9344 results about "Powder" patented technology

The invention discloses crack-chloride ion double-triggered subsea tunnel corrosion-resistant concrete and a preparation method thereof, and relates to the field of subsea tunnel engineering materials. The concrete is prepared from the following components in parts by weight: 400 to 500 parts of Portland cement, 50 to 80 parts of fly ash, 60 to 100 parts of superfine mineral powder, 1000 to 1100 parts of coarse aggregate, 700 to 800 parts of fine aggregate, 140 to 160 parts of water, 10 to 20 parts of self-repairing microcapsules and 1 to 5 parts of a water reducing agent, the self-repairing microcapsule comprises a capsule wall material, a self-repairing material and a layered dihydroxyl composite metal oxide. A crack-chloride ion double-response system is constructed, and the limitation of traditional single trigger repair is broken through. When a crack with a certain width appears in the concrete, the capsule wall of the self-repairing microcapsule is broken to release the repairing component, so that effective filling of the crack is realized; and meanwhile, the layered double-metal hydroxide can directionally adsorb chloride ions to form a stable compound, so that the migration rate of the chloride ions is remarkably reduced.

The invention provides a data correction method and system combined with lattice structure additive manufacturing process characteristics, and the method comprises the steps: firstly employing a Newton iteration method, taking the radius of a pillar as a variable, optimizing the relative density of an iteration target and generating a lattice structure geometric model under the condition that a process constraint condition is satisfied, and extracting actual geometric parameters after forming through CT scanning, the elastic modulus is corrected through the pillar diameter deviation and the defect volume fraction, a compression failure mechanism is combined, a density-related failure criterion is introduced, a nonlinear relation with the relative density is constructed through specific energy absorption data, material plasticity parameters are inversely optimized, and a defect coupling evaluation model is constructed according to the surface powder sticking rate and the pillar diameter deviation. And establishing a Gaussian mixture model based on a stress-strain curve to screen out abnormal data, and finally fusing the parameters to construct a data correction model. The dot matrix structure design precision can be improved, and then a high-quality data basis is provided for performance prediction-structure design two-way feedback.

The invention relates to the technical field of filling materials, and particularly discloses an ardealite-based high-strength anti-seepage filling material and a preparation process thereof, the ardealite-based high-strength anti-seepage filling material comprises 50%-65% of pretreated ardealite, 15%-25% of Portland cement, 5%-15% of superfine slag powder, 5%-10% of electrolytic manganese residues, 5%-8% of silica fume, 3%-6% of metakaolin, 2%-4% of a composite alkali activator and 0.5%-1.2% of a polycarboxylic acid water reducer, 0.3%-0.8% of an organic silicon water repellent and 0.05%-0.1% of cellulose ether; according to the invention, through chemical reaction of Mn < 2 + > in the electrolytic manganese residue and SO4 < 2-> in the phosphogypsum, micron-sized manganite crystals (MnAl2 (SO4) 4. 22H2O) are generated to actively fill internal micro-cracks of the material, so that a filling body is endowed with a self-repairing function and the impermeability is improved, and a composite alkali activator composed of NaOH and water glass is used for synergistically activating potential gelling activity of the superfine slag powder and the silica fume, so that the self-repairing filling material is prepared. And the formation of hydration products is accelerated, and 0.3-0.5 T of pulsed magnetic field is applied in the stirring process, so that the manganite crystals are guided to orderly grow along the expected stress direction of the filling body, and the compressive strength is improved.

