Saponification negative pressure reaction kettle

By designing a negative pressure reactor, using a blower and a one-way valve system to maintain negative pressure inside the reactor and eliminate bubbles, and combining stirring blades and heat-conducting blocks to improve the heating effect, the problem of bubbles affecting the saponification quality during the saponification process is solved, and efficient saponification is achieved.

CN224167463UActive Publication Date: 2026-04-28JINZHOU YULIYUAN ORGANIC CHEMICAL RAW MATERIALS CO LTD
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Patent Information

Authority / Receiving Office
CN · China
Patent Type
Utility models(China)
Current Assignee / Owner
JINZHOU YULIYUAN ORGANIC CHEMICAL RAW MATERIALS CO LTD
Filing Date
2025-05-16
Publication Date
2026-04-28

AI Technical Summary

Technical Problem

In existing reaction vessels, the raw materials are prone to generating bubbles during the saponification process, which affects the saponification quality.

Method used

A saponification negative pressure reactor was designed. The reactor body is kept under negative pressure by a blower and a one-way valve system to eliminate air bubbles in the raw materials. The sealing cover prevents outside air from entering. The heating effect is improved by combining stirring blades and heat-conducting blocks.

Benefits of technology

It effectively eliminates air bubbles inside the reactor, improves saponification effect, ensures saponification quality, and maintains a negative pressure state inside the reactor to prevent external air from affecting it.

✦ Generated by Eureka AI based on patent content.

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Abstract

The utility model discloses a saponification negative pressure reaction kettle which comprises a kettle body, a shell is fixedly installed on the inner wall face of the kettle body, an air outlet pipe communicated with the shell is fixedly installed in the side wall of the kettle body, and a first one-way valve is arranged on the air outlet pipe. An exhaust fan is fixedly mounted on the outer side wall surface of the kettle body, the air inlet end of the exhaust fan is communicated with an air inlet pipe, and one end, far away from the exhaust fan, of the air inlet pipe penetrates through the upper wall of the kettle body; a second one-way valve is arranged on the air inlet pipe, and air in the kettle body can be pumped under the action of the exhaust fan, the air inlet pipe and the second one-way valve, so that the interior of the kettle body is in a negative pressure state, bubbles in raw materials can disappear quickly, and the saponification effect is improved; meanwhile, under the action of the sealing cover, the feeding pipe can be sealed, so that external air is prevented from entering the kettle body from the feeding pipe to influence the negative pressure effect, and convenience is brought to people.
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Description

Technical Field

[0001] This utility model relates to the technical field of reaction vessels, specifically a saponification negative pressure reaction vessel. Background Technology

[0002] In a broad sense, a reaction vessel is a container where physical or chemical reactions occur. Through structural design and parameter configuration, it achieves the heating, evaporation, cooling, and low-to-high-speed mixing functions required by the process. Reaction vessels are widely used in petroleum, chemical, rubber, pesticide, dye, pharmaceutical, and food industries as pressure vessels to complete processes such as vulcanization, nitration, hydrogenation, hydrocarbonation, polymerization, and condensation.

[0003] Existing reaction vessels can only heat and stir the saponification raw materials during processing. However, after stirring, the raw materials are prone to generating a large number of bubbles, which can affect the saponification process and thus the quality of the saponification. Utility Model Content

[0004] To solve the above problems, namely the problems raised in the background art, this utility model proposes a saponification negative pressure reactor, including a reactor body, a shell fixedly installed on the inner wall of the reactor body, an annular pipe fixedly installed on the lower wall of the reactor body, an air inlet pipe fixedly connected to the annular pipe, and one end of the air inlet pipe penetrating the lower wall of the reactor body;

[0005] An exhaust pipe communicating with the shell is fixedly installed inside the side wall of the vessel body, and a first one-way valve is provided on the exhaust pipe;

[0006] An exhaust fan is fixedly installed on the outer wall of the vessel body. The air inlet end of the exhaust fan is connected to an air inlet pipe, and the end of the air inlet pipe away from the exhaust fan passes through the upper wall of the vessel body.

[0007] A second one-way valve is installed on the air inlet pipe.

