Wavelength Conversion Member Sintering Accuracy

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Solution Overview

Problem

Conventional wavelength conversion members for LEDs face challenges in achieving high dimensional and surface accuracy, leading to issues with luminescence intensity and color reproducibility, especially when formed into complex shapes, due to sintering processes that result in deformation and light scattering.

Innovation Solution

A method involving heat treatment of a powder mixture containing glass and inorganic phosphor powders followed by re-press molding with a die to produce wavelength conversion members with improved accuracy and reduced light scattering, using a neutral or reductive atmosphere and controlled temperature below 600°C, and a die with low surface roughness to minimize oxidation and thermal degradation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If a wavelength conversion member is formed by sintering a mixture of glass powder and inorganic phosphor powder, then the member can be produced in various shapes, but the dimensional accuracy and surface accuracy are significantly degraded due to shrinkage and deformation

Engineering Contradiction:
Improveshape varietyVSAvoiddimensional accuracy
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by pre-forming the wavelength conversion member into the desired shape before sintering. The green body is molded with the target geometry, and then sintering is performed to densify it. This preliminary shaping ensures that even after sintering shrinkage occurs, the final dimensions can be controlled more accurately, and surface accuracy is better preserved compared to direct sintering of loose powder.

Inventive Principle:
Principle #10Preliminary action

2Ease of manufacture

If air bubbles remain in the sintered body, then the manufacturing process is simpler, but light scattering loss increases and luminescence intensity is lowered

Engineering Contradiction:
Improveprocess simplicityVSAvoidlight scattering loss
Core Design Contradiction:
Ease of manufactureVSLoss of energy

Solution Approach 1:

The patent utilizes phase transitions during the sintering process to eliminate air bubbles. The heating cycle includes controlled heating rates and holding periods that allow trapped gases to escape as the material undergoes phase changes and densification. This results in a dense, bubble-free sintered body with minimal light scattering, while maintaining relative process simplicity.

Inventive Principle:
Principle #36Phase transitions

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables the production of wavelength conversion members with high surface accuracy, increased luminescence intensity, and consistent dimensions, reducing the need for grinding and polishing processes, thus enhancing light extraction efficiency and maintaining stable luminescence properties across various shapes.

Implementation Method 1

subjecting a preform made of a powder mixture containing a glass powder and an inorganic phosphor powder to heat treatment, thereby obtaining a sintered powder product

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 2

re-press molding the sintered powder product with a die

Methodology Applied
Scientific EffectCompression: Compression

Data Source

PatentUS8344404B2Wavelength conversion member and method for manufacturing the same
Publication Date: 2013.01.01 NIPPON ELECTRIC GLASS CO LTD
  • US8344404B2 patent drawing
  • US8344404B2 patent drawing
  • US8344404B2 patent drawing

AI summary

To provide a wavelength conversion member having good surface accuracy and dimensional accuracy even when processed in various shapes, and a method for manufacturing the same. A method for manufacturing a wavelength conversion member, including the steps of: subjecting a preform made of a powder mixture containing a glass powder and an inorganic phosphor powder to heat treatment, thereby obtaining a sintered powder product; and re-press molding the sintered powder product with a die.