The invention discloses a high-strength and high-toughness aluminum nitride ceramic and a preparation method thereof, and relates to the technical field of ceramics, a sol-gel method is adopted to coat the surface of aluminum nitride with a stable shell layer to form a core-shell structure, meanwhile, the low lattice mismatch rate of a core-shell interface is utilized to reduce thermal resistance, and toughness and thermal conductivity are both considered; according to the external magnetic field tape casting method, the magnetic dipole moment orientation principle is utilized, an external magnetic field is applied in the tape casting stage, the in-plane mechanical property is improved, and the fracture toughness is improved through the magnetism of aluminum nitride whiskers; a reinforcement is introduced to improve the mechanical property and corrosion resistance of the aluminum nitride ceramic material, multi-granularity powder is compounded, large-particle aluminum nitride powder is used as a sintering and heat-conducting framework material, and high activity provided by submicron particles is utilized to promote sintering, so that the sintering temperature of aluminum nitride can be remarkably reduced, and the performance is greatly improved; and the aluminum nitride substrate expands more application fields on a future packaging circuit.

The invention relates to the technical field of quality detection, in particular to a gas atomization powder sphericity degree multi-dimensional online analysis system and a method thereof.The gas atomization powder sphericity degree multi-dimensional online analysis system comprises a dynamic dual-mode imaging module, a transverse wind field auxiliary detection unit and a multi-dimensional feature fusion analysis module; the transverse wind field auxiliary detection unit is used for applying controllable transverse wind power through an airflow nozzle orthogonal to the powder falling direction and measuring the deflection track of gas atomization powder ball particles in combination with a laser displacement sensor. The online calibration module is used for spraying standardized spherical particles to the powder flow according to a preset period; the traditional density detection depends on destructive sampling and off-line measurement, the efficiency is low, and the whole production line particles cannot be covered; through an orthogonal wind field trajectory inversion technology, a density value and an internal defect mark are synchronously output through non-contact dynamic measurement, 100% lossless online full inspection of a production line is realized, and sampling limitation and aging bottleneck of a traditional means are broken through.

The invention provides an early-strength rapid-repair grouting material and a preparation method thereof, and the early-strength rapid-repair grouting material is mainly prepared from the following raw materials: 50 to 150 parts of sulphoaluminate cement, 10 to 150 parts of aluminate cement, 200 to 350 parts of a regenerated gelling powder material, 1200 to 1400 parts of quartz sand, 50 to 100 parts of silica fume, 10 to 150 parts of mineral powder, 10 to 100 parts of fly ash, 15 to 50 parts of a composite retarder, 0.1 to 2 parts of a water reducing agent and 1 to 10 parts of an early strength agent. 0.01 to 1 part of a water-retaining agent and 200 to 300 parts of water. The early-strength quick-repair grouting material is characterized in that activated low-cementitious active mineral solid waste is adopted as a main cementitious material, and the product has excellent construction stability, low-carbon weather resistance, corrosion resistance, micro-expansion quick-hardening early strength and economical efficiency.

The invention relates to the technical field of program control, in particular to a precise powder supply control system, which is characterized in that multi-cycle differential processing of a rotating speed fluctuation ratio of a spiral feeder is performed on multiple key parameters such as a powder batch particle size value, a batch density value, an accumulated discharging amount and a feeding cycle; abnormal fluctuation numbers are extracted in different periods and combined according to the abnormal fluctuation numbers to generate a feeding feature set, a fuzzy neural network is utilized to improve the fitting precision of a discharging rate change trend under a nonlinear condition, the screening capability of extreme value interference is improved, a fluctuation difference value sequence is associated with symbol consistency and a density mean value, and the accuracy of the fluctuation difference value sequence is improved. Analyzing the variation trend of the discharge deviation in the symbol direction and the numerical slope, matching the numbers to establish a feed deviation grade section sequence, adopting a generative adversarial network to construct a target and actual discharge quantity difference value sequence, dividing symbol consistent sections, extracting the coupling trend of the fluctuation slope and the average density value, and obtaining a target discharge quantity difference value sequence; and misjudgment caused by deviation mode covering is avoided.

