Method for preparing high-purity yttrium oxide ceramic for etching based on segmented oxygen feeding calcination

By employing a segmented oxygen-assisted calcination and three-stage sintering method, the problems of low purity and insufficient flexural strength of yttrium oxide ceramics were solved, enabling the preparation of high-purity yttrium oxide ceramics and ensuring the material's density and flexural strength.

CN122403983APending Publication Date: 2026-07-17成都超纯应用材料股份有限公司
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
成都超纯应用材料股份有限公司
Filing Date
2026-04-17
Publication Date
2026-07-17

AI Technical Summary

Technical Problem

Existing technologies for preparing high-purity yttrium oxide ceramics suffer from several drawbacks. Insufficient reaction of organic matter in the yttrium oxide preform leads to low ceramic purity, and incomplete grain growth during sintering results in crystal defects and insufficient flexural strength.

Method used

The method employs segmented oxygen calcination and three-stage sintering, including oxygen calcination in the main decomposition stage and the deep decomposition stage, combined with slow heating and long holding time, followed by three-stage sintering, gradually reducing the heating rate to ensure complete decomposition of organic matter and complete grain growth.

Benefits of technology

This improved the purity and flexural strength of yttrium oxide ceramics, prevented ceramic cracking, and ensured the density and high purity of the material.

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Abstract

本申请涉及功能陶瓷技术领域,具体涉及一种基于分段通氧煅烧制备蚀刻用高纯氧化钇陶瓷的方法,通过制得的氧化钇素胚依次进行两段的分段通氧煅烧和升温速率呈梯度下降的三段烧结,以提高氧化钇陶瓷材料的纯度、使晶粒生长完全,提高烧结密度和抗弯强度。
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