A reaction apparatus for producing a polypropylene nucleating agent

Abstract

The utility model relates to polypropylene nucleating agent production technical field discloses a reaction unit for producing polypropylene nucleating agent, including bottom column, ring frame, reaction kettle, the ring frame fixed setting is in the top of bottom column, the reaction kettle fixed sleeve joint is in the inside of ring frame, the top fixed mounting of reaction kettle inside has the connecting column, the bottom fixed mounting of connecting column has the shell, compared with traditional device, the device passes through the rotation of stirring vane no.

Description

Technical Field

[0001] This utility model relates to the field of polypropylene nucleating agent production technology, and more specifically, to a reaction apparatus for producing polypropylene nucleating agents. Background Technology

[0002] Polypropylene nucleating agents are important modifying additives for polypropylene (PP). They accelerate crystallization and refine grain size by altering PP's crystallization behavior. They are mainly classified into α-crystalline and β-crystalline nucleating agents, including inorganic, organic, and polymeric types. Preparation methods are diverse, such as chemical reaction synthesis. Applications include improved transparency, surface gloss, mechanical and thermal properties, and enhanced processing performance. Future development trends emphasize high efficiency, environmental friendliness, and multifunctionality. The production of polypropylene nucleating agents requires reaction equipment.

[0003] In conventional reaction equipment, materials are first placed inside the device, then a crushing mechanism breaks down the solids. A stirrer then moves the materials, ensuring thorough mixing between the solids and the solution. However, because some solids have densities different from the solution upon entering the device, sedimentation occurs, causing the solids to settle at the bottom. While the crushing mechanism mixes the solids with the solution at the bottom, the solution in the upper part of the device fails to mix evenly with the solids. This results in uneven mixing of solids and liquids within the device, necessitating modification and optimization. Utility Model Content

[0004] To overcome the shortcomings of the prior art, this utility model provides a reaction apparatus for producing polypropylene nucleating agents, which has the advantages of sufficient reaction and easy cleaning.

[0005] To achieve the above objectives, the present invention provides the following technical solution: a reaction apparatus for producing polypropylene nucleating agents, comprising a bottom column, an annular frame, and a reaction vessel, wherein the annular frame is fixedly disposed above the bottom column, and the reaction vessel is fixedly sleeved inside the annular frame;

[0006] A connecting column is fixedly installed on the top of the inner side of the reaction vessel, and a shell is fixedly installed on the bottom of the connecting column. A bevel gear one is rotatably installed on the top of the inner side of the shell, and bevel gear two is rotatably installed on both sides inside the shell. The bevel gear one and bevel gear two mesh with each other. A rotating shaft two is fixedly installed on one side of the bevel gear two. One end of the rotating shaft two extends to the outside of the shell. A stirring blade one is fixedly sleeved on the outer surface of the rotating shaft two, and a stirring blade two is fixedly sleeved on one end of the rotating shaft two.

[0007] As a preferred embodiment of this utility model, a crushing mechanism is fixedly installed at the bottom of the bevel gear, a rotating plate is fixedly installed at the bottom of the crushing mechanism, a connecting plate is fixedly installed on the side of the rotating plate, a cleaning plate is fixedly installed above one end of the connecting plate, and the side of the cleaning plate is movably connected to the inside of the reaction vessel.

[0008] As a preferred embodiment of this utility model, a stirring motor is fixedly installed above the reaction vessel, and a rotating shaft is fixedly installed at the bottom of the stirring motor. The bottom of the rotating shaft extends into the interior of the reaction vessel and passes through the upper and lower sides of the connecting column. The bottom of the rotating shaft extends into the interior of the outer shell and is fixedly connected to a bevel gear. A protective shell is fixedly installed above the reaction vessel, and the protective shell is located outside the stirring motor.

[0009] As a preferred embodiment of the present invention, the crushing mechanism includes a connecting roller fixedly disposed at the bottom of a bevel gear. The bottom of the connecting roller extends to the bottom of the outer casing and is fixedly mounted with an impeller. The bottom of the impeller is fixedly connected to a rotating plate, and a stirrer is fixedly mounted at the bottom of the rotating plate.