The invention provides nano-silicon-based high-strength concrete and a preparation method thereof, and belongs to the technical field of concrete.The concrete is prepared from cement, mineral powder, fly ash, machine-made sand, first-class gravel, second-class gravel, an additive, nano-silicon or a nano-silicon composite modified material and water; the additive is a polycarboxylic acid water reducer and / or a polyether air entraining agent. According to the prepared concrete, the nano silicon material with good dispersity is added, so that the cement consumption can be reduced, the cost can be reduced, and the workability, the strength and the durability can be improved; and the preparation process is simple and convenient, is suitable for large-scale production, and can be widely applied to the engineering fields of high-rise buildings, bridges, tunnels and the like.

The invention relates to the technical field of intelligent optimization, and discloses a 3D printing powder proportion optimization method and system based on artificial intelligence. The method comprises the following steps: collecting historical data corresponding to a powder material based on a printing process of a 3D printed finished product, and performing multivariate analysis on the historical data to generate a plurality of powder compositions; the material simulation model is used for carrying out property simulation on any powder composition, outputting material property data and extracting a powder ratio meeting the printing requirement; the finished product prediction model performs finished product prediction on any powder ratio, outputs a finished product prediction result, performs matching optimization on the finished product prediction result and ideal finished product data, and screens out an optimal powder ratio and a corresponding optimal printing process; and performance testing is conducted on the actual printing finished product, if the actual printing finished product does not meet the requirement, the step is executed repeatedly, and a new optimal powder proportion and a new optimal printing technology are screened out again. According to the method, the precision of 3D printing powder proportion optimization is improved.

The invention is suitable for the technical field of advanced powder metallurgy and ceramic material sintering, and provides an assembly line type flash sintering system and a sintering method. The system comprises a powder loading and pre-pressing module, a first automatic graphite paper pressing, paving and replacing module, a sintering module, a demolding and sampling module and a second automatic graphite paper pressing, paving and replacing module which are sequentially arranged in the material flowing direction, all the modules are connected through the vacuum switching module to form a continuous vacuum environment; the system further comprises a conveying system which is used for driving the sintering units bearing materials to sequentially flow among the modules. The continuous flash sintering device is suitable for carrying out efficient and full-automatic continuous flash sintering treatment on powder materials in a vacuum or protective atmosphere environment, the platform overturning risk can be fundamentally avoided, and the stability and safety of the sintering process are ensured.

The invention provides a high-precision laser additive manufacturing method and device based on metal powder melting, and relates to the technical field of metal additive manufacturing, and the high-precision laser additive manufacturing device comprises a multi-element powder supply and electrification unit which is used for carrying out independent metering supply and airflow dispersion mixing on various metal powder in an inert atmosphere environment and enabling powder particles to obtain controllable charges; the electromagnetic field cooperative control unit is used for actively regulating and controlling the falling speed and the transverse track of the powder particles through the cooperative effect of a longitudinal magnetic field and a transverse electric field when the powder particles are in a charged state; the invention provides a metal powder forming technology path based on particle size active conveying and spatial positioning, and active conveying and accurate positioning of the metal powder particles in the flying process are realized by performing electrified regulation and control on single or small-scale metal powder particles and utilizing the action of an electromagnetic field. Therefore, layer-by-layer stacking forming is completed under the condition of not depending on the whole powder laying layer.

The invention relates to a preparation method of a flexible solid hydrogen storage bed body, which comprises the following steps: S1, mixing 74-90% by mass of hydrogen storage alloy powder and 3-16% by mass of carbon-based heat conduction material for 20-50 minutes in a mechanical stirring manner to obtain a dry powder mixture; s2, adding an organic silicon material with the mass fraction of 5-16%, and continuously mechanically stirring for 1-5 hours to obtain a non-dry powder mixture; and S3, carrying out vacuum drying on the non-dry powder mixture in the S2 at 60-100 DEG C for 8-20 hours, and naturally cooling to room temperature to obtain the required novel non-dry powdery hydrogen storage bed body. Through the synergistic effect of the hydrogen storage alloy, the expanded graphite and the double-liquid silica gel, the flexible solid hydrogen storage material is formed on the basis of optimizing the material ratio and the process sequence. The synergistic effect of the materials breaks through the defect that a traditional hydrogen storage bed body is too high in rigidity or in a loose powder state, and finally the hydrogen storage bed body has high hydrogen storage efficiency, stable cycle life and excellent safety performance.

