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Tin is a chemical element with the symbol Sn (from Latin: stannum) and atomic number 50. Tin is a silvery metal that characteristically has a faint yellow hue. Tin, like indium, is soft enough to be cut without much force. When a bar of tin is bent, the so-called tin cry can be heard as a result of sliding tin crystals reforming; this trait is shared by indium, cadmium, and frozen mercury. Pure tin after solidifying keeps a mirror-like appearance similar to most metals. However, in most tin alloys (such as pewter) the metal solidifies with a dull gray color. Tin is a post-transition metal in group 14 of the periodic table of elements. It is obtained chiefly from the mineral cassiterite, which contains stannic oxide, SnO₂. Tin shows a chemical similarity to both of its neighbors in group 14, germanium and lead, and has two main oxidation states, +2 and the slightly more stable +4. Tin is the 49th most abundant element on Earth and has, with 10 stable isotopes, the largest number of stable isotopes in the periodic table, thanks to its magic number of protons. It has two main allotropes: at room temperature, the stable allotrope is β-tin, a silvery-white, malleable metal, but at low temperatures, it transforms into the less dense grey α-tin, which has the diamond cubic structure. Metallic tin does not easily oxidize in air.
Method, system and equipment for detecting oxygen content of copper alloy melt
InactiveCN120161094AThermometers using electric/magnetic elementsUsing electrical meansOxygen contentCopper alloy
The invention relates to the technical field of tin-containing copper alloy manufacturing, in particular to a method, system and equipment for detecting the oxygen content of copper alloy melts.The method comprises the steps that resistivity data of the copper alloy melts.The temperature data of the copper alloy melts.The resistivity data of the copper alloy melts.The temperature data of the copper alloy melts.The resistivity data of the copper alloy meltsare acquired in real time; the resistivity data are corrected based on the temperature data, and standardized resistivity irrelevant to the temperature is obtained; a correlation model of the resistivity and the oxygen content is established according to the linear influence relation of oxygen impurities in the copper alloy melt on the resistivity, a real-time oxygen content value is output based on the standardized resistivity, and an oxygen content fluctuation trend is generated; and according to the real-time oxygen content value and the oxygen content fluctuation trend, the oxygen content tolerance threshold value of the copper alloy melt is dynamically adjusted based on the oxygen sensitivity requirements of different alloying stages. By means of the method, the problems that in a traditional oxygen content detection method, due to the fact that temperature distribution is uneven, alloy element interaction and solidification behaviors are not systematically modeled, the detection precision is low, and microstructure control fails are effectively solved.
Owner:CHANGZHOU TONGTAI HIGH CONDUCTIVITY NEW MATERIALS CO LTD
Corrosion-resistant nickel-based alloy welding wire and production process thereof
The invention belongs to the technical field of nickel-based alloy welding wires, and discloses a corrosion-resistant nickel-based alloy welding wire and a production process thereof, and the corrosion-resistant nickel-based alloy welding wire comprises the following components in percentage by mass: 50-65% of nickel, 16-24% of chromium, 8-10% of molybdenum, 3.5-5.5% of niobium and tantalum, 3-4.5% of copper, 3-4% of tungsten, 0.5-1.0% of tin, 0.1-0.3% of rare earth element, 0.1-0.5% of grain boundary optimizer, 2-5% of nano reinforced phase and the balance of Fe and other inevitable impurities. Through multi-element alloying design, nano reinforced phase compounding and gradient coating synergistic effect, comprehensive improvement of corrosion resistance, high-temperature mechanical property and welding manufacturability is achieved; a welding wire base body is based on nickel, a compact and self-repairing gradient oxidation film is formed by accurately regulating and controlling the atomic proportion of chromium, molybdenum and tungsten, and the chloride ion permeation resistance and the high-temperature oxidation resistance are remarkably improved; therefore, the welding wire has excellent corrosion resistance, high-temperature strength and welding adaptability.
