455 results about "Acetic anhydride" patented technology

The invention relates to the technical field of polyimide films, in particular to a PI film and a preparation method thereof. The PI film comprises the following raw materials in parts by mass: 100-150 parts of soluble polyimide resin, 5-15 parts of biphenyl epoxy resin, 5-10 parts of activated titanium dioxide, 1-5 parts of a curing agent and 1-3 parts of a curing accelerator, the soluble polyimide resin comprises the following raw materials in parts by mass: 5-10 parts of a first monomer, 25-30 parts of a second monomer, 50-60 parts of a third monomer, 20-30 parts of acetic anhydride and 5-15 parts of triethylamine. The size stability and heat resistance of the film can be remarkably improved, meanwhile, the outstanding transparency of the polyimide film can be guaranteed, and the application of the film in the field of flexible display is met.

The invention discloses a sodium alginate embedded iron-carbon microcapsule material for repairing cadmium and arsenic polluted soil and a preparation method of the sodium alginate embedded iron-carbon microcapsule material, and belongs to the technical field of soil heavy metal pollution repairing materials. The material comprises straw biochar, high-iron steel slag powder, a sulfydryl acetylated chitosan-iron monatomic cluster compound, a boron-doped graphitized carbon coated cobalt ferrite nanosheet, sodium alginate, calcium chloride and sodium carbonate. Wherein the sulfydryl acetylated chitosan is prepared by reacting chitosan with sulfydryl acetic anhydride, dialyzing and drying, and performing solvothermal reaction with ferric nitrate under high pressure. The preparation method comprises the following steps: pyrolyzing and drying the straw biochar, reacting the high-iron steel slag with sulfuric acid, adding the biochar, adjusting the pH value, adding sodium carbonate, mixing to obtain an iron-carbon-based passivation material, mixing with two modified compounds, mixing with a sodium alginate solution, dropwise adding a calcium chloride solution, and stirring and curing. The material can be applied to remediation of cadmium and arsenic polluted soil.

The invention relates to the technical field of polyimide fibers, in particular to a method for preparing polyimide fibers of different color systems based on in-situ coloring, which comprises the following steps: carrying out condensation polymerization on perylene tetracarboxylic dianhydride compounds or perylene diimide, diamine monomers and dianhydride monomers to obtain a polyamide acid solution; adding acetic anhydride and pyridine into the polyamide acid solution for chemical ring-closure reaction to obtain a polyimide solution; and carrying out wet spinning on the obtained polyimide solution to obtain the colored polyimide fiber. The method for preparing the polyimide fibers of different color systems based on in-situ coloring is simple in process and environmentally friendly, and the prepared polyimide fibers of different color systems are high in color fastness and excellent in mechanical property.

The invention relates to the technical field of acetic anhydride content optical detection, in particular to an acetic anhydride content optical detection device and method.The acetic anhydride content optical detection device comprises a detection box, a cleaning seat is fixedly connected into the detection box, a squeezing plate is fixedly connected into the cleaning seat, a scrubbing mechanism is rotatably connected to the squeezing plate, and a wiping ring is arranged in the cleaning seat; the bottom of one side of the detection box is fixedly connected with the exhaust hood in a penetrating manner, the inner wall of the detection box is rotatably connected with the push-pull mechanism, the box cover is arranged above the detection box, and the Fourier transform infrared spectrometer is fixedly arranged on the inner wall of one side of the detection box. The outer wall of the light-transmitting tube type liquid pool is automatically cleaned, fingerprints can be effectively removed, it is ensured that an optical path is not interfered, light rays are prevented from being scattered or absorbed when passing through the light-transmitting tube type liquid pool, and the accuracy, efficiency, repeatability and consistency in the experiment process can be greatly improved.