The invention belongs to the technical field of nickel electrode slurry preparation, discloses a preparation process of ultra-fine particle size roll-printed nickel electrode slurry for an ultra-high capacity MLCC, and aims to solve the problems that in the prior art, ultra-fine nickel powder is easy to oxidize, the cost of covering nickel nitride powder is high, a covering layer is easy to damage and agglomerate during dispersion, and the performance of the slurry is poor. The method comprises three steps of raw material pretreatment, synchronization of material dispersion and nitridation, post-treatment and nitrogen protection, wherein the pretreatment is used for removing impurities and preventing oxidation, dispersion and nitridation are carried out synergistically through a sand mill and an ultrahigh-pressure homogenizer in a graded regulation and control mode, the post-treatment comprises filtering, inspection and double-layer vacuum packaging, the raw materials are prepared according to a specific proportion, key parameters are precisely regulated and controlled, and finally the slurry is prepared. Roll printing adaptability and co-firing requirements are met, independent nitridation and reduction procedures are omitted, cost is reduced, slurry uniformity, dispersion stability and MLCC reliability are improved, and large-scale mass production can be achieved.

The invention relates to the field of building material preparation, in particular to a high-strength concrete material and a preparation method thereof.According to the high-strength concrete material, through the synergistic effect of core-shell type temperature-sensitive resin particles, a pH response type expanding agent and industrial solid waste composite micro powder, multi-environment self-adaptive crack resistance and mechanical property breakthrough are achieved. The core component is prepared from 180 to 240 parts of cement, industrial solid waste composite micro powder (30 to 50 parts of fly ash-based nano SiO2 and 50 to 70 parts of steel slag micro powder), 10 to 15 parts of core-shell resin particles and 8 to 12 parts of pH response type expanding agent. According to the preparation process, multi-section intelligent stirring (ultra-high-speed shearing and dispersing of the nanometer material) and dynamic maintenance of the internet of things are adopted, the hydration process is precisely regulated and controlled, and the finally prepared material has excellent compressive strength and anti-cracking performance. The method is suitable for severe scenes such as ocean engineering and plateau buildings, and has wide application prospects.

The invention discloses an aluminum-based composite material powder continuous forming press with an automatic powder feeding function, and relates to the technical field of powder type presses, the aluminum-based composite material powder continuous forming press comprises a main base, a pressing die is fixedly installed in the main base, and a stamping head driven by a stamping mechanism is further arranged on the main base; a material mixing mechanism used for mixing powder in the pressing mold is arranged in the main base, a demolding mechanism used for demolding is arranged in the pressing mold, a powder feeding mechanism and a discharging mechanism which are used for feeding powder and discharging are further arranged on the main base, the material mixing mechanism comprises a guide table, and a guide sliding block driven by a lifting driving part is slidably connected into the guide table; during use, through the linkage design of the lifting sliding seat, the connecting rod, the guide sliding blocks and the spherical hammer rods in the material mixing mechanism, the spherical hammer rods knock and mix powder in a mold, the powder fluidity is remarkably improved, it is guaranteed that the powder is evenly distributed in the mold, and the pressing quality is guaranteed.

The invention provides a rotating electrode atomization powder preparation control system and a control method. A multivariable machine learning prediction model among the electrode rotating speed, the plasma arc power, the protective gas flow, the powder particle size and the sphericity degree is established; calculating the optimal electrode rotating speed, plasma arc power and protective gas flow by using the multivariable machine learning prediction model according to the target powder particle size and sphericity; the optimal technological parameters are applied to the powder making process, and a powder making system is operated; the electrode rotating speed, the electric arc power and the gas pressure are monitored in real time in the atomization process, and technological parameters are dynamically adjusted to compensate fluctuation; the image acquisition unit is used for acquiring images of flying powder particles, particle size distribution and sphericity are analyzed in real time through an AI visual model, and the electrode rotating speed, plasma arc power and protective gas flow are fed back and adjusted according to analysis results.