[0010] As a preferred embodiment of this utility model, an emulsifier motor is fixedly installed above the reaction tank. One end of the drive shaft of the emulsifier motor extends into the interior of the reaction tank and is fixedly installed with an emulsifying stirrer. A second protective shell is fixedly installed above the reaction tank, and the second protective shell is located outside the emulsifier motor.

[0011] As a preferred embodiment of this utility model, a feeding port is provided at the top of the reaction vessel, a jacket is fixedly sleeved on the outer side of the bottom of the reaction vessel, and a discharge valve is fixedly installed at the bottom of the reaction vessel, with the bottom of the discharge valve penetrating through the upper and lower sides of the jacket.

[0012] As a preferred embodiment of this utility model, a controller is fixedly installed on the side of the reaction vessel, and the controller is electrically connected to the discharge valve, the jacket, the stirring motor and the emulsifier motor.

[0013] Compared with the prior art, the beneficial effects of this utility model are as follows:

[0014] 1. This utility model uses a stirring motor to drive the rotation of a rotating shaft, which in turn drives the rotation of a bevel gear. When the bevel gear rotates, it drives the rotation of stirring blades one and two. Compared with traditional devices, this device uses the rotation of stirring blades one and two to stir the solid and liquid inside the device vertically. Compared with other devices, this device can stir the solid and solution by rotating the impeller and the emulsifying stirrer. It can stir the upper and lower layers of solid and solution, as well as the horizontal solid and solution, thereby improving the efficiency of stirring and reaction. This allows the solid and solution to mix quickly, thus improving the reaction efficiency of the device.

[0015] 2. This utility model drives the rotation of the first rotating shaft by starting the stirring motor, which in turn drives the rotation of the connecting roller. The rotation of the connecting roller drives the rotation of the rotating plate and the connecting plate. When the connecting plate rotates, it drives the rotation of the cleaning plate. Compared with traditional devices, this device cleans the inner wall of the reaction vessel by rotating the cleaning plate. Compared with traditional devices that directly rinse with water, this device can clean the inner wall of the reaction vessel more efficiently and can clean the inner wall of the reaction vessel as a whole, thus avoiding affecting the purity of the solution in the next use. Attached Figure Description

[0016] Figure 1 This is a schematic diagram of the structure of this utility model;

[0017] Figure 2 This is a schematic diagram of the internal structure of the reaction vessel of this utility model;

[0018] Figure 3 This is a schematic diagram of the internal structure of the outer shell of this utility model;

[0019] Figure 4 This utility model Figure 3 A magnified view of part A;

[0020] Figure 5 This is a schematic diagram of the connection structure between bevel gear one and bevel gear two of this utility model;

[0021] Figure 6 This is a schematic diagram of the emulsifying stirrer of this utility model.

[0022] In the diagram: 1. Base column; 2. Annular frame; 3. Reaction tank; 4. Controller; 5. Feed port; 6. Discharge valve; 7. Jacket; 8. Protective shell one; 9. Stirring motor; 10. Connecting column; 11. Outer shell; 12. Rotating shaft one; 13. Bevel gear one; 14. Bevel gear two; 15. Rotating shaft two; 16. Stirring blade one; 17. Stirring blade two; 18. Connecting roller; 19. Impeller; 20. Stirrer; 21. Protective shell two; 22. Emulsifier motor; 23. Emulsifying stirrer; 24. Rotating plate; 25. Connecting plate; 26. Cleaning plate. Detailed Implementation

[0023] The technical solutions of the present utility model will be clearly and completely described below with reference to the accompanying drawings of the embodiments. Obviously, the described embodiments are only some embodiments of the present utility model, and not all embodiments. Based on the embodiments of the present utility model, all other embodiments obtained by those of ordinary skill in the art without creative effort are within the protection scope of the present utility model.