The invention provides low-dielectric and high-heat-resistance adamantane type maleimide resin as well as a preparation method and application thereof, and belongs to the technical field of synthetic resin for electronic materials. The preparation method comprises the following steps: S1, dissolving an adamantane type amino compound to obtain a solution A; dissolving maleic anhydride to obtain a solution B; s2, dropwise adding the solution A into the solution B; s3, acetic anhydride and a catalyst are added into the solution obtained after the stirring reaction in the step S2, then the temperature is increased to 90-110 DEG C, and a heat preservation reaction is conducted for 4-6 h; and S4, cooling the solution subjected to the heat preservation reaction in the step S3, and then washing and removing the solvent to prepare the low-dielectric and high-heat-resistance adamantane type maleimide resin. The adamantane type maleimide resin provided by the invention can solve the problems of poor solubility and high brittleness of maleimide resin, and meanwhile, the resin is endowed with excellent heat resistance. In addition, the adamantane type maleimide resin can also be used for preparing copper-clad plates with low dielectric constant and low dielectric loss.

The invention discloses a peracetylated polysaccharide derivative mixing accelerator as well as a preparation method and application thereof, and relates to the technical field of polysaccharide derivatives. Alkyl polyglucoside and glycidyl ether are subjected to etherification reaction to obtain polysaccharide derivatives; and adding acetic anhydride and an organic weak base catalyst into the polysaccharide derivative, and carrying out esterification reaction to obtain the peracetylated polysaccharide derivative. The obtained peracetylated polysaccharide derivative can be used for reducing the minimum miscible pressure of CO2 in an offshore oilfield. The polysaccharide derivative provided by the invention is simple in synthesis process, and the molecular activity of the polysaccharide derivative can be regulated and controlled by changing the number of carbon dioxide-philic groups and the length of oleophylic unsaturated hydrocarbon chains, so that the polysaccharide derivative can be used in the CO2 oil displacement process of oilfield exploitation, and the minimum miscible pressure in the CO2 oil displacement process is effectively reduced.

The invention discloses a BTCP-Ac-Eu-MOF double-fluorescence-emission fluorescent probe as well as a preparation method and application thereof, and belongs to the technical field of detection probes. The preparation method comprises the following steps: synthesizing BTCP from salicylic acid and 2-aminothiophenol to obtain a product 1, and reacting the product 1 with acetic anhydride and triethylamine to obtain BTCP-Ac; the preparation method comprises the following steps: mixing europium nitrate hexahydrate and trimesic acid, and performing high-temperature reaction to obtain Eu-MOF powder; and the BTCP-Ac and the Eu-MOF are mixed, such that the BTCP-Ac / Eu-MOF dual-fluorescence emission fluorescent probe is obtained. The europium metal organic framework has a clear structure, ultrahigh porosity and a designable function, the europium metal organic framework is combined with AIE fluorescent molecules to enhance the performance of the europium metal organic framework, and the fluorescence of the europium metal organic framework can be used as a colorimetric reference, so that the function of sensitively, quickly and conveniently indicating the freshness of meat products is realized.

The invention discloses a preparation method of a six-membered azaspiro dihydrobenzofuran compound. According to the method, a C2-alkyne benzofuran derivative is taken as a raw material, metal palladium is taken as a catalyst, and a corresponding product is generated through reaction in an organic solvent at the temperature of 40-120 DEG C under the combined action of a ligand and acetic anhydride. Under the action of palladium, a ligand, a solvent and acetic anhydride, alkyne triple bonds and indole double bonds are subjected to triple addition and bicyclic addition, and rapid construction of a six-membered azaspiro structure dihydrobenzofuran product is achieved. The reaction conditions are mild, the operation is simple and convenient, and the method has the advantages of easily available reaction raw materials, wide substrate applicability, excellent yield and enantioselectivity, easily separated target products and the like.

The invention discloses a method for extracting light-color lignin based on a ternary complex solvent and application of the light-color lignin in sunscreen cream, and belongs to the field of lignin separation and high-value utilization thereof. The method comprises the following specific steps: mixing choline chloride, lactic acid and acetic anhydride to prepare a ternary composite solvent, heating plant fiber raw materials and the ternary composite solvent to react, and extracting the light-color lignin. According to the method disclosed by the invention, the molar ratio of choline chloride to lactic acid to acetic anhydride is 1: 1: (3-5), and the extracted lignin is faint yellow and shows a lighter color compared with other disclosed technologies. And after the prepared light-color lignin is mixed with the sunscreen cream according to the doping amount of 8wt%, the sunscreen index SPF reaches 38 and is close to the requirements of commercial sunscreen cream, and the light-color lignin does not generate a stain phenomenon on the skin when being smeared and used, has certain practical value and effectively expands the application potential of the lignin in the fields of cosmetics, ultraviolet absorbers and the like.