Owner:SHANDONG TENGDA SPECIAL STEEL WIRE TECH CO LTD
Method and device for preparing Ti-TiN core-shell powder
ActiveCN120190345ATransportation and packagingMetal-working apparatusElectrostatic separationNitrogen gas
The invention relates to a method and device for preparing Ti-TiN core-shell powder, and the method comprises the steps that in an atomizing chamber, mixed gas is blown to a molten pool on the surface of an electrode bar, liquid drops are subjected to primary refining and primary coating nitrogen increasing treatment, the mixed gas comprises argon and nitrogen, and the volume content of the nitrogen does not exceed 10%; high-temperature pure nitrogen is blown to the flying liquid drops, so that secondary refining and secondary coating nitrogen increasing treatment are carried out, and the temperature of the high-temperature pure nitrogen is 1000-1500 DEG C; the powder which is not fully coated and the powder which is fully coated are separated through an electrostatic separation device; and the powder which is not fully coated is subjected to third-time coating nitrogen increasing treatment, so that the Ti-TiN core-shell structure powder is obtained. The prepared powder is core-shell powder with large thickness and small fineness, the yield is high, the shell layer structure is uniform, the sphericity degree of the powder is high, and the preparation efficiency is high.
Owner:XIAN SAILONG AM TECH CO LTD
Uniformly-distributed saw blade and preparation method thereof
The invention discloses a uniformly distributed saw blade and a preparation method thereof, and relates to the technical field of saw blades. The evenly-distributed saw blade comprises a base body and tool bits, a plurality of tool bits are annularly welded to the periphery of the base body, a plurality of diamonds are distributed on the tool bits through a net plate adsorption evenly-distributed technology, the tool bits are formed by sintering matrix powder, and the matrix powder comprises, by weight, 30%-40% of copper powder, 20%-30% of copper-tin diffusion powder, 10%-20% of carbonyl iron powder and 5%-10% of nickel powder. And 10%-15% of tin powder. According to the saw blade preparation process, a screen adsorption uniform distribution process and saw blade uniform distribution design are adopted, it is guaranteed that when the first diamond is consumed by 1 / 5-2 / 3, the second diamond can be exposed, it is guaranteed that edges are exposed when the diamonds are consumed to any height, and the cutting continuity of the diamonds is improved. The diamond of 60-100 meshes is used in the saw blade, a finer cutting face can be formed in the cutting process, and the saw blade is suitable for machining tasks with the high requirement for cutting precision. The 60-100-mesh diamond particles are suitable for cutting hard and brittle materials, and edge breakage and cracks of the materials can be reduced in the cutting process.
Owner:QUANZHOU ZHONGZHI NEW MATERIAL TECH
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.15% ≤ Manganese ≤ 0.7% 3% ≤ Silicon ≤ 3.6% 0.7% ≤ Aluminum ≤ 1.3 % Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0% ≤ Nickel ≤ 1% 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 30 to 40% when calculated in accordance with Bertotti method.
Owner:ARCELORMITTAL SA
Tin precursors for deposition of EUV dry resist
PendingUS20250346767A1Group 4/14 element organic compoundsPhotosensitive material processingExtreme ultravioletPolymer chemistry
The present disclosure relates to precursor compositions for forming irradiation sensitive films. In particular, the disclosure is directed to use of metal-containing precursors having haloaliphatic or unsaturated substituents, or other reactive moieties which advantageously react in the presence of extreme ultraviolet exposure to form resist films having increased etch resistance and / or reduced shrinkage upon processing. Alternatively, the use of metal-containing precursors having haloaliphatic or unsaturated substituents, or other reactive moieties for patterning structures having carbon-containing underlayers may advantageously react with the underlayer to increase adhesion of the resist film to the underlayer.
Owner:LAM RES CORP
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001 % ≤ Carbon ≤ 0.007 % 0.15% ≤ Manganese ≤ 0.2% 3% ≤ Silicon ≤ 3.6% 0.7% ≤ Aluminum ≤ 1.3 % Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% with 3.85% ≤ Si+AI+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1 % 0% ≤ Titanium ≤ 0.1 % 0% ≤ Vanadium ≤ 0.1 % 0% ≤ Chromium ≤ 1 % 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten ≤ 0.1 % 0% ≤ Cobalt ≤ 1 % 0% ≤ Arsenic ≤ 0.05% 0.001 % ≤ Calcium ≤ 0.01 % 0% ≤ Copper ≤ 1 % 0% ≤ Nickel ≤ 1 % 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, of 35 to 55% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.635T to 1.670T.
