X-ray Diffraction Apparatus for Transparent Sapphire Substrates

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Solution Overview

Problem

Conventional X-ray diffraction apparatuses face challenges in accurately specifying the in-plane position of crystal defects, especially in optically transparent substances like sapphire substrates, as they rely on imprecise methods and cannot utilize reflective optical microscopes for measurement.

Innovation Solution

An X-ray diffraction apparatus that combines X-ray topography with optical image-capturing means and video synthesis to generate synthesized video data, allowing for precise specification of in-plane positions within an X-ray topograph, enabling accurate alignment and measurement of crystal defects in transparent samples.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If conventional X-ray diffraction apparatuses are used to measure transparent samples, then the measurement can be performed, but the in-plane position of crystal defects cannot be accurately specified

Engineering Contradiction:
Improveposition specification accuracyVSAvoidoperational complexity
Core Design Contradiction:
Measurement precisionVSEase of operation

Solution Approach 1:

The patent combines X-ray topography means with optical image-capturing means into a single integrated apparatus. The X-ray topography provides internal structure information of transparent samples while the optical image-capturing means captures the external appearance and position. By merging these two measurement systems, the patent enables accurate specification of in-plane positions of crystal defects in transparent samples, resolving the contradiction between measurement precision and operational complexity.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent introduces video synthesis means as an intermediary that processes and combines images from both X-ray topography and optical image-capturing means. This intermediary system correlates the internal X-ray structure with the external optical appearance, enabling accurate position specification without requiring complex manual alignment operations. The video synthesis acts as a mediator that automatically integrates the two measurement systems.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Productivity

If trial and error method is used for alignment, then the measurement can be performed, but the measurement time is excessively long

Engineering Contradiction:
Improvemeasurement speedVSAvoidalignment time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent performs preliminary action by capturing optical images of the sample before X-ray measurement. The optical image-capturing means records the external appearance and position information in advance, which is then used to guide the X-ray measurement positioning. This preliminary capture of position information eliminates the need for time-consuming trial and error alignment during the actual measurement process.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent implements feedback by using the optical image information to guide and adjust the X-ray measurement positioning. The video synthesis means provides real-time correlation between optical appearance and X-ray internal structure, allowing operators to quickly identify and position defects without repeated trial and error attempts. The feedback loop significantly reduces alignment time and improves measurement efficiency.

Inventive Principle:
Principle #23Feedback

3Reliability

If reflective optical microscope is used for transparent samples, then the sample can be observed, but the measurement is not feasible due to optical transparency

Engineering Contradiction:
Improvedetection capabilityVSAvoidsample type compatibility
Core Design Contradiction:
ReliabilityVSAdaptability or versatility

Solution Approach 1:

The patent creates a universal measurement system that can handle both opaque and transparent samples. The optical image-capturing means serves as a universal interface that works with reflective optical microscopes for opaque samples while also being adaptable for transparent samples when combined with X-ray topography. This multi-functional approach allows the same apparatus to measure diverse sample types reliably.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The patent employs a composite measurement approach combining two different measurement techniques (optical imaging and X-ray topography) to measure transparent samples. Just as composite materials combine different material properties, this composite measurement system combines the strengths of optical imaging (for position reference) and X-ray topography (for internal structure) to achieve reliable detection of crystal defects in transparent samples that neither method could achieve alone.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables quick and accurate X-ray measurements by making transparent samples visible through X-ray topography and specifying arbitrary positions within the in-plane region, overcoming the limitations of conventional methods that rely on trial and error for alignment.

Implementation Method 1

X-ray topography is a measurement method devised so that a wide area of a sample is irradiated with X-rays, and the diffracted rays exiting the sample are detected in a plane

Methodology Applied
Scientific EffectX-ray diffraction: Bragg Diffraction

Data Source

PatentUS9074992B2X-ray diffraction apparatus and X-ray diffraction measurement method
Publication Date: 2015.07.07 RIGAKU CORP
  • US9074992B2 patent drawing
  • US9074992B2 patent drawing
  • US9074992B2 patent drawing

AI summary

There is provided an X-ray diffraction apparatus comprising an X-ray topography device for providing a spatial geometric correspondence to an X-ray exiting from a planar region of a sample to detect the X-ray as a planar X-ray topograph, and outputting the X-ray topograph as a signal; a two-dimensional imaging device for receiving a light-image of the planar region of the sample and outputting the light-image as a signal specified by planar positional information; and a video-synthesizing arithmetic control device for generating synthesized video data on the basis of an output signal from the X-ray topograph and an output signal from the imaging device.