Preparation method of solid peracetic acid

By using hydrogen peroxide with a mass concentration of 30-50 wt% for oxidation and esterification reaction, the safety accident risk of synthesis of solid peracetic acid in high-concentration hydrogen peroxide in the prior art has been successfully solved, and safe, stable and convenient production of solid peracetic acid is achieved.

CN120081771AInactive Publication Date: 2025-06-03HUZHOU BAITE BIOLOGICAL TECH CO LTD
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Patent Information

Application Number
CN202510068955.9
Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
Filing Date
2025-01-16
Publication Date
2025-06-03
Estimated Expiration
Not applicable · inactive patent

AI Technical Summary

Technical Problem

The use of high concentration of hydrogen peroxide in the prior art to synthesize solid peracetic acid has a risk of safety accidents, which limits its large-scale production and wide application.

Method used

Hydrogen peroxide with a mass concentration of 30-50 wt% was used for oxidation reaction, and anhydrous peracetic acid was reacted by reaction of acetic anhydride with hydrogen peroxide, and esterification was carried out with sodium perborate and acetic acid, and finally solid peracetic acid was obtained through the separation and purification step.

Benefits of technology

It reduces safety risks in the production process, simplifies process control, improves the stability and safety of solid peracetic acid, is suitable for industrial production, and reduces logistics costs and difficulty in use.

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Abstract

The invention relates to the technical field of disinfectant preparation, and particularly discloses a preparation method of solid peracetic acid. Firstly, hydrogen peroxide and acetic anhydride are subjected to an oxidation reaction to prepare anhydrous peracetic acid, and then sodium perborate and anhydrous peracetic acid are subjected to an esterification reaction to prepare solid peracetic acid. Compared with the prior art, the method has the advantages that the use of high-concentration hydrogen peroxide is avoided, the solid peracetic acid is obtained by a safer, simpler and more convenient method, and the method is suitable for industrial production.
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