Owner:ARCELORMITTAL SA
Manufacturing method of 925 silver jewelry
The invention discloses a manufacturing method of 925 silver jewelry, which comprises the following steps: S1, preparing alloy components, S2, designing a cast tree structure, S3, casting, and S4, densifying a casting, the alloy components comprise 92.5-93.0% of silver, 1.0-3.0% of platinum, 0.05-0.5% of copper, 1.5-3.5% of zinc, 1.5-3.5% of indium, 0.03-0.3% of tin, 0.05-0.5% of germanium, 0.03-0.3% of rare earth, and 0.003-0.02% of boron. According to the manufacturing method, alloy components are optimized, the casting performance of the alloy components is improved, the casting process is optimized, the feeding capacity of molten metal is improved, shrinkage porosity and air holes are reduced, the initial density of the casting is improved, and subsequent composite treatment is carried out, so that the density from the surface to the shallow surface of the casting is further improved, grains are refined, and the surface roughness is further reduced; and the requirement of high brightness of the jewelry surface is met.
Owner:GUANGZHOU PANYU POLYTECHNIC
Method for preparing tin dioxide powder
The invention relates to the technical field of synthesis and preparation of nano materials, in particular to a method for preparing tin dioxide powder, which comprises the following steps: S1, preparing a 0.1-5 mol / L tin salt solution, adding a compound additive into the tin salt solution, and carrying out ball milling treatment after ultrasonic dispersion to obtain a pretreated tin salt solution; s2, freezing and freezing the pretreated tin salt solution in an ultralow-temperature environment to obtain a frozen sample; s3, transferring the frozen sample into a vacuum freeze dryer for dehydration treatment to obtain solid powder; and S4, carrying out high-temperature calcination on the solid powder to obtain tin dioxide powder. Zero sewage discharge is achieved in the preparation process, the problem of sewage discharge and treatment of traditional liquid-phase powder preparation is solved, meanwhile, the phenomenon of sintering agglomeration accompanied by traditional solid-phase calcination can be avoided, high-quality superfine tin dioxide powder preparation is achieved, the method is simple and safe in process, and industrial large-scale production and preparation are easy to achieve.
Owner:HUNAN AITIO NEW MATERIAL CO LTD
A double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a double cold rolled non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.2% ≤ Manganese ≤ 0.24% 3.1% ≤ Silicon ≤ 3.5% 0.8% ≤ Aluminum ≤ 1.1% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0.001% ≤ Nickel ≤ 0.01 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less from 30% to 35% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.645T to 1.660T.
Owner:ARCELORMITTAL SA
A double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a double cold rolled non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.1% ≤ Manganese ≤ 0.2% 3.1% ≤ Silicon ≤ 3.6% 0.8% ≤ Aluminum ≤ 1.1% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0.001% ≤ Nickel ≤ 0.01 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, is from 35% to 45% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.64T to 1.66T.
Owner:ARCELORMITTAL SA
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001 % ≤ Carbon ≤ 0.007 % 0.09% ≤ Manganese ≤ 0.15% 2.5% ≤ Silicon ≤ 3% 0.1 % ≤ Aluminum ≤ 0.5 % Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1 % 0% ≤ Titanium ≤ 0.1 % 0% ≤ Vanadium ≤ 0.1 % 0% ≤ Chromium ≤ 1 % 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1 % 0% ≤ Cobalt ≤ 1 % 0% ≤ Arsenic ≤ 0.05% 0.001 % ≤ Calcium ≤ 0.01 % 0% ≤ Copper ≤ 1 % 0% ≤ Nickel ≤ 1 % 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 35% to 45% when calculated in accordance of Bertotti method.
Owner:ARCELORMITTAL SA
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.15% ≤ Manganese ≤ 0.25% 2.9% ≤ Silicon ≤ 3.4% 0.7% ≤ Aluminum ≤ 1.3 % 0.05% ≤ Nickel ≤ 1% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less than 35% when calculated in accordance of Bertotti method.
Owner:ARCELORMITTAL SA
Preparation method of tin or tin alloy coated copper powder and low-temperature conductive paste
The present invention provides a method for preparing tin or tin alloy-coated copper powder and a low-temperature conductive paste, wherein the method comprises the following steps: S10, pretreating the surface of the copper powder to remove oxides and impurities on the copper powder surface; S20, placing the pretreated copper powder in an electroplating solution containing an organic phosphine compound additive; electroplating the copper powder using tin metal or tin alloy as an anode and copper powder as a cathode, wherein the copper powder is dispersed during the electroplating process; S30, after the electroplating is completed, filtering, washing, and drying to obtain the tin or tin alloy-coated copper powder. The addition of the organic phosphine compound in the present invention greatly improves the compactness of the tin or tin alloy coating formed on the surface of the copper powder, thereby making the prepared tin-coated copper powder or tin alloy-coated copper powder have the advantage of better oxidation resistance.