The invention relates to the technical field of tunnel engineering building materials, in particular to a double-slurry synchronous grouting material based on shield silty-fine sand and a preparation method of the double-slurry synchronous grouting material based on shield silty-fine sand. The liquid A is prepared from, by weight, 20%-30% of cement, 30%-50% of shield silty-fine sand, 5%-10% of bentonite, 5%-15% of mineral admixture, 0.1%-0.5% of stabilizer and 20%-30% of water, and the stabilizer is a water-soluble high-molecular polymer; the solution B is a water glass solution, and the volume ratio of the solution A to the solution B is (10-15): 1; the double-slurry synchronous grouting material further comprises a retarder and a coagulant, the retarder is citric acid, and the coagulant is a nano Ca (OH) 2 crystal nucleus. Bidirectional and gradient regulation and control of the gelation time between 5s and 100s can be realized through the coagulant and the retarder, and diversified requirements of different geological conditions and construction progress on slurry operation time are met.

The invention belongs to the technical field of ceramic materials, and discloses a high-entropy boride composite silicon carbide ceramic with a controllable microstructure and a preparation method and application thereof. The method comprises the following steps: carrying out ball milling, drying and sieving on Zr, Ta, Nb, W, Cr, B4C and SiB6 to obtain mixed powder; the preparation method comprises the following steps: putting a boron carbide powder into a graphite mold of which the inner surface is coated with a BN layer, heating to 1850-2050 DEG C, carrying out SPS sintering, and preparing the high-entropy boride composite silicon carbide ceramic with controllable microstructure under 20-35 MPa and a vacuum degree of 10 Pa, and the molecular formula of the high-entropy boride composite silicon carbide ceramic is (Zr0. 2Ta0. 2Nb0. 2W0. 2Cr0. 2) B2-SiC. The ceramic has good mechanical properties, the hardness at room temperature is 27-32 GPa, the fracture toughness is 4.5-6 MPa.m < 1 / 2 >, the bending strength is 450-600 MPa, and the ceramic can be applied to extreme environments or the field of radiation protection.

The invention provides spiral feeder and metering scale integrated equipment for improving feeding precision, and relates to the technical field of metering and feeding of powdery and granular materials. According to the integrated equipment, a frequency converter is additionally arranged on a spiral scale, so that a constant-speed spiral metering scale is changed into a speed-regulating spiral metering scale, a signal separator is introduced to divide a PID negative feedback signal output by an instrument into two paths, the two paths respectively control a frequency converter of a steady-flow spiral feeder and a frequency converter of a metering screw, and meanwhile, a speed measuring sensor is additionally arranged on the spiral scale; and synchronous double-closed-loop control is realized. The spiral scale solves the problems that when an existing spiral scale is used for metering powder, flow is unstable, and arching, jet flow, blocking and the like are prone to occurring, the dynamic deviation can be controlled within 0.5%, the feeding precision and stability are remarkably improved, and the spiral scale is suitable for metering and feeding of powdery and granular materials in the industries of cement, chemical engineering, metallurgy, ceramics, grain, transportation and the like.

