107 glue-based room-temperature end-capped silicone rubber and preparation method thereof

By mixing 107 gum, isobornyl silane and catalyst under a nitrogen atmosphere, and adding other modified components, a room temperature end-sealed silicone rubber with excellent mechanical properties and stability was prepared, which solved the catalytic and storage problems and poor storage stability in the prior art.

CN119708860AInactive Publication Date: 2025-03-28GUANGZHOU YIHENG SILICONE CO LTD
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Patent Information

Application Number
CN202411948377.X
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2024-12-27
Publication Date
2025-03-28
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

The existing room-temperature end-sealed silicone rubber based on 107 rubber has catalytic and storage difficulties, and due to its room-temperature crosslinking, the storage stability is poor, and it is prone to yellowing of vulcanization due to moisture, which reduces stability and increases viscosity, affects the final performance.

Method used

The 107 gum, isobornyl silane and the catalyst were mixed evenly under a nitrogen atmosphere. After stirring at room temperature, dimethyl silicone oil, modified filler, methyl trimethoxysilane, γ-aminopropyl triethoxysilane and organotin catalyst were added, and the room temperature end-sealed silicone rubber was obtained after evacuation and stirring.

Benefits of technology

It improves the thermal stability and processing performance of room-temperature end-sealing base rubber, optimizes the formula and components, and makes room-temperature end-sealing silicone rubber have excellent mechanical properties and stability, reduces viscosity changes during storage, and promotes aging resistance.

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Abstract

The invention discloses room-temperature end-capped silicone rubber based on 107 glue and a preparation method of the room-temperature end-capped silicone rubber, and relates to the technical field of silicone rubber. The preparation method comprises the following steps: step 1, uniformly mixing 107 glue, isobornyl silane and a catalyst in a nitrogen atmosphere; stirring at room temperature for 1-1.5 hours to obtain room-temperature end-capping base glue; and 2, uniformly stirring and mixing the room-temperature end-capped base rubber, dimethyl silicone oil, the modified filler, methyltrimethoxysilane, gamma-aminopropyltriethoxysilane and an organic tin catalyst in a nitrogen atmosphere, and finally vacuumizing and stirring to obtain the room-temperature end-capped silicone rubber. According to the invention, the prepared room-temperature end-capped silicone rubber has excellent mechanical properties and stability.
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