Variable Angle Refractive Index Measurement for Thin Films

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Solution Overview

Problem

Current spectroscopic ellipsometry systems face difficulties in measuring the refractive index of thin films with thickness less than 10 nm and those with small light absorption coefficients, requiring oblique incident angles and struggling with materials of multiple phases or amorphous materials.

Innovation Solution

The system employs a setup with a first and second distributed Bragg reflector, a light source directing incident light at a flexible angle between 0° to 85°, and a processor to calculate the refractive index of thin films with thickness ranging from 1 nm to 50 μm and light absorption coefficients from 10 cm−1 to 105 cm−1, using wavelengths from 50 nm to 50 μm.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If spectroscopic ellipsometry systems use oblique incident angles (70-80°) to measure refractive index, then measurement capability for thin films is improved, but measurement flexibility and ease of operation deteriorate due to difficulty in optimizing incident angle for materials with multiple phases or amorphous materials

Engineering Contradiction:
Improverefractive index measurement capabilityVSAvoidincident angle optimization flexibility
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The patent changes the incident angle parameter from fixed oblique angles (70-80°) to a variable range (0°-85°), allowing optimization for different material types. This parameter change enables the system to adapt to various materials including amorphous materials and materials with multiple phases, resolving the contradiction between measurement precision and operational flexibility.

Inventive Principle:
Principle #35Parameter changes

2Measurement precision

If spectroscopic ellipsometry systems use fixed oblique incident angles, then measurement for specific material types is optimized, but adaptability to measure thin films with wide range of thickness and absorption coefficients deteriorates

Engineering Contradiction:
Improverefractive index measurement accuracyVSAvoidmeasurement range for thickness and absorption coefficient
Core Design Contradiction:
Measurement precisionVSAdaptability or versatility

Solution Approach 1:

The patent introduces dynamic adjustment capability for incident angle within the range of 0° to 85°, allowing the system to adapt to different measurement requirements. This dynamic parameter adjustment enables accurate measurement of thin films with wide thickness ranges (1 nm to 50 μm) and varied absorption coefficients, enhancing both precision and adaptability simultaneously.

Inventive Principle:
Principle #15Dynamics

3Measurement precision

If spectroscopic ellipsometry systems require oblique incident angles for measurement, then thin film measurement capability is improved, but device complexity and difficulty of detecting and measuring increase

Engineering Contradiction:
Improvethin film measurement capabilityVSAvoidsystem configuration complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent creates a universal measurement system that can handle various thin film characteristics (thickness from 1 nm to 50 μm, absorption coefficients from 10 to 10^5 cm^-1) using a single configurable setup with incident angles from 0° to 85°. This multi-functional capability reduces device complexity by eliminating the need for multiple specialized configurations while maintaining high measurement precision.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration allows for accurate refractive index measurement of thin films across a wide thickness and absorption range without the need for oblique incident angles, enhancing measurement flexibility and precision.

Implementation Method 1

a first light probe comprising a first distributed Bragg reflector which reflects light having a wavelength in a range of from 50 nm to 50 μm; a second light probe comprising a second distributed Bragg reflector which reflects light having a wavelength in a range of from 50 nm to 50 μm

Methodology Applied
Scientific EffectDistributed Bragg reflector reflection: Reflection

Data Source

PatentUS11366059B2System and method to measure refractive index at specific wavelengths
Publication Date: 2022.06.21 APPLIED MATERIALS INC
  • US11366059B2 patent drawing
  • US11366059B2 patent drawing
  • US11366059B2 patent drawing

AI summary

Apparatus, methods and are disclosed for measuring refractive index of a material film. The method and apparatus utilize a reference measurement and as series of reflectance measurements at a range of wavelengths and thickness values for the material film to determine the refractive index of the material film.