[0024] like Figures 1 to 6 As shown, this utility model provides a reaction device for producing polypropylene nucleating agents, including a bottom column 1, an annular frame 2, and a reaction vessel 3. The annular frame 2 is fixedly disposed above the bottom column 1, and the reaction vessel 3 is fixedly sleeved inside the annular frame 2.

[0025] A connecting column 10 is fixedly installed on the top of the inner side of the reaction vessel 3. A shell 11 is fixedly installed on the bottom of the connecting column 10. A bevel gear 13 is rotatably installed on the top of the inner side of the shell 11. Bevel gears 14 are rotatably installed on both sides inside the shell 11. Bevel gears 13 and 14 mesh with each other. A rotating shaft 15 is fixedly installed on one side of the bevel gear 14. One end of the rotating shaft 15 extends to the outside of the shell 11. A stirring blade 16 is fixedly sleeved on the outer surface of the rotating shaft 15. A stirring blade 17 is fixedly sleeved on one end of the rotating shaft 15.

[0026] When the operator uses the equipment, they first start the stirring motor 9 via the controller 4. When the stirring motor 9 starts, it drives the rotation of the rotating shaft 12. When the rotating shaft 12 rotates, it drives the rotation of the bevel gear 13. When the bevel gear 13 rotates, it meshes with the bevel gear 14, so the rotation of the bevel gear 13 drives the rotation of the bevel gear 14. When the bevel gear 14 rotates, it drives the rotation of the rotating shaft 15. When the rotating shaft 15 rotates, it drives the rotation of the stirring blades 16 and 17, thereby fully mixing the solid and liquid inside the reaction vessel 3.

[0027] By starting the stirring motor 9, the rotating shaft 12 is driven to rotate, which in turn drives the bevel gear 14 to rotate. When the bevel gear 14 rotates, it drives the stirring blades 16 and 17 to rotate. Compared with traditional devices, this device uses the rotation of the stirring blades 16 and 17 to stir the solids and liquids inside the device vertically. Compared with other devices, the device uses the rotation of the impeller 19 and the emulsifying stirrer 23 to stir the solids and solutions. This device can stir the upper and lower layers of solids and solutions, as well as the horizontal layers of solids and solutions, thereby improving the efficiency of stirring and reaction. This allows the solids and solutions to mix quickly, thus improving the efficiency of the device's reaction.

[0028] Among them, a crushing mechanism is fixedly installed at the bottom of the bevel gear 13, a rotating plate 24 is fixedly installed at the bottom of the crushing mechanism, a connecting plate 25 is fixedly installed on the side of the rotating plate 24, a cleaning plate 26 is fixedly installed on the top of one end of the connecting plate 25, and the side of the cleaning plate 26 is movably connected to the inside of the reaction tank 3.

[0029] When the operator uses the device, they first start the stirring motor 9 via the controller 4 to drive the rotating shaft 12 to rotate. When the rotating shaft 12 rotates, it drives the bevel gear 13 to rotate. As the bevel gear 13 rotates, it drives the connecting roller 18 to rotate. When the connecting roller 18 rotates, it drives the rotating plate 24 to rotate. When the rotating plate 24 rotates, it drives the connecting plate 25 to rotate. When the connecting plate 25 rotates, it drives the cleaning plate 26 to rotate. As the cleaning plate 26 rotates, it cleans the inner wall of the reaction vessel 3.

[0030] By starting the stirring motor 9, the rotating shaft 12 is driven to rotate, which in turn drives the connecting roller 18 to rotate. The rotation of the connecting roller 18 drives the rotating plate 24 and the connecting plate 25 to rotate. When the connecting plate 25 rotates, it drives the cleaning plate 26 to rotate. Compared with the traditional device, this device cleans the inner wall of the reaction tank 3 by rotating the cleaning plate 26. Compared with the traditional device, which directly rinses with water, this device can clean the inner wall of the reaction tank 3 more efficiently and can clean the inner wall of the reaction tank 3 as a whole, thereby avoiding affecting the purity of the solution in the next use.