Owner:JINGLAN ADVANCED MATERIAL CO LTD
A double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a double cold rolled non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.1% ≤ Manganese ≤ 0.3% 3.1% ≤ Silicon ≤ 3.8% 0.6% ≤ Aluminum ≤ 0.8% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0.001% ≤ Nickel ≤ 0.01 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, of 40 to 50% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.66T to 1.7T.
Owner:ARCELORMITTAL SA
Ruthenium and samarium double monatomic doped three-dimensional titanium-based tin antimony nickel electrode and preparation method and application thereof
The invention discloses a ruthenium and samarium double monatomic doped three-dimensional titanium-based tin antimony nickel electrode and a preparation method and application thereof. The preparation method of the electrode comprises the following steps: (1) pretreating the titanium felt; (2) preparing a sol impregnation liquid; (3) sol coating and drying: dipping the pretreated titanium felt in the prepared sol dipping liquid, fully adsorbing and then drying to form a uniform precursor layer; and (4) roasting treatment is conducted, specifically, the dried titanium felt is placed in a muffle furnace to be roasted, and then the steps of dipping, drying and roasting are repeated till the final ruthenium and samarium double monatomic doped three-dimensional titanium-based tin-antimony-nickel electrode is obtained. In the prepared electrocatalyst, ruthenium and samarium are doped into a tin-antimony-nickel electrode in a monatomic form, the utilization efficiency of ruthenium and samarium atoms is improved, and the electrode is endowed with excellent electrocatalytic activity. The unique three-dimensional structure and double-monatomic doping significantly enhance the electron transfer rate and the reaction kinetic characteristics, so that the electrode shows excellent stability and efficient hypochlorous acid generation ability.
Owner:ZHEJIANG UNIV OF TECH
Low-cost high-stability Ti / IrO2-SnO2-SbO2 gradient active coating anode and preparation process
PendingCN120945431ARuthenium/rhodium/palladium/osmium/iridium/platinum oxides/hydroxidesAntimony oxides/hydroxides/oxyacidsIridiumPhysical chemistry
The invention discloses a Ti / IrO2-SnO2-SbO2 gradient active coating anode with low cost and high stability and a preparation process of the Ti / IrO2-SnO2-SbO2 gradient active coating anode. The gradient active coating is characterized in that the gradient active coating is composed of 3-5 layers, the total thickness is 5-15 microns, the thickness of each layer is 1-5 microns, the molar percentage content of iridium in a bottom layer is 0-5%, the sum of the molar percentage content of tin and antimony is 95-100%, the molar percentage content of iridium in a surface layer is 10-20%, the sum of the molar percentage content of tin and antimony is 80-90%, and the thickness of each layer is 1-5 microns. The molar percentage content of iridium from the bottom layer to the surface layer is sequentially increased from 2% to 10%, the molar percentage content of tin and antimony is sequentially reduced from 2% to 10%, and the total iridium loading amount in the gradient active coating is 0.05-0.2 mg / cm < 2 >. The preparation method comprises the three steps of titanium substrate pretreatment, precursor salt alcohol solution preparation and gradient active coating preparation. By adopting a gradient coating mode, the thermal stress between the coating and the titanium substrate in the preparation process is remarkably reduced, the consumption of noble metal is reduced, the oxygen evolution activity of the anode is improved, and the service life of the anode is prolonged. The method is simple to operate and low in cost, and has remarkable industrialization advantages.
Owner:DALIAN UNIV OF TECH +1
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.17% ≤ Manganese ≤ 0.4% 3% ≤ Silicon ≤ 3.6% 0.7% ≤ Aluminum ≤ 1.3 % Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0% ≤ Nickel ≤ 1% 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less than 25% when calculated in accordance of Bertotti method.