The invention belongs to the technical field of energetic plasticizer preparation, and particularly discloses a method for preparing N-butyl nitroxyethyl nitramine through ionic liquid nitration. The method comprises the following steps: mixing an ionic liquid nitrating agent with butyl ethanolamine to obtain a mixed solution; and mixing the mixed solution with a catalyst and acetic anhydride, reacting, and carrying out post-treatment to obtain the N-butyl nitroxyethyl nitramine. According to the method, the ionic liquid with stable properties is adopted as the nitrating agent, the reaction is mild when the ionic liquid is mixed with the butylethanolamine, violent heat release caused when fuming nitric acid is in contact with the butylethanolamine is effectively avoided, and the ionic liquid precursor can be recycled through simple extraction after the reaction.

The invention provides a method for detecting the hydroxyl value of a polyether material. The method comprises the following steps: (1) constructing a standard quantitative system of a derivatization reagent; (2) fully reacting a to-be-detected polyether material with the excessive derivatization reagent; (3) testing the peak area of the unreacted derivatization reagent by adopting chromatography; (4) comparing with a standard quantitative system of the derivatization reagent, and calculating the content of the unreacted derivatization reagent; and (5) calculating the consumption of the derivatization reagent in the step (2) by using the calculated content of the unreacted derivatization reagent, thereby calculating the hydroxyl value of the polyether material according to the stoichiometric relationship. Wherein the derivatization reagent comprises at least one hydroxyl esterifying agent selected from the following groups: phthalic anhydride, acetic anhydride and benzoyl chloride.

The invention discloses an environment-friendly p-hydroxyacetophenone production process, and particularly relates to the technical field of p-hydroxyacetophenone production, which comprises the following steps: step 1, respectively putting dissolved phenol and acetic anhydride into a synthesis reaction kettle, stirring and heating to 128 DEG C, refluxing for 5 hours at normal pressure, then carrying out heat preservation treatment, and reacting to generate phenyl acetate; 2, cooling phenyl acetate generated by the reaction to 60 DEG C, washing with water, standing for layering, and discharging phenyl acetate to generate a small amount of by-products containing 90% of glacial acetic acid; and 3, pumping the dehydrated phenyl acetate into a reaction kettle by a vacuum pump, gradually adding aluminum trichloride, then adding acidic water for hydrolysis, cooling to 60 DEG C, and discharging to obtain a liquid crude product of p-hydroxyacetophenone and o-hydroxyacetophenone. The environment-friendly performance of implementation is good, conditions needed by the technology are mild, the unstable condition is not prone to occurring in the operation process, and the practical application effect of the method is ideal.

The invention discloses a modified bamboo fiber reinforced polypropylene composite material and a preparation method thereof, and belongs to the field of polypropylene composite materials, the modified bamboo fiber reinforced polypropylene composite material is characterized by comprising the following raw materials by mass: 1-10 parts of modified bamboo fiber, 80-90 parts of polypropylene, and 1-5 parts of a compatilizer. The modified bamboo fiber is prepared by modifying the surface of bamboo fiber by using acetic anhydride as an acetylation reagent and concentrated sulfuric acid and glacial acetic acid as a solvent system. Through acetylation modification of the bamboo fiber, the surface hydrophobic effect of the bamboo fiber is greatly improved, the bamboo fiber adapts to a polypropylene polymer non-polar material, and the interfacial compatibility between the bamboo fiber and polypropylene is improved. Fine fibers can be separated from the modified bamboo fibers through two screw extrusion processes under the shearing action of the screws and are uniformly dispersed in a polypropylene matrix, the fine fibers have the effect of a heterogeneous nucleating agent on polypropylene, the reinforcing effect of the bamboo fibers on the polypropylene is improved, and the composite material is endowed with more excellent mechanical performance and thermal stability.

