Synthesis process of creatine nitrate
Through the process flow of creatine reaction solution preparation, pretreatment of creatine preparation and nitrate preparation in the creatine nitrate synthesis process, the problems of low yield and high production cost of traditional processes are solved, and high yield and low cost creatine nitrate crystals are achieved.
CN119684163AInactive Publication Date: 2025-03-25HUOSHAN WEIKANG BIOTECHNOLOGY CO LTD
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Patent Information
- Application Number
- CN202510047923.0
- Authority / Receiving Office
- CN · China
- Patent Type
- Applications(China)
- Current Assignee / Owner
- Filing Date
- 2025-01-13
- Publication Date
- 2025-03-25
- Estimated Expiration
- Not applicable · inactive patent
AI Technical Summary
Technical Problem
The yield of traditional creatine nitrate synthesis process is low, and the mother liquor needs to be refined after crystallization, which increases production costs.
Method used
The process flow including preparation of nitric acid reaction solution, preparation of pretreatment creatine and preparation of nitrate is adopted. The pretreatment creatine is slowly added to the nitric acid reaction solution, and warm water is added to conduct a secondary reaction after cooling, and then color absorption is used with activated carbon, and finally freeze and crystallization is frozen.
Benefits of technology
It improves the crystallization yield of creatine nitrate, reduces side reactions, and reduces production costs.
✦ Generated by Eureka AI based on patent content.
Abstract
The invention discloses a synthesis process of creatine nitrate. The synthesis process comprises the following steps: (1) preparing a nitric acid reaction solution; (2) preparing pretreated creatine; and (3) preparing nitrate. According to the synthetic process, in the treatment process, fibrous sepiolite is used, then creatine monohydrate is added, so that one part of creatine monohydrate can be adsorbed by the fibrous sepiolite, the other part of creatine monohydrate is dissolved in water, a nitric acid reaction solution is slowly added, and the reaction time is shortened; creatine monohydrate adsorbed on the surface of fibrous sepiolite can be slowly dissolved in the solution and continuously participates in the reaction, warm water is added after cooling, stirring is performed for secondary reaction, reaction potential energy is provided for the reaction of residual materials, the product yield can be increased, and side reactions are reduced.
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