Owner:ARCELORMITTAL SA
Hot-dip galvanized low-alloy high-strength steel plate and production method thereof
InactiveCN120591661AHot-dipping/immersion processesManufacturing convertersAustenite grainChemical composition
The invention relates to the technical field of metallurgy, in particular to a hot galvanizing low-alloy high-strength steel plate which comprises the following chemical components in percentage by mass: 0.06%-0.08% of C, 0.20%-0.25% of Si, 1.20%-1.35% of Mn, less than or equal to 0.015% of P, less than or equal to 0.005% of S, 0.020%-0.060% of Alt, 0.035%-0.050% of Nb, 0.010%-0.020% of Ti, less than or equal to 0.0050% of O, less than or equal to 0.0060% of N and the balance of Fe and inevitable impurities. The contents of C, Si and Mn in the chemical components are controlled, the welding performance of the hot-dip galvanizing low-alloy high-strength steel and the surface quality of a finished product are considered, Nb microalloying is mainly adopted, a proper amount of microalloy element Ti is added to form TiN, austenite grain coarsening is limited in the slab heating and heat preservation process, and fine and dispersed precipitated phases are finally obtained in combination with process control; the hot-dip galvanized low-alloy high-strength steel finished product is good in structure form and excellent in comprehensive performance.
Owner:BENGANG STEEL PLATES CO LTD
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.21% ≤ Manganese ≤ 0.7% 3% ≤ Silicon ≤ 3.6% 0.7% ≤ Aluminum ≤ 1.3 % Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0% ≤ Nickel ≤ 1% 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 35% to 45% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.63T to 1.66T.
Owner:ARCELORMITTAL SA
Tin-based alloy preformed soldering lug and preparation method thereof
The invention discloses a tin-based alloy preformed soldering lug and a preparation method thereof.The preparation method comprises the following steps that a copper fiber reinforced framework with gradient density distribution is prepared, the copper fiber reinforced framework comprises a high-density area and a low-density area, and hollowed-out gaps are formed through a weaving technology; tin-based slurry with different components and functions is prepared from outer-layer slurry with tin-antimony-copper-nickel as a main body, middle-layer slurry with tin-antimony-copper as a base body and inner-layer slurry with tin-antimony-copper rare earth as a base body, the three kinds of tin-based slurry are sequentially filled into preset areas of hollow-out gaps of a reinforced framework, and a gradient structure material is formed; the gradient structure material is subjected to press-fit forming and post-treatment, and a preformed soldering lug is obtained; a framework is firstly built, then materials are filled, and copper fibers in the soldering lugs provide good support and heat conduction channels, so that a gradient transition structure with continuous change of components and performance is realized, and the integrity, the impact resistance and the bonding strength of the materials are greatly enhanced.
Owner:SHENZHEN XINGHONGTAI TIN
Non-ferrous metal solder for low-temperature brazing and application
The invention relates to the field of solder materials, and provides a non-ferrous metal solder for low-temperature brazing and application, the solder is composed of carbon-coated copper nanorods, tin-bismuth alloy-coated silver nanoparticles, 2-mercaptobenzimidazole, rosin resin, an organic active agent, a dispersing agent, ionic liquid, hydroxyethyl cellulose, indium nitrate and citric acid. The silver particles are of a core-shell structure and are coated with tin-bismuth alloy layers, and continuous carbon layers are formed on the surfaces of the copper nanorods, so that the conductivity and the interface stability of the solder are effectively improved. The non-ferrous metal solder with excellent conductivity, low melting point and good wettability is prepared through step-by-step mixing, hot press molding and low-temperature heat treatment processes, and is suitable for electronic device packaging, power device connection and flexible circuit interconnection, and the defects of existing solder in the aspects of low-temperature welding and high conductivity are overcome.
Owner:HUNAN YISIDI TECH CO LTD
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 %, 0.15% ≤ Manganese ≤ 0.25%, 3.2% ≤ Silicon ≤ 3.8%, 0.7% ≤ Aluminum ≤ 1.3 %, 0 % ≤ Phosphorus ≤ 0.15 %, 0 % ≤ Sulfur ≤ 0.006 %, 0 % ≤ Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1%, 0% ≤ Titanium ≤ 0.1%, 0% ≤ Vanadium ≤ 0.1%, 0% ≤ Chromium ≤ 1%, 0% ≤ Molybdenum ≤ 0.5%, 0% ≤ Tungsten≤ 0.1%, 0% ≤ Cobalt ≤ 1%, 0% ≤ Arsenic ≤ 0.05%, 0.001% ≤ Calcium ≤ 0.01%, 0% ≤ Copper ≤ 1%,0.001% ≤ Nickel ≤ 0.01, 0 % ≤ Boron ≤ 0.05%, 0 % ≤ Lead ≤ 0.2%, 0% ≤ Tin≤ 0.2%, 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current loss in total iron loss less than 33 % when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.630T to 1.65T.
