Method for separating capsorubin and other carotenoids from capsicum oleoresin

By using low-temperature saponification method and solvent extraction and crystallization technology in chili oleoresin, the degradation problem of carotenoids such as capsicum eretinoin at high temperature is solved, and efficient and low-loss separation and purification effects are achieved.

CN120344301APending Publication Date: 2025-07-18KEMIN INDUSTRIES INC
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Patent Information

Application Number
CN202380085280.8
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Priority Date
2022-11-11
Filing Date
2023-10-18
Publication Date
2025-07-18

AI Technical Summary

Technical Problem

Prior Art When separating capsicin and other carotenoids from chili oleoresin, conventional saponification methods are usually carried out at high temperatures, resulting in significant losses of these heat-unstable compounds, and lacking effective separation methods under mild conditions.

Method used

The low-temperature saponification method was used to treat the pepper oleoresin at ambient temperature of 50°C using propylene glycol and ethanol potassium hydroxide solution. The capsicum oleoresin, β-carotene, β-cryptoxanthin and zeaxanthin were then separated by solvent extraction and crystallization, avoiding the influence of alkali and heat at high temperatures.

Benefits of technology

The separation of high-purity capsicum eretinol and other carotenoids is achieved, avoiding the degradation of esterides at high temperatures, and improving the separation efficiency and product purity.

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Abstract

The present invention relates to a novel process for the isolation of capsorubin and several other carotenoids from capsicum oleoresin, which is a concentrated extract of capsicum fruit (Capsicum annuum). In another aspect, the present invention relates to the use of mild non-aqueous saponification processes and aqueous saponification processes for separating high purity capsorubin and other carotenoids from capsicum oleoresins at temperatures of about 20 DEG C to 50 DEG C. In another aspect, the present invention relates to a saponification process that produces a crystalline mixture of capsorubin, beta-carotene, beta-cryptoxanthin and zeaxanthin, which can be separated by solvent extraction and crystallization to provide high purity capsorubin as well as other carotenoids.
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