The present application discloses an efficient stirring device 100, which includes a stirring tank body 101 forming an inner tank space to accommodate a mixture of powder materials and liquid materials; a stirring paddle103 and a stirring main shaft 104, at least a portion of which is disposed within the inner tank space and rotates around a central axis; a stirring motor 105; and the efficient stirring device further includes: a plurality of scraping members 101 rotatably disposed within the inner tank space to scrape off the mixture adhering to the inner wall of the stirring tank body when rotating on their own axes; a plurality of transmission shafts 107, at least a portion of which is disposed within the inner tank space; a power main shaft 108 for driving the transmission shafts to rotate on their own axes and to revolve around the central axis; and a scraping motor 109 for driving the scraping main shaft to rotate. Among them, the scraping members are connected to the transmission shafts in a non-rotating manner to move with the transmission shafts, and the transmission shafts are disposed parallel to the power main shaft. The advantage of the present application is that it provides an efficient stirring device that improves the wetting efficiency by disposing scraping members within the inner tank space that rotate on their own axes and revolve to scrape off the mixture adhering to the inner wall of the stirring tank body.

The invention belongs to the technical field of solid waste concrete, and discloses fireproof sound-insulation heat-preservation light-weight high-strength all-solid waste concrete and a preparation method thereof.The fireproof sound-insulation heat-preservation light-weight high-strength all-solid waste concrete is prepared from an all-solid waste fireproof cementing material, all-solid waste light aggregate, water and a functional additive; the all-solid-waste fireproof cementing material comprises an alkaline activator component and an active powder component, the alkaline activator component comprises red mud and carbide slag in a mass ratio of (1.5-2.5): 1, and the active powder component comprises granulated blast furnace slag and low-temperature activated calcined coal gangue powder in a mass ratio of (1.0-1.8): 1; the all-solid-waste lightweight aggregate comprises coarse aggregate and fine aggregate in a mass ratio of (1-1.5): 1, wherein both the coarse aggregate and the fine aggregate comprise high-temperature expanded and roasted coal gangue lightweight aggregate; wherein the low-temperature activated and calcined coal gangue powder is obtained by performing gradient temperature control calcination on coal gangue at 650-800 DEG C and then grinding the coal gangue until the specific surface area is greater than or equal to 500m < 2 > / kg; the high-temperature expanded and roasted coal gangue lightweight aggregate is obtained by roasting and expanding coal gangue at 1100-1300 DEG C and then screening and grading.

The invention discloses a method for preparing spherical metal fine powder by using coarse / waste powder through ultrasonic atomization, which comprises the following steps of: (1) collecting coarse / waste powder raw materials for ultrasonic atomization powder preparation, (2) conveying the coarse / waste powder to an electric arc melting area through argon gas flow, and carrying out melting and ultrasonic atomization powder preparation processing; (3) in the powder preparation process, the powder is continuously collected by using argon circulating airflow, so that the continuity of the powder preparation process is ensured; and (4) finally screening the prepared powder in particle size ranges to obtain high-quality spherical fine powder in different particle size ranges. According to the method, the recycling and reusing problems of 3D printing splashing waste powder and coarse powder in the traditional gas atomization powder manufacturing process are solved, and the powder pollution risk is remarkably reduced; according to the ultrasonic atomization re-powdering technology, the high-quality spherical metal fine powder needed by additive manufacturing can be efficiently prepared, powder waste discharge and environmental burden are reduced, the obtained powder can be directly used as a high-quality raw material for additive manufacturing, and green and sustainable development of the metal additive manufacturing industry is promoted.

The invention relates to the technical field of material transportation, in particular to a conveying pressure control method and device of a powder and particle pneumatic conveying system. The method comprises the steps that the material humidity, the conveying pressure and the air speed of a frequency conversion fan are obtained; determining a humidity adjusting coefficient; in the pressurization stage, a suppression coefficient is determined according to the current wind speed and the target wind speed; according to the humidity adjustment coefficient and the inhibition coefficient, inhibiting the proportionality item to obtain a target proportionality coefficient; enhancing the differential term in combination with the humidity adjustment coefficient and the pressure deviation to obtain a target differential coefficient; in the pressure reduction stage, the standard humidity is compared with the air speed and the conveying pressure under the material humidity at the current sampling moment and the humidity adjusting coefficient, the integral item is adjusted, and a target integral coefficient is obtained; and adjusting the conveying pressure based on the adjusted PID coefficient. The problem of asymmetry of bidirectional adjustment of pressurization and depressurization can be solved, the adjustment logic is optimized, and the conveying efficiency and stability of pneumatic conveying of powder and particle materials are improved.