Owner:ARCELORMITTAL SA
A double cold rolled non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a double cold rolled non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.15% ≤ Manganese ≤ 0.3% 3.2% ≤ Silicon ≤ 3.8% 0.8% ≤ Aluminum ≤ 1.1% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0.001% ≤ Nickel ≤ 0.01 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤ Tin≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less than 30% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.66T to 1.69T.
Owner:ARCELORMITTAL SA
Low-strength high-formability austenitic stainless steel and manufacturing method thereof
According to the low-strength high-formability austenitic stainless steel and the manufacturing method thereof, C + N is controlled to be smaller than or equal to 0.035%, the manganese content is controlled to be within 1.5%, the tin content is limited to be 0.01%-0.30%, the copper content is limited to be 2.4%-4.5%, and the tin-copper ratio is that (Sn / Cu) * 1000 is larger than or equal to 5 and smaller than or equal to 50, so that it is guaranteed that tin exerts the beneficial effects such as the corrosion resistance is improved, and the harm of tin segregation can be controlled to be at the low level; according to the finally obtained austenitic stainless steel, the yield strength is smaller than or equal to 160 Mpa, the tensile strength is smaller than or equal to 500 Mpa, the ductility is larger than or equal to 55%, the grain size grade is 6-8, edge cracks cannot occur during hot rolling, the martensite content of a cup drawing deformation part is 0.05% or below during large deformation machining, in other words, the austenite phase is still stable under the complex deformation condition, deformation cracks are avoided, and the service life of the austenitic stainless steel is prolonged. The comprehensive effects of high corrosion resistance, low strength and high forming machinability of the material are achieved.
Owner:BAOSTEEL DESHENG STAINLESS STEEL
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 %, 0.15% ≤ Manganese ≤ 0.25%, 2.9% ≤ Silicon ≤ 3.4%, 0.8% ≤ Aluminum ≤ 1.1 %, 0 % ≤ Phosphorus ≤ 0.15 %, 0 % ≤ Sulfur ≤ 0.006 %, 0 % ≤ Nitrogen ≤ 0.09%,with 3.85% ≤ Si+Al+Mn ≤ 5.5% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1%, 0% ≤ Titanium ≤ 0.1%, 0% ≤ Vanadium ≤ 0.1%, 0% ≤ Chromium ≤ 1%, 0% ≤ Molybdenum ≤ 0.5%, 0% ≤ Tungsten≤ 0.1%, 0% ≤ Cobalt ≤ 1%, 0% ≤ Arsenic ≤ 0.05%, 0.001% ≤ Calcium ≤ 0.01%, 0% ≤ Copper ≤ 1%, 0% ≤ Nickel ≤ 1%, 0 % ≤ Boron ≤ 0.05%, 0 % ≤ Lead ≤ 0.2%, 0% ≤ Tin≤ 0.2%, 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current loss in total iron loss less than 25% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.625T to 1.690T.
Owner:ARCELORMITTAL SA
A non-oriented electrical steel and a method of manufacturing non-oriented electrical steel thereof
The invention deals with a non-oriented electrical steel sheet having a composition comprising of the following elements, expressed in percentage by weight: 0.0001% ≤ Carbon ≤ 0.007 % 0.30% ≤ Manganese ≤ 0.7% 3% ≤ Silicon ≤ 3.6% 0.4% ≤ Aluminum ≤ 0.8 % 0.05% ≤ Tin≤ 0.15% Phosphorus ≤ 0.15 % Sulfur ≤ 0.006% Nitrogen ≤ 0.09% and can contain one or more of the following optional elements 0% ≤ Niobium ≤ 0.1% 0% ≤ Titanium ≤ 0.1% 0% ≤ Vanadium ≤ 0.1% 0% ≤ Chromium ≤ 1% 0% ≤ Molybdenum ≤ 0.5% 0% ≤ Tungsten≤ 0.1% 0% ≤ Cobalt ≤ 1% 0% ≤ Arsenic ≤ 0.05% 0.001% ≤ Calcium ≤ 0.01% 0% ≤ Copper ≤ 1% 0% ≤ Nickel ≤ 1% 0 % ≤ Boron ≤ 0.05% 0 % ≤ Lead ≤ 0.2% 0% ≤Antimony ≤ 0.2% the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of said steel sheet being made of ferrite and comprising in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 25% to 35% when calculated in accordance of Bertotti method.