[0008] Preferably, the upper wall of the vessel is provided with a feed pipe, and one end of the feed pipe is provided with a sealing cap;

[0009] A discharge pipe is fixedly installed on the lower end face of the shell, and one end of the discharge pipe penetrates the lower wall of the vessel body;

[0010] The lower wall of the housing has a discharge port that communicates with the discharge pipe, and a valve is provided on the discharge pipe.

[0011] Preferably, the vessel body is provided with a stirring shaft, the top end of the stirring shaft rotatably penetrates the upper wall of the vessel body, a bracket is fixedly installed on the upper wall of the vessel body, a motor is fixedly installed on the bracket, and the output end of the motor is fixedly connected to the top end of the stirring shaft;

[0012] A stirring blade is fixedly installed inside the vessel and on the outer surface of the stirring shaft.

[0013] Preferably, a heat-conducting block is fixedly installed inside the side wall of the housing.

[0014] Preferably, a connecting pipe is fixedly connected to the annular pipe, and a third one-way valve is provided on the connecting pipe.

[0015] The beneficial technical effects of this utility model are as follows: under the action of the exhaust fan, the air inlet pipe and the second one-way valve, the air inside the reactor can be drawn, so that the reactor is in a negative pressure state, which can make the bubbles in the raw materials disappear quickly and improve the saponification effect.

[0016] At the same time, the sealing cap can seal the feed pipe, preventing outside air from entering the reactor body through the feed pipe and affecting the negative pressure effect, thus bringing convenience to people. Attached Figure Description

[0017] Figure 1 The diagram shows a front sectional view of the present invention.

[0018] Figure 2 This utility model is shown Figure 1 A magnified structural diagram of part A.

[0019] The attached diagram shows the following components: 1. vessel body; 2. shell; 3. annular pipe; 4. air inlet pipe; 5. air outlet pipe; 6. first one-way valve; 7. exhaust fan; 8. air inlet pipe; 9. second one-way valve; 10. feed pipe; 11. sealing cover; 12. discharge pipe; 13. valve; 14. stirring shaft; 15. stirring blade; 16. heat-conducting block; 17. connecting pipe; 18. third one-way valve. Detailed Implementation

[0020] Preferred embodiments of the present invention will now be described with reference to the accompanying drawings. Those skilled in the art should understand that these embodiments are merely illustrative of the technical principles of the present invention and are not intended to limit the scope of protection of the present invention.

[0021] This utility model proposes a saponification negative pressure reactor, including a reactor body 1, a shell 2 fixedly installed on the inner wall of the reactor body 1, an annular pipe 3 fixedly installed on the lower wall of the reactor body 1, an air inlet pipe 4 fixedly connected to the annular pipe 3, and one end of the air inlet pipe 4 penetrating the lower wall of the reactor body 1.

[0022] The annular pipe 4 is connected to the external steam pipe. Under the action of the inlet pipe 4, the external steam can enter between the shell 2 and the side wall of the vessel 1 to heat the side wall of the shell 2.

[0023] An exhaust pipe 5, which communicates with the shell 2, is fixedly installed inside the side wall of the vessel body 1. A first one-way valve 6 is provided on the exhaust pipe 5.

[0024] The vent pipe 5 facilitates the discharge of air between the shell 2 and the side wall of the vessel 1 to the outside, while the first one-way valve 6 prevents outside air from entering the space between the shell 2 and the side wall of the vessel 1 through the vent pipe 5.

[0025] An exhaust fan 7 is fixedly installed on the outer wall of the vessel body 1. The air inlet end of the exhaust fan 7 is connected to an air inlet pipe 8. The end of the air inlet pipe 8 away from the exhaust fan 7 passes through the upper wall of the vessel body 1.

[0026] A second check valve 9 is installed on the air inlet pipe 8;

[0027] Under the action of the air inlet pipe 8, the exhaust fan 7 can draw the air in the vessel body 1, making the space inside it a negative pressure state. At the same time, the second one-way valve 9 can prevent the air drawn out by the exhaust fan 7 from flowing back into the vessel body 1 and affecting the negative pressure state.