[0031] The reaction vessel 3 is fixedly mounted with a stirring motor 9 on top. A rotating shaft 12 is fixedly mounted on the bottom of the stirring motor 9. The bottom of the rotating shaft 12 extends into the interior of the reaction vessel 3 and passes through the upper and lower sides of the connecting column 10. The bottom of the rotating shaft 12 extends into the interior of the outer shell 11 and is fixedly connected to the bevel gear 13. A protective shell 8 is fixedly mounted on top of the reaction vessel 3. The protective shell 8 is located outside the stirring motor 9.

[0032] The controller 4 starts the stirring motor 9, which drives the rotating shaft 12 to rotate. As the rotating shaft 12 rotates, it drives the bevel gear 13 to rotate.

[0033] The crushing mechanism includes a connecting roller 18 fixedly disposed at the bottom of the bevel gear 13. The bottom of the connecting roller 18 extends to the bottom of the outer casing 11 and is fixedly mounted with an impeller 19. The bottom of the impeller 19 is fixedly connected to the rotating plate 24, and an agitator 20 is fixedly mounted at the bottom of the rotating plate 24.

[0034] The rotation of the bevel gear 13 drives the rotation of the connecting roller 18, which in turn drives the rotation of the impeller 19, thus crushing the solids at the bottom of the inner side of the device.

[0035] An emulsifier motor 22 is fixedly installed on the top of the reaction tank 3. One end of the drive shaft of the emulsifier motor 22 extends into the interior of the reaction tank 3 and is fixedly installed with an emulsifying stirrer 23. A protective shell 21 is fixedly installed on the top of the reaction tank 3, and the protective shell 21 is located outside the emulsifier motor 22.

[0036] The emulsifier motor 22 is started by the controller 4 to drive the rotation of the emulsifying stirrer 23, thereby mixing the solids and solutions inside the device.

[0037] The reaction tank 3 has a feeding port 5 at the top, a jacket 7 is fixedly sleeved on the bottom outside of the reaction tank 3, and a discharge valve 6 is fixedly installed at the bottom of the reaction tank 3. The bottom of the discharge valve 6 passes through the upper and lower sides of the jacket 7.

[0038] Raw materials can be added into the device through the feed port 5, and the raw materials can be discharged from the device through the discharge valve 6. The device is heated through the jacket 7.

[0039] The side of the reaction tank 3 is fixedly equipped with a controller 4, which is electrically connected to the discharge valve 6, the jacket 7, the stirring motor 9 and the emulsifier motor 22.

[0040] The design of controller 4 controls the operation of the device, thereby improving the safety of the device during operation.

[0041] Working principle and usage process of this utility model:

[0042] When the operator uses the equipment, they first start the stirring motor 9 via the controller 4. When the stirring motor 9 starts, it drives the rotation of the rotating shaft 12. When the rotating shaft 12 rotates, it drives the rotation of the bevel gear 13. When the bevel gear 13 rotates, it meshes with the bevel gear 14, so the rotation of the bevel gear 13 drives the rotation of the bevel gear 14. When the bevel gear 14 rotates, it drives the rotation of the rotating shaft 15. When the rotating shaft 15 rotates, it drives the rotation of the stirring blades 16 and 17, thereby fully mixing the solid and liquid inside the reaction vessel 3.

[0043] When the operator uses the device, they first start the stirring motor 9 via the controller 4 to drive the rotating shaft 12 to rotate. When the rotating shaft 12 rotates, it drives the bevel gear 13 to rotate. As the bevel gear 13 rotates, it drives the connecting roller 18 to rotate. When the connecting roller 18 rotates, it drives the rotating plate 24 to rotate. When the rotating plate 24 rotates, it drives the connecting plate 25 to rotate. When the connecting plate 25 rotates, it drives the cleaning plate 26 to rotate. As the cleaning plate 26 rotates, it cleans the inner wall of the reaction vessel 3.

