method 2

pressurizing the liquid to pass through a narrow space

Methodology Applied
Scientific EffectPressure: Pressure Increase

Implementation Method 3

crystallize sugar

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Implementation Method 4

liquid supersaturated with sugar

Methodology Applied
Scientific EffectSupersaturation: Supersaturation

Data Source

PatentEP3015557B1Method for producing a sugar-crystal-containing fluid
Publication Date: 2020.01.08 MITSUI SUGAR CO LTD
  • EP3015557B1 patent drawingFigure 1
  • EP3015557B1 patent drawingFigure 2
  • EP3015557B1 patent drawingFigure 3(A)~3(B)

AI summary

PURPOSE: An object of the present invention is to provide a method for producing a sugar crystal-containing liquid with good reproducibility, wherein crystallization is enhanced, it is unnecessary to add seed crystals which may affect the number of grains and a size of the crystals, and graining conditions are stable. CONSTITUTION: The present invention is a method for producing a sugar crystal-containing liquid, wherein the method comprises steps of preparing a liquid supersaturated with sugar; and applying a shearing force to the liquid, characterized in that the step of applying the shearing force comprises exerting a pressure higher than atmospheric pressure on the liquid to make the liquid pass through a narrow space.