The invention relates to a method for accurately controlling the acetyl substitution degree of cellulose acetate, which comprises the following steps: adding ground wood pulp into a reaction kettle, adding acetic acid, stirring at room temperature, then adding acetic acid, acetic anhydride and sulfuric acid, mixing, starting acetylation reaction, and gradually raising the system temperature in the reaction process. After reacting for a period of time, stretching a probe of an on-line infrared instrument into the reaction kettle to collect infrared spectrum data on line, adding a magnesium acetate solution, and starting hydrolysis reaction; adding part of the magnesium acetate solution and water after a period of time, maintaining for a period of time, adding part of the magnesium acetate solution after the relative esterification degree monitored by an online infrared instrument reaches a target value, and terminating the hydrolysis reaction; compared with the prior art, the hydrolysis reaction endpoint can be accurately identified on line, esterification degree fluctuation caused by inaccurate reaction time control is avoided, the production efficiency and economic benefits are improved, and the product quality is favorably improved.

The present invention relates to a method for preparing a high-purity peramivir intermediate. The method comprises the following steps: Step 1: adding compound II to a reaction kettle, and dropwise adding a sodium borohydride methanol solution; after the dropwise addition is completed, the reaction is stirred at a controlled temperature; purified water and a sodium nitrite solution are added, and the reaction is stirred to prepare compound (III); Step 2: adding acetic anhydride dropwise to compound (III), and the reaction is stirred at a controlled temperature; Step 3: adding a sodium carbonate aqueous solution, stirring, separating the liquids, collecting the organic phase, concentrating under reduced pressure, adding a solvent, stirring and crystallizing, and centrifuging until no obvious liquid flows out; vacuum drying the filter cake to obtain an off-white crude peramivir acetylate (IV); Step 4: refining to obtain an off-white solid peramivir acetylate (IV). #imgabs0#

The present application relates to a kind of five-ring thiazole indole ketone piperazine amide derivatives and purposes thereof.The derivatives take ethyl cyanoacetate as starting material, generate hydroxylamine compound (A) under the action of sodium nitrite and phosphoric acid;Obtain 2-amino ethyl cyanoacetate (B) by reduction, in turn with acetic anhydride, lawson reagent is reacted, and 5-amino-4-carboxylate thiazole compound (D) is obtained;After bromination by NBS, under the catalysis of phosphorus oxychloride, react with tetrahydropyridine indole ketone, generate 2-bromo-6,7-dihydrothiazolo [5'',4'':4',5'] pyrimido [1',2':1,2] pyrindo [3,4-b] indole-4 (12H) -ketone (F), again under alkaline condition, first with Boc piperazine, then by Boc treatment and obtain compound (H);Finally, react with acyl chloride, and 28 different substitution structures of five-ring thiazole indole ketone piperazine amide compound (I1-I28) are synthesized.The 28 compounds are tested on three kinds of cancer cells, and the results show that: 28 compounds have significant inhibitory activity on Hela cervical cancer cells, HT-29 human colon cancer cells and HGC-27 human gastric cancer cells.

The application discloses a synthesis method of 2'-OMe adenosine, comprising the following steps: S1. dissolving adenosine in DMF, and reacting with a methylation reagent in the presence of a base to obtain a mixture of 2'-OMe adenosine and 3'-OMe adenosine; S2. reacting the mixture of 2'-OMe adenosine and 3'-OMe adenosine with acetic anhydride in a solvent to obtain an acetylated mixture; S3. deacetylating the acetylated mixture under the action of ammonia, and crystallizing to obtain 2'-OMe adenosine; the application uses cheap and easily available raw materials and a safe alkylating reagent, synthesizes 2'-OMe adenosine through a shorter route, avoids column chromatography operation, and provides a new synthesis method of 2'-OMe adenosine which is easy to process.

The present invention belongs to the technical field of enameled wires, and particularly relates to a liquid crystal polymer paint for enameled wires and an enameled wire. The liquid crystal polymer paint for enameled wires comprises a modified LCP and a diluent, the diluent being DMF or DMAC, and the modified LCP is obtained by a condensation polymerization reaction of a monomer, acetic anhydride and a modified monomer, and the modified monomer is glycerol or trimellitic anhydride. The enameled wire comprises a flat copper wire, a primer coated on the surface of the flat copper wire, and a topcoat coated on the surface of the primer, the primer being a liquid crystal polymer paint for enameled wires modified with trimellitic anhydride, and the topcoat being a liquid crystal polymer paint for enameled wires modified with glycerol. The technical solution provided by the present invention, through graft modification of LPC, enables it to be dissolved in a solvent, so that it can be used as a paint, especially as an enameled wire, having the advantages of oil resistance, high temperature resistance, stable electrical properties, etc.

