Valve Configuration for TEOS Deposition Uniformity

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Solution Overview

Problem

Conventional substrate processing systems face challenges in achieving uniform deposition rates and reducing defects, particularly due to the mixing of helium and tetraethyl orthosilicate (TEOS) in delivery lines, which leads to micro-bubble formation and unstable film deposition.

Innovation Solution

The method involves a liquid precursor delivery system with a controller-operated valve configuration that minimizes the mixing of TEOS and helium in supply conduits, using a purge gas to prevent micro-bubble formation and reducing the need for extensive priming, thereby stabilizing film deposition rates and reducing defects.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Device complexity

If liquid precursor (TEOS) and purge gas (helium) are supplied through mixed delivery lines, then the system can operate with simpler valve configuration, but micro-bubbles form and deposition uniformity deteriorates

Engineering Contradiction:
Improvevalve configuration complexityVSAvoiddeposition rate uniformity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The delivery system is segmented into separate pathways: one for liquid precursor (TEOS) and another for purge gas (helium). This segmentation prevents mixing of the two substances in the delivery lines, eliminating micro-bubble formation while maintaining controlled valve operations for precise deposition uniformity.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The harmful mixing effect is extracted by removing the common delivery line configuration. Instead of mixing TEOS and helium in a shared conduit, the system extracts them into separate supply paths, allowing independent control and preventing the formation of unstable gas-liquid mixtures that cause deposition defects.

Inventive Principle:
Principle #2Taking out (Extraction)

2Manufacturing precision

If extensive priming is performed to remove micro-bubbles, then deposition uniformity can be improved, but processing time and productivity decrease

Engineering Contradiction:
Improvedeposition rate uniformityVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The system performs preliminary action by maintaining separate delivery lines for liquid precursor and purge gas from the start, preventing micro-bubble formation before it occurs. This eliminates the need for time-consuming post-preparation priming steps, as the system is configured to avoid the problem rather than correct it later.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The harmful priming step is skipped entirely by redesigning the delivery system architecture. Instead of performing extensive priming to remove micro-bubbles, the system rushes through the setup phase with a pre-configured separate delivery system that prevents micro-bubble formation, directly transitioning to productive deposition operation.

Inventive Principle:
Principle #21Skipping (Rushing through)

3Measurement precision

If liquid precursor metering is increased for precision, then deposition control improves, but the system becomes more sensitive to micro-bubble contamination

Engineering Contradiction:
Improveliquid precursor metering precisionVSAvoiddeposition stability
Core Design Contradiction:
Measurement precisionVSReliability

Solution Approach 1:

The contamination source is extracted by separating the liquid precursor delivery path from the purge gas path. This extraction eliminates micro-bubble contamination in the TEOS supply, allowing precise metering of the liquid precursor without sensitivity to gas mixing, thereby maintaining both precision and reliability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The system creates an inert environment for liquid precursor delivery by using separate, dedicated tubing and valve configurations that prevent contamination. This inert delivery environment protects the precisely metered TEOS from micro-bubble formation, ensuring stable and reliable deposition control.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces defects and improves deposition rate uniformity by eliminating micro-bubble-induced instability, achieving a substantial reduction in thickness range and defect performance.

Implementation Method 1

a liquid precursor may be vaporized into a carrier gas

Methodology Applied
Scientific EffectVaporization: Evaporation

Implementation Method 2

perform plasma-enhanced chemical vapor deposition (PECVD)

Methodology Applied
Scientific EffectPlasma-enhanced chemical vapor deposition: Plasma Enhanced Chemical Vapour Deposition

Data Source

PatentUS9617637B2Systems and methods for improving deposition rate uniformity and reducing defects in substrate processing systems
Publication Date: 2017.04.11 LAM RES CORP
  • US9617637B2 patent drawing
  • US9617637B2 patent drawing
  • US9617637B2 patent drawing

AI summary

Systems and methods for delivering liquid precursor in a substrate processing system include supplying liquid precursor using a first valve in fluid communication with a liquid precursor source; supplying purge gas using a second valve in fluid communication with a purge gas source; arranging a third valve having a first input port in fluid communication with an output port of the first valve and a second input port in fluid communication with an output port of the second valve; arranging an input port of a first divert injector valve in fluid communication with an output port of the third valve; and operating the first valve, the second valve, the third valve and the first divert injector valve in first, second, third and fourth modes.