Method for observing microscopic formation process of porous membrane prepared by phase separation method

By designing an observation device consisting of a cover glass slide, a slide, and a gasket, and controlling the non-solvent flow rate, the problem of poor repeatability in the preparation of porous membranes by phase separation method was solved, and efficient and accurate observation of the phase separation mechanism was achieved.

WO2026103414A1 Publication Date: 2026-05-21DALIAN INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES
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Patent Information

Application Number
PCT/CN2025/127493
Authority / Receiving Office
WO · WO
Patent Type
Applications
Current Assignee / Owner
Priority Date
2024-11-15
Filing Date
2025-10-14
Publication Date
2026-05-21

AI Technical Summary

Technical Problem

Existing technologies suffer from poor repeatability and difficulty in accurately controlling the distribution of non-solvent flow fields during the preparation of porous membranes via phase separation, resulting in unclear membrane pore structure formation mechanisms and limited observation methods.

Method used

An observation device was designed, including a coverslip, a slide, a fixing device, and a gasket. By adjusting the gap width between the coverslip and the slide, the flow rate of the non-solvent is controlled, and the phase separation process of the polymer solution and the non-solvent is observed using a microscope.

Benefits of technology

This study achieved highly repeatable observation of the microscopic formation process of porous membranes prepared by phase separation, elucidated the phase separation mechanism, and improved the stability and reliability of experimental results.

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Abstract

Disclosed in the present invention are a method and device for observing a microscopic formation process of a porous membrane prepared by a phase separation method. Observation using the device has the advantages such as easy disassembly and cleaning, and good repeatability. The microstructural evolution and kinetic rate during the formation of porous membranes from different non-solvent induced polymer solutions can be observed. The experimental results are clear and intuitive, enabling simple, accurate, and convenient evaluation of the functions and effects of different non-solvents, which is of great significance for porous membrane preparation research and the field of interface synthesis.
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