The invention discloses a method for synthesizing a polysubstituted trifluoromethyl olefin compound from gem-difluoroallyl alcohol. The preparation method comprises the following steps: in a nitrogen (N2) atmosphere, sequentially adding a gem-difluoroallyl alcohol (R1R2OHCR3C = CF2) compound, acetic anhydride (Ac2O), a solvent dichloromethane (DCM) and a fluorine source pyridine hydrofluoride (Py.9HF) reagent into a 10mL Schlenk tube to obtain a mixture, stirring the mixture at room temperature (rt) until the reaction is finished, filtering, washing and drying to obtain the compound. A crude product obtained by the reaction is subjected to silica gel column chromatography separation to obtain the high-selectivity polysubstituted trifluoromethyl olefin compound. The preparation method disclosed by the invention can be carried out under mild conditions and is simple and convenient to operate, most of the adopted raw materials are simple and easily available or commercialized reagents, the reaction raw materials are easily available, the yield of the target product is high, the functional group compatibility of the product is good, and the application range of a substrate is relatively wide; the obtained polysubstituted trifluoromethyl olefin compound contains a plurality of functional groups such as trifluoromethyl, olefin and the like. The method provides a more efficient and safer new strategy for synthesizing the polysubstituted trifluoromethyl olefin under mild conditions, particularly, metal participation is avoided, a new opportunity is provided for green medicine synthesis, and the method is predicted to have wide application prospects in the fields of medicine research and development, natural product derivative synthesis, life science and the like.

The invention discloses a method for preparing methyltriacetoxysilane from acetic anhydride-containing acetyl chloride distillation tailings, and relates to the technical field of organic silicon synthesis, the method comprises the following steps: adding methyl trichlorosilane and acetic anhydride-containing acetyl chloride distillation tailings into a reaction kettle, stirring and heating; after a total reflux condition is reached, maintaining total reflux for a period of time, and then starting to collect acetyl chloride; continuously heating until the collection of acetyl chloride is completed, stopping heating, and when the temperature of the kettle is reduced to room temperature, heating again and starting vacuum negative pressure; when the kettle temperature reaches a set value, stopping heating, stopping stirring, and closing vacuum negative pressure; and after the kettle temperature is reduced to room temperature, adding pretreated activated carbon, carrying out decoloration reaction, and carrying out suction filtration after the reaction is completed, thereby obtaining the product. According to the method, a large amount of acetic anhydride in the acetyl chloride distillation tailings is used as a raw material and directly reacts with methyl trichlorosilane to prepare methyltriacetoxysilane, and the quality of the obtained product is remarkably higher than that of a product prepared by a normal process.

The application discloses a synthesis method of afugan, which comprises the following steps: 1-[3-chloro-5-(trifluoromethyl)phenyl]-2,2,2-trifluoroacetone and 4-acetylnaphthalene carboxylic acid are added into a solvent, a base is added, DMAP is added after complete reaction at 50-80 DEG C, acetic anhydride is added dropwise, tetrabutylammonium bromide is added after complete reaction, and an aqueous solution of sodium hydroxide and hydroxylamine hydrochloride is added, and reaction is carried out at 0-5 DEG C, so that an intermediate is obtained; the intermediate is reacted with acyl chloride under the action of DMF and dichloromethane, so that 4-(5-(3-chloro-5-(trifluoromethyl)phenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazole-3-yl)-1-naphthalene carboxylic chloride is prepared; 2-amino-N-(2,2,2-trifluoroethyl)acetamide hydrochloride and a dichloromethane solution of a base are added dropwise, and reaction is carried out at 0-5 DEG C, so that afugan is obtained. The method has a short route, high yield and suitability for large-scale industrial production.