[0028] Specifically, the upper wall of the vessel body 1 is provided with a feed pipe 10, and one end of the feed pipe 10 is provided with a sealing cap 11;

[0029] The feed pipe 10 allows workers to easily add the raw materials to be saponified into the reactor body 1. The sealing cover 11 can seal one end of the feed pipe 10 to prevent outside air from entering the reactor body 1 through the feed pipe 10. At this time, the side wall of the shell 2, which has been heated by steam, can heat the raw materials to saponify them. A temperature sensor is fixedly installed on the outer surface of the shell 2. The temperature sensor is electrically connected to the external control panel and can detect the temperature of the raw materials.

[0030] A discharge pipe 12 is fixedly installed on the lower end face of the shell 2, and one end of the discharge pipe 12 penetrates the lower wall of the vessel body 1;

[0031] A discharge port communicating with the discharge pipe 12 is formed in the lower wall of the housing 2, and a valve 13 is provided on the discharge pipe 12;

[0032] When valve 13 is open, the saponified raw material can be easily discharged through the discharge pipe 12; when closed, the discharge pipe 12 can be sealed.

[0033] Specifically, the vessel body 1 is equipped with a stirring shaft 14. The top end of the stirring shaft 14 rotates through the upper wall of the vessel body 1. A bracket is fixedly installed on the upper wall of the vessel body 1. A motor is fixedly installed on the bracket. The output end of the motor is fixedly connected to the top end of the stirring shaft 14.

[0034] A stirring blade 15 is fixedly installed inside the vessel body 1 and on the outer surface of the stirring shaft 14;

[0035] The rotation of the motor output end can drive the stirring shaft 14 to rotate. At this time, the rotation of the stirring shaft 14 can drive the stirring blade 15 to stir the raw materials and improve the saponification effect.

[0036] Specifically, a heat-conducting block 16 is fixedly installed inside the side wall of the housing 2;

[0037] The heat-conducting block 15 can absorb the heat of the steam and direct the absorbed heat to the raw materials, thereby improving the heating effect on the raw materials.

[0038] Specifically, a connecting pipe 17 is fixedly connected to the annular pipe 3, and a third one-way valve 18 is provided on the connecting pipe 17.

[0039] The connecting pipe 17 can be connected to an external steam pipe, allowing steam to be delivered into the annular pipe 3. At the same time, the third one-way valve 18 can prevent the steam in the annular pipe 3 from flowing back. Meanwhile, the lower wall of the vessel body 1 is fixedly connected to a water outlet pipe, which can discharge the water generated by the steam. A sealing cap is provided on the water outlet pipe to seal one end of the water outlet pipe.

[0040] Working principle: First, the raw materials to be saponified are added to the vessel body 1 through the feed pipe 10, ensuring the raw materials are located inside the shell 2. At this time, the operator seals one end of the feed pipe 10 with the sealing cap 11 to prevent outside air from entering the vessel body 1. Then, the external steam pipe is connected to the connecting pipe 17 to ensure continuity, and steam is transported to the annular pipe 3. The steam in the annular pipe 3 is then transported through the air inlet pipe 4 to the space between the side wall of the vessel body 1 and the shell 2, heating the side wall of the shell 2 and the heat-conducting block 16. Simultaneously, under the action of the first one-way valve 6 of the air outlet pipe 5, the gas between the side wall of the vessel body 1 and the shell 2 can be discharged to the outside, allowing steam to fill the space between the side wall of the vessel body 1 and the shell 2, improving the heating effect on the side wall of the shell 2 and the heat-conducting block 16. At this point, the process is complete. The rotation of the motor output can drive the stirring shaft 14 to rotate. At this time, the rotation of the stirring shaft 14 can drive the stirring blade 15 to stir the raw material, so that the raw material can contact the side wall of the shell 2 and the heat-conducting block 16, which can improve the heating effect. After stirring is completed, the exhaust fan 7 is started. Under the action of the air inlet pipe 8, the exhaust fan 7 can draw the air in the vessel 1, making the space inside it a negative pressure state. At the same time, the negative pressure state inside the vessel 1 can make the air bubbles in the raw material disappear. Meanwhile, the second one-way valve 9 can prevent the air drawn out by the exhaust fan 7 from flowing back into the vessel 1, affecting the negative pressure state and improving the negative pressure effect. After saponification is completed, the valve 13 is opened, which can discharge the saponified raw material in the shell 2 from the storage tank 12 for easy collection and convenience.

