Continuous preparation process of high-purity magnesium oxide particles

By employing a continuous composite precipitation, hydrothermal crystallization, and gradient calcination process, the problem of unstable quality in the preparation of high-purity magnesium oxide has been solved, resulting in magnesium oxide particles with high purity, uniform particle size, and high thermal stability, suitable for high-end electronic devices, high-end ceramics, and optical materials.

CN122444200AActive Publication Date: 2026-07-24NANJING BAOCHUN NEW MATERIAL TECH CO LTD
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Patent Information

Application Number
CN202610933319.2
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2026-06-26
Publication Date
2026-07-24
Estimated Expiration
2046-06-26

AI Technical Summary

Technical Problem

Existing high-purity magnesium oxide preparation processes suffer from large batch-to-batch variations, unstable product quality, and difficulty in meeting the requirements of continuous mass production. Furthermore, impurity removal is incomplete, and thermal stability and density are insufficient, failing to meet the requirements of high-end applications.

Method used

A continuous composite precipitation, hydrothermal crystallization, and gradient calcination process is adopted to generate a uniform basic magnesium carbonate precursor through a composite precipitant. Combined with countercurrent washing and airflow classification, the purity and particle regularity of the product are improved. Gradient calcination matches the thermal decomposition kinetics of the precursor to ensure the thermal stability of the product.

Benefits of technology

Magnesium oxide particles with high purity (≥99.95%), uniform particle size (1.8-2.1μm), low impurities (2.1-4.2ppm) and high thermal stability (0.04%-0.08% thermal weight loss) have been achieved, making them suitable for applications in high-end electronic devices, high-end ceramics and optical materials.

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Abstract

The invention relates to the technical field of preparation of inorganic high-purity powder materials, in particular to a continuous preparation process of high-purity magnesium oxide particles, the purity of the magnesium oxide particles is not lower than 99.95%, the D50 particle size is 1.8-2.1 [mu] m, the particle size distribution span is 0.70-0.85, the total content of trace metal impurities is 2.1-4.2 ppm, the thermal weight loss ratio is 0.04-0.08%, and the bulk density is 0.48-0.55 g / cm < 3 >. A continuous production mode is adopted, a traditional intermittent process is replaced, whole-process continuous operation of raw material feeding, reacting, crystallizing, washing, drying, calcining and grading is achieved, the stability and uniformity of the production process are greatly improved, the batch quality difference is eliminated, and the industrial large-scale production requirement is met.
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