The invention relates to the technical field of chemical engineering, and discloses a method for improving the chromaticity and purity of acetic anhydride based on a reflux ratio, and the method comprises the following steps: optimizing an evaporation tower, an acetic acid rectifying tower and an acetic anhydride rectifying tower, and installing an online detection instrument and an automatic control valve to construct an intelligent rectification control system; evaporating the crude acetic anhydride by using the optimized evaporation tower to obtain crude acetic anhydride steam; feeding the crude acetic anhydride steam into an acetic acid rectifying tower, calculating an initial reflux ratio, inputting the initial reflux ratio into a control system, and starting a reflux system to preliminarily remove acetic acid; monitoring the acetic acid content through an online gas chromatograph, and finely adjusting the reflux ratio until the reflux ratio reaches the standard when the measured acetic acid content is higher than a target value; feeding the crude acetic anhydride reaching the standard into an acetic anhydride rectifying tower, calculating an initial reflux ratio, inputting the initial reflux ratio into a control system, and starting to obtain an intermediate product; monitoring chromaticity and purity through an on-line platinum-cobalt colorimeter and an on-line gas chromatograph, and updating the reflux ratio to be qualified according to a bivariate adjustment formula; and finally, carrying out all-item detection on a finished product, and locking reflux ratio parameters after confirming that the finished product is qualified.

The invention discloses a preparation method of a dipicolinic acid anhydride solution, which comprises the following steps: 1, adding acetic anhydride into a reaction kettle, heating, adding dipicolinic acid, mixing, and further heating for reaction; 2, after the reaction is finished, acetic anhydride and acetic acid are recycled in a distillation mode; and 3, the reaction liquid without acetic anhydride and acetic acid is subjected to vacuum rectification, the obtained fraction flows into a receiving kettle in a gaseous state during rectification, the receiving kettle is filled with a solvent capable of dissolving dipicolinic acid anhydride, the mass of the distilled material is determined through a weighing method, and the mass fraction of the product in the solution is 10-15%. The method has the advantages that the process route is simple, the steps are few, the acetic anhydride is convenient and environment-friendly to reuse, the production cost is effectively reduced, and the product purity is high and can reach 99% or above. And the solution is low in water content and more convenient to use, and meets the requirements of additives of lithium ion battery electrolytes.

The invention relates to the technical field of cholesterol preparation, and discloses a preparation method of plant-derived cholesterol, which comprises the following steps: 1) heating and dissolving phytosterol with n-amyl alcohol, adding stigmasterol until saturation, cooling and crystallizing, and then carrying out solid-liquid separation to obtain a stigmasterol crude product; 2) heating and dissolving the stigmasterol crude product with absolute ethyl alcohol, adding pyridine, and continuously dropwise adding acetic anhydride for reaction; after the reaction is completed, adding deionized water for mixing, extracting with n-hexane for multiple times, separating an upper-layer oil phase, and concentrating and drying the oil phase to obtain a white solid; 3, the white solid is subjected to oxidation reduction, witting reaction and hydrogenation reaction, and cholesterol is obtained.The method has the advantages that compared with the prior art that the plant source cholesterol is directly prepared from the raw material phytosterol, the process is simplified, and meanwhile the product yield can be increased.

To provide a method for producing a trimellitic anhydride ester satisfying high yield, high purity and low chlorine content required for an electronic material by a simple operation.SOLUTION: The method for producing a trimellitic anhydride ester includes a step A of reacting a trimellitic anhydride halide and a specific alkanediol to obtain a crude trimellitic ester, and a step B of purifying the crude trimellitic ester, wherein the step B includes a step B1 of mixing a poor solvent having an octanol / water partition coefficient of -2.0 or more and 0.0 or less and a boiling point of 40°C or more and 120°C or less with the crude trimellitic ester to reprecipitate the crude trimellitic ester, and a step B2 of heating the mixed liquid containing at least the crude trimellitic ester after the reprecipitation and acetic anhydride, and recrystallizing the trimellitic ester.SELECTED DRAWING: None

The utility model discloses a production device of 3-acetamino phthalic acid, and belongs to the technical field of chemical production devices. The device comprises an acylation reaction device, an acidification device and a solid-liquid filtering device. The acylation reaction device comprises an acylation reaction kettle with a stirring device, an acetic anhydride high-position metering tank with a first rotor flow meter, a solid feeding hole and a first conveying pump; the acidification device comprises an acidification reaction kettle with a stirring device, a hydrochloric acid high-position metering tank with a second rotor flow meter, an online pH meter and a second delivery pump; and the solid-liquid filtering device comprises solid-liquid separation equipment, a filtrate receiving tank and a product collecting tank. All the devices of the device are connected through pipelines and stop valves. According to the utility model, the dosage of hydrochloric acid is reduced by adjusting the dosage of acetic anhydride and controlling the acidification pH value, so that the production cost is reduced, and the quality and yield of the product 3-acetamino phthalic acid are improved.