[0041] Although the present invention has been described with reference to preferred embodiments, various modifications can be made to it and components can be replaced with equivalents without departing from the scope of the present invention. In particular, the technical features mentioned in the various embodiments can be combined in any manner as long as there is no structural conflict. The present invention is not limited to the specific embodiments disclosed herein, but includes all technical solutions falling within the scope of the claims.

[0042] In the description of this utility model, terms such as "center," "upper," "lower," "left," "right," "vertical," "horizontal," "inner," and "outer," which indicate direction or positional relationships, are based on the direction or positional relationships shown in the accompanying drawings. These are used merely for ease of description and do not indicate or imply that the device or element must have a specific orientation, or be constructed and operated in a specific orientation; therefore, they should not be construed as limitations on this utility model. Furthermore, the terms "first," "second," and "third" are used for descriptive purposes only and should not be construed as indicating or implying relative importance.

[0043] Furthermore, it should be noted that, in the description of this utility model, unless otherwise explicitly specified and limited, the terms "installation," "connection," and "joining" should be interpreted broadly. For example, they can refer to a fixed connection, a detachable connection, or an integral connection; they can refer to a mechanical connection or an electrical connection; they can refer to a direct connection or an indirect connection through an intermediate medium; and they can refer to the internal connection of two components. Those skilled in the art can understand the specific meaning of the above terms in this utility model according to the specific circumstances.

[0044] The term "comprising" or any other similar term is intended to cover non-exclusive inclusion, such that a process, article, or apparatus / device that comprises a list of elements includes not only those elements but also other elements not expressly listed, or elements inherent to those processes, articles, or apparatus / devices.

[0045] The technical solution of this utility model has been described in conjunction with the preferred embodiments shown in the accompanying drawings. However, it will be readily understood by those skilled in the art that the protection scope of this utility model is obviously not limited to these specific embodiments. Without departing from the principle of this utility model, those skilled in the art can make equivalent changes or substitutions to the relevant technical features, and the technical solutions after these changes or substitutions will all fall within the protection scope of this utility model.

Claims

1. A saponification negative pressure reactor, comprising a reactor body (1), characterized in that, A shell (2) is fixedly installed on the inner wall of the vessel body (1), and an annular pipe (3) is fixedly installed on the lower wall of the vessel body (1). An air inlet pipe (4) is fixedly connected to the annular pipe (3), and one end of the air inlet pipe (4) penetrates the lower wall of the vessel body (1). An exhaust pipe (5) communicating with the shell (2) is fixedly installed inside the side wall of the vessel body (1), and a first one-way valve (6) is provided on the exhaust pipe (5). An exhaust fan (7) is fixedly installed on the outer wall of the vessel body (1). The air inlet end of the exhaust fan (7) is connected to an air inlet pipe (8). The end of the air inlet pipe (8) away from the exhaust fan (7) passes through the upper wall of the vessel body (1). A second one-way valve (9) is provided on the air inlet pipe (8).

2. The saponification negative pressure reactor according to claim 1, characterized in that, The upper wall of the vessel body (1) is provided with a feed pipe (10), and one end of the feed pipe (10) is provided with a sealing cap (11). A discharge pipe (12) is fixedly installed on the lower end face of the shell (2), and one end of the discharge pipe (12) penetrates the lower wall of the vessel body (1); The lower wall of the housing (2) has a discharge port that communicates with the discharge pipe (12), and a valve (13) is provided on the discharge pipe (12).

3. The saponification negative pressure reactor according to claim 1, characterized in that, The vessel body (1) is provided with a stirring shaft (14). The top end of the stirring shaft (14) rotates through the upper wall of the vessel body (1). A bracket is fixedly installed on the upper wall of the vessel body (1). A motor is fixedly installed on the bracket. The output end of the motor is fixedly connected to the top end of the stirring shaft (14). A stirring blade (15) is fixedly installed inside the vessel body (1) and on the outer surface of the stirring shaft (14).

4. The saponification negative pressure reactor according to claim 1, characterized in that, A heat-conducting block (16) is fixedly installed inside the side wall of the housing (2).

5. The saponification negative pressure reactor according to claim 1, characterized in that, A connecting pipe (17) is fixedly connected to the annular pipe (3), and a third one-way valve (18) is provided on the connecting pipe (17).