The embodiment of the invention relates to the field of radioactive waste treatment, in particular to a solidification method. According to the method, a conveying and jacking device is used for conveying a material containing device to enable the material containing device to receive powdery materials, a clamping and transferring device and a lifting device are used for conveying the material containing device completing feeding into a material processing device to enable the powdery materials to be partially molten, and a pressurizing device is used for pressing and compacting the partially molten materials; and finally, ingot-shaped solid materials are formed in the material containing device, then the lifting device and the clamping and transferring device are utilized again to transfer the material containing device to the conveying and jacking device so as to transfer the ingot-shaped solid materials, in this way, the process from powder feeding to ingot forming of the materials is conducted in the material containing device, the situation that a material container is replaced in the midway is avoided, and the production efficiency is improved. Operation steps are simplified; and the clamping and transferring device, the lifting device and the conveying and jacking device all participate in the front process and the rear process of material treatment, so that reuse of equipment parts is achieved, and the equipment composition is simplified.

The invention relates to the technical field of solid waste treatment and recycling, and discloses a waste incineration fly ash geopolymer composite material and a preparation method thereof, and the composite material is prepared from waste incineration fly ash, apatite minerals, zero-valent iron powder, persulfate and an alkali activator. The preparation method comprises the following steps: mixing the waste incineration fly ash, apatite minerals, zero-valent iron powder and persulfate to obtain composite powder; performing frequency conversion mechanochemical synergistic activation on the composite powder, wherein the activation process comprises a low-temperature activation stage and a high-energy pulse activation stage; and finally, mixing the activated powder with an alkali activator, pouring, molding and curing. According to the method, the reduction reaction and the oxidation reaction are driven step by step in the same system by regulating and controlling the mechanical energy input time sequence, the compatibility problem of a reducing agent and an oxidizing agent is solved, different types of persistent organic pollutants are synergistically degraded, meanwhile, heavy metal is stabilized, and the treatment effect is good. And the fly ash is recycled to prepare a geopolymer material with mechanical properties.

The invention relates to the technical field of concrete materials, and discloses rapidly-reinforced high-performance sprayed concrete for an existing tunnel lining and a preparation method of the rapidly-reinforced high-performance sprayed concrete. The sprayed concrete is prepared from the following raw materials in parts by weight: 300 to 350 parts of low-calcium high belite sulphoaluminate cement, 80 to 100 parts of superfine slag powder, 3 to 8 parts of a trigger type activating agent, 5 to 15 parts of slow-release particles, 2 to 5 parts of nanogel, 800 to 900 parts of fine aggregate, 800 to 900 parts of coarse aggregate, 30 to 50 parts of copper-plated steel fiber, 0.8 to 1.2 parts of polypropylene fiber, 30 to 40 parts of a viscosity-adjusting accelerator, 10 to 20 parts of a water reducing agent and 160 to 180 parts of water. The sprayed concrete is high in compressive strength and good in durability, the double threats of chemical corrosion and chloride ion permeation / steel bar corrosion are cooperatively solved, and the requirement for rapid reinforcement of tunnels and underground engineering is met.

The invention relates to the technical field of pavement materials, in particular to a solid waste-based cementing material stable coal-based solid waste road base material and a preparation method thereof. According to the material, secondary modified regenerated coarse and fine aggregate is used as a framework, coal gangue powder and granulated blast furnace slag micro powder are matched, and two-step engineering of dopamine / double-amino-terminated polyethylene glycol co-deposition grafting and high-modulus silicate pre-coating is adopted, so that the synergistic improvement of the surface wettability and the interface density of the aggregate is realized. The system is cooperated with low-modulus excitation liquid and polypropylene fibers, and the mixing uniformity of the material and the quality of an interface transition area are optimized through a thin-pulp stone-wrapping and densification segmentation process. The material gives consideration to high resilience modulus, rut resistance and durability, significantly reduces the problems of high water absorption, weak interface, early cracks and the like of the recycled aggregate, is adaptive to a traditional road construction window, and has good application prospects.