Owner:ARCELORMITTAL SA
Tin-copper co-doped porous carbon as well as preparation method and application thereof
PendingCN120174411ATransportation and packagingMetal-working apparatusMelamine phosphatePorous carbon
The invention belongs to the technical field of carbon materials, and provides tin-copper co-doped porous carbon and a preparation method and application thereof.The preparation method comprises the steps that A, raw materials are mixed, a hydrochloric acid solution is added to adjust the pH of a system to 5-6, stirring and cooling are conducted to the room temperature, then standing is conducted to form wet gel, freeze drying is conducted, and gel is obtained; wherein the raw materials comprise 0.8 g to 1.2 g of copper acetylacetonate, 4 g to 6 g of 2-aminobenzaldehyde, 4 g to 6 g of melamine phosphate, 4 g to 6 g of resorcinol and 8 ml to 12 ml of a formaldehyde solution with the concentration being 30 wt%; b, carbonizing the gel in inert protective gas to obtain copper-doped porous carbon; c, tin powder and the copper-doped porous carbon obtained in the step B are subjected to ball milling and mixing according to the mass ratio of 2: (7-12), then the mixture is placed in inert protective gas to be carbonized, and the tin-copper co-doped porous carbon is obtained. The prepared porous carbon material is high in CO2 electrocatalytic activity and has a wide application prospect.
Owner:ENERGY RESOURCES INST HEBEI ACADEMY OF SCI
0.5-10 [mu] m visible light-intermediate infrared metamaterial conical stacked perfect absorber
The present invention relates to a tapered stack absorber capable of perfect light absorption in the spectral range of 0.5 [mu] m to 10 [mu] m. The structure is formed by periodically arranging conical unit structures in the horizontal direction, the bottommost layer of each unit structure is a square titanium (Ti) plate with the thickness of d and the width of p, and the square titanium (Ti) plate is used for preventing transmission of electromagnetic waves. On the basis of a Ti plate, 18 TiN / VO2 disc composite layers are stacked from bottom to top, the radius size is decreased by delta t every time, the radius of the bottom composite layer is D1, and the radius of the top composite layer is D2. The upper layer of the composite layer is a TiN layer with the height of h, and the lower layer of the composite layer is a VO2 layer with the height of h. The structure can realize perfect absorption from visible light to a middle infrared band (0.5-10 [mu] m).
![0.5-10 [mu] m visible light-intermediate infrared metamaterial conical stacked perfect absorber](https://images-eureka.patsnap.com/patent_img/abd78d22-9699-44c9-88f8-0e3a2809de2e/CN120143323A.png "0.5-10 [mu] m visible light-intermediate infrared metamaterial conical stacked perfect absorber")
Owner:XIANGTAN UNIV
Magnetic code disc film material and preparation method and application thereof
The invention provides a magnetic code disc film material and a preparation method and application thereof. By introducing the TiN layer, a proper amount of nitrogen atoms can enter lattice gaps of iron, electron cloud distribution of iron atoms is changed, and the magnetic moment of the iron atoms is changed; the magnetic moment of Fe atoms can be influenced by N atoms and crystal structures, an alpha-Fe8N phase is formed in FeCoCr through introduction of N ions, the average magnetic moment of each Fe atom in the alpha-Fe8N phase is 2.4 mu B, alpha-Fe8N is a metastable phase, a sample can finally form stable gamma '-Fe4N through annealing, and the magnetic moment of the stable gamma'-Fe4N is generally about 2.5 mu B-2. 7 mu B and is higher than the magnetic moment 2.2 mu B of the Fe atoms in metal Fe; besides, Ti forms a Ti-Fe weak magnetic phase pinning magnetic domain wall in the FeCoCr thin film, and the coercive force and residual magnetism of the FeCoCr layer can be effectively improved at the same time through the method.
Owner:JIHUA LAB