[0044] It should be noted that, in this document, relational terms such as "first" and "second" are used only to distinguish one entity or operation from another, and do not necessarily require or imply any such actual relationship or order between these entities or operations. Furthermore, the terms "comprising," "including," or any other variations thereof are intended to cover non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to such process, method, article, or apparatus.

[0045] Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made to these embodiments without departing from the principles and spirit of the present invention, the scope of which is defined by the appended claims and their equivalents.

Claims

1. A reaction device for producing polypropylene nucleating agent, comprising a bottom column (1), a ring frame (2), a reaction tank (3), characterized in that: The annular frame (2) is fixedly installed above the bottom column (1), and the reaction vessel (3) is fixedly sleeved on the inner side of the annular frame (2); A connecting column (10) is fixedly installed on the top of the inner side of the reaction vessel (3). A shell (11) is fixedly installed on the bottom of the connecting column (10). A bevel gear (13) is rotatably installed on the top of the inner side of the shell (11). A bevel gear (14) is rotatably installed on both sides inside the shell (11). The bevel gear (13) and the bevel gear (14) mesh with each other. A rotating shaft (15) is fixedly installed on one side of the bevel gear (14). One end of the rotating shaft (15) extends to the outside of the shell (11). A stirring blade (16) is fixedly sleeved on the outer surface of the rotating shaft (15). A stirring blade (17) is fixedly sleeved on one end of the rotating shaft (15).

2. The reaction apparatus for producing a polypropylene nucleating agent according to claim 1, characterized by: A crushing mechanism is fixedly installed at the bottom of the bevel gear (13), a rotating plate (24) is fixedly installed at the bottom of the crushing mechanism, a connecting plate (25) is fixedly installed on the side of the rotating plate (24), a cleaning plate (26) is fixedly installed above one end of the connecting plate (25), and the side of the cleaning plate (26) is movably connected to the inside of the reaction vessel (3).

3. The reaction apparatus for producing a polypropylene nucleating agent according to claim 1, characterized by: A stirring motor (9) is fixedly installed on the top of the reaction vessel (3). A rotating shaft (12) is fixedly installed on the bottom of the stirring motor (9). The bottom of the rotating shaft (12) extends into the interior of the reaction vessel (3) and passes through the upper and lower sides of the connecting column (10). The bottom of the rotating shaft (12) extends into the interior of the outer shell (11) and is fixedly connected to the bevel gear (13). A protective shell (8) is fixedly installed on the top of the reaction vessel (3). The protective shell (8) is located outside the stirring motor (9).

4. The reaction apparatus for producing a polypropylene nucleating agent according to claim 2, wherein: The crushing mechanism includes a connecting roller (18) fixedly disposed at the bottom of a bevel gear (13). The bottom of the connecting roller (18) extends to the bottom of the outer casing (11) and is fixedly mounted with an impeller (19). The bottom of the impeller (19) is fixedly connected to a rotating plate (24), and a stirrer (20) is fixedly mounted at the bottom of the rotating plate (24).

5. The reaction apparatus for producing a polypropylene nucleating agent according to claim 1, wherein: An emulsifier motor (22) is fixedly installed above the reaction tank (3). One end of the drive shaft of the emulsifier motor (22) extends into the interior of the reaction tank (3) and is fixedly installed with an emulsifying stirrer (23). A protective shell (21) is fixedly installed above the reaction tank (3). The protective shell (21) is located outside the emulsifier motor (22).

6. The reaction apparatus for producing a polypropylene nucleating agent according to claim 1, characterized by: The reaction vessel (3) has a feeding port (5) at the top, a jacket (7) is fixedly sleeved on the bottom outside of the reaction vessel (3), and a discharge valve (6) is fixedly installed at the bottom of the reaction vessel (3). The bottom of the discharge valve (6) passes through the upper and lower sides of the jacket (7).

7. The reaction apparatus for producing a polypropylene nucleating agent according to claim 1, wherein: A controller (4) is fixedly installed on the side of the reaction vessel (3). The controller (4) is electrically connected to the discharge valve (6), the jacket (7), the stirring motor (9), and the emulsifier motor (22).

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