This invention provides an ethyl-containing alkoxy-terminated organosilicon polymer, its preparation method, and its applications. The preparation method includes: S1, mixing methylvinylcyclotetrasiloxane, a solvent, and a first catalyst, introducing hydrogen gas, and reacting at 50-70°C until the methylvinylcyclotetrasiloxane content is no higher than 5%, filtering to remove impurities and obtain the product; S2, under nitrogen protection, ring-opening the product obtained in step S1 with acetic anhydride in the presence of a ring-opening catalyst, neutralizing and hydrolyzing, removing impurities, and obtaining the product; S3, under nitrogen protection, reacting the product of step S2 with hexamethyldisilazane at 40-50°C for 1-3 hours, adding N,N-diethylamino-trialkoxysilane, and reacting at 50-60°C for 1-3 hours. The polymer obtained by this invention, as a thermally conductive powder treatment agent, can effectively improve the dispersion performance of powders and enhance the heat resistance of products without reducing their tensile strength.

The present invention provides a method for preparing the active pharmaceutical ingredient of fenfluramine. Aspects of the present invention include (a) hydrolyzing a 2-(3-(trifluoromethyl)phenyl)acetonitrile composition to produce a 2-(3-(trifluoromethyl)phenyl)acetic acid composition; (b) reacting the 2-(3-(trifluoromethyl)phenyl)acetic acid composition with acetic anhydride and a catalyst to prepare a 1-(3-(trifluoromethyl)phenyl)propan-2-one composition; and (c) reducing and aminating the 1-(3-(trifluoromethyl)phenyl)propan-2-one composition with a borohydride reducing agent and ethylamine to produce a fenfluramine composition. The present invention also provides a composition and a pharmaceutical ingredient comprising a pharmaceutically acceptable salt of fenfluramine prepared according to the method and having less than a total of 0.2% by weight of trifluoromethyl regioisomers.

The invention discloses a flexible glass cutting fluid and a preparation method thereof, and the preparation method comprises the following steps: S1, adding cellobiose into DMF, then adding chloroacetic anhydride and pyridine, and carrying out a stirring reaction to obtain an intermediate; s2, adding the intermediate into DMF (Dimethyl Formamide), and then carrying out constant-temperature reaction on glycerol monocaprylate, 2-(2-hydroxyphenyl) benzothiazole and triethylamine to obtain a modifier; s3, uniformly mixing a modifier, sodium dioctyl sulfosuccinate and a polyoxyethylene polyoxypropylene block copolymer, so as to obtain a composite surfactant; s4, adding the composite surfactant, the propylene glycol, the defoaming agent, the sterilizing agent and the triethanolamine into the water, and uniformly stirring to obtain the cleaning agent. According to the prepared cutting fluid, the protection effect on a flexible glass base material and a surface functional layer of the flexible glass base material is remarkably improved while the excellent wettability is kept, microcrack generation and surface damage in the cutting process are reduced, and the cutting fluid is particularly suitable for precise glass processing of flexible display devices.

The invention relates to a battery and electric equipment. The battery comprises a shell, a battery cell assembly and electrolyte, wherein the shell is provided with an accommodating cavity; the battery cell assembly is positioned in the accommodating cavity; the battery cell assembly comprises a positive pole piece, a diaphragm and a negative pole piece which are arranged in a laminated manner, the positive pole piece comprises a positive active material, the positive active material comprises an inner core and a carbon coating layer, the outer periphery of the inner core is coated with the carbon coating layer, the inner core comprises lithium iron phosphate, and the carbon coating layer is provided with a C-O bond; the electrolyte is used for infiltrating at least part of the battery cell assembly, the electrolyte comprises a first additive, and the first additive comprises thiohydroxyacetic anhydride; wherein the mass ratio of the first additive in the electrolyte is a, the quantity ratio of the C-O bonds in the carbon-containing chemical bonds in the carbon coating layer is b, and the battery meets the relational expression: 0.25 < = 100a / b < = 20.