Single-Crystal X-ray Analysis Sample Holder with Integrated Information Storage
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Solution Overview
Problem
Conventional single-crystal X-ray structure analysis using crystalline sponges requires precise and time-consuming operations for handling and installing small, fragile samples, which limits accessibility and efficiency, especially for non-specialists, and complicates sample management and storage.
Innovation Solution
A single-crystal X-ray structure analysis apparatus with a sample holder and applicator that facilitates quick and easy handling of small samples using a porous complex crystal, incorporating information acquisition and storage via bar codes or semiconductor devices, allowing for user-friendly operation without specialized knowledge.
Engineering Contradictions & Design Principles
Engineering Contradiction Analysis
1Measurement precision
If conventional single-crystal X-ray structure analysis using crystalline sponges is performed, then precise structure analysis capability is achieved, but the operation becomes complex and time-consuming due to precise handling requirements of small, fragile samples
Solution Approach 1:
The crystalline sponge is integrated within a holder that contains an information holding section, creating a nested structure where the fragile sample is protected inside a larger assembly that includes identification and management components. This allows the small, fragile crystalline sponge to be handled as part of a more robust integrated unit.
Solution Approach 2:
The holder serves as an intermediary between the operator and the fragile crystalline sponge. It provides a interface for handling, storing, and identifying the sample without requiring direct manipulation of the fragile sponge itself, thus simplifying operations while maintaining measurement precision.
2Productivity
If conventional handling procedures are used for crystalline sponges, then sample analysis is possible, but the risk of sample damage increases due to the small and fragile nature of the samples
Solution Approach 1:
The holder is designed to protect the crystalline sponge before handling operations begin. The structure provides physical support and protection for the fragile sample, cushioning it against damage during storage, transport, and installation procedures.
Solution Approach 2:
Information about the crystalline sponge is recorded in an information holding section before the analysis process begins. This preliminary documentation ensures proper handling procedures can be followed and helps maintain sample integrity throughout the analysis workflow.
3Ease of manufacture
If manual handling and installation of crystalline sponges is performed, then sample preparation is possible, but the time required for operations increases due to precise and careful manipulation needed
Solution Approach 1:
The holder combines multiple functions into a single component: physical support for the crystalline sponge, information storage for sample identification, and a standardized interface for installation. This merging reduces the number of separate operations needed and simplifies the overall preparation process.
Solution Approach 2:
The holder design appears to be universal, capable of accommodating crystalline sponges while providing standardized interfaces for handling and installation. This multi-functionality allows the same holder structure to perform multiple tasks (support, identify, protect, and facilitate installation) without requiring specialized procedures.
4Loss of information
If conventional sample management procedures are used, then basic tracking is possible, but comprehensive information management becomes complex without integrated information holding sections
Solution Approach 1:
The information holding section is merged with the physical holder structure, combining sample management information with the physical sample container. This integration ensures that information and sample remain associated without requiring separate tracking systems.
Solution Approach 2:
The holder with its integrated information holding section provides self-service functionality for sample management. The identification information is automatically available with the sample, enabling straightforward tracking and management without requiring complex external systems or procedures.
Applied Scientific Principles
This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.
Function Achieved in This Case
Enables high-yield, efficient, and versatile single-crystal X-ray structure analysis by simplifying the handling and management of small, fragile samples, making the process more accessible and reducing the risk of sample damage during operations.
Implementation Method 1
a porous complex crystal capable of soaking the sample in a plurality of fine pores formed therein
Implementation Method 2
an X-ray irradiation section that irradiates the X-rays from the X-ray source to the sample held by the sample holder attached to the goniometer; an X-ray detection measurement section that detects and measures X-rays diffracted or scattered by the sample
Data Source
AI summary
User-friendly single-crystal X-ray structure analysis apparatus and method for quickly performing a single-crystal X-ray structure analysis using a crystalline sponge and enabling the analysis including management of related information, and a sample holder and an applicator therefor are provided. There are provided a single-crystal X-ray structure analysis apparatus that performs a structure analysis of a material is provided, the apparatus comprising a sample holder that comprises a porous complex crystal capable of soaking the sample in a plurality of fine pores formed therein and that holds the sample; a goniometer that rotationally moves with the sample holder 250 being attached; and an information acquisition section 600 that acquires information about the porous complex crystal.