The invention relates to the technical field of non-oxide ceramic-based composite materials, in particular to Fe-N-based high-entropy nitride ceramic as well as a preparation method and application thereof. The method comprises the following steps: by taking iron powder as a sintering aid, mixing (Hf < 0.2 > Zr < 0.2 > Ti < 0.2 > Nb < 0.2 > Ta < 0.2 >) N high-entropy powder with the iron powder, and carrying out ball milling treatment to obtain ball-milled powder; and under the oxygen-free condition, the ball-milled powder is subjected to sintering treatment, transformation from the loose ball-milled powder to compact and uniform solid solution ceramic is achieved in the sintering treatment process, and the Fe-N-based high-entropy nitride ceramic is obtained. According to the method, a nitride thermal reduction method sintering process is adopted, energy is provided for densification of the Fe-N-based high-entropy nitride ceramic by utilizing reaction heat release of the (Hf0. 2Zr0. 2Ti0. 2Nb0. 2Ta0. 2) N high-entropy powder and the iron powder, the sintering temperature is reduced, energy is saved, and the defect that densification needs to be carried out under a high-temperature condition in the prior art is overcome.

The invention discloses an energy-saving type electric grinding device for plugging agent production, and relates to the technical field of grinding devices, the energy-saving type electric grinding device comprises a grinding box and a feeding bin, and further comprises a driving assembly; the driving assembly comprises a supporting frame, a driving motor, a small bevel gear and a large bevel gear. A heat dissipation opening is formed in the end of the driving motor, a heat absorption cover is arranged above the heat dissipation opening, and a heat conduction pipe is fixed to the end, away from the driving motor, of the heat absorption cover. A ventilation pipe made of metal is fixed to one side of the feeding bin, the air inlet end of the ventilation pipe is connected with the air outlet end of the heat conduction pipe, an electric heating wire is wound around the outer wall of the ventilation pipe, and the electric heating wire is wrapped with ceramic fiber cotton. A movable shaft is rotationally connected into the feeding bin; a plurality of uniformly distributed scattering plates are fixed on the side surface of the movable shaft; a rotating shaft is movably connected into the grinding box, and a grinding ball is fixed to the unoccupied end of the rotating shaft; and synchronous operation of material grinding and crushing can be achieved, heat dissipation is accelerated, meanwhile, material particles are dried, and the material grinding efficiency is improved.

The invention discloses a preparation method of thermal shock resistant magnesium aluminate spinel transparent ceramic, and belongs to the technical field of ceramic materials. The preparation method comprises the following steps: (1) synthesizing crystalline MgAl2O4 nano powder by adopting an additive-free hydrothermal method; (2) depolymerizing the powder, performing water-based gel casting to prepare a green body, and performing staged debonding treatment on the green body; (3) carrying out two-step vacuum presintering on the green body; (4) carrying out hot isostatic pressing densification treatment in a subgrain growth temperature region of 1380-1420 DEG C; and (5) carrying out annealing treatment on the densified ceramic. High-purity crystalline powder is synthesized through an additive-free hydrothermal method, grain boundary impurities are eliminated, and the intermediate infrared transmittance is remarkably improved; by combining the synergistic effect of optimized two-step pre-sintering and hot isostatic pressing in a sub-grain region, precise refinement of the grain size is realized; and finally, the bending strength, the fracture toughness and the critical thermal shock temperature difference of the material are greatly improved under the strengthening mechanism of ultrafine grains and defect-free grain boundaries.