2663results about How to "Reduce dosage" patented technology

The invention relates to a superconductive annular air-core reactor structure optimization method, a medium and a program product, and the optimization method comprises the steps: optimizing the structure parameters of a superconductive reactor through an MATLAB and COMSOL joint simulation technology, and carrying out the optimization of the structure parameters of the superconductive reactor through a multi-objective genetic algorithm, thereby achieving the optimization of the structure parameters of the superconductive reactor. Iterative optimization is conducted on structural parameters such as the coil inner diameter, the surrounding radius, the number of turns of the coils, the number of the coils and the number of parallel branches of the electric reactor, the optimization target comprises the minimum strip use amount and alternating current loss, and in the optimal solution set, according to the strip use amount and the alternating current loss, the strip cost and the refrigeration cost are calculated. And finally, outputting an optimal structure parameter meeting a design index so as to realize the minimization of the total cost. Compared with the prior art, the method can be used for structural optimization of the superconducting reactors with different capacities, structural parameters with the lowest cost under different indexes can be obtained by setting constraint conditions, and economic benefits of reactor design are improved.

The invention provides a bismuth oxide-based epoxy resin composite material with a radiation shielding function as well as a preparation method and application of the bismuth oxide-based epoxy resin composite material. According to the preparation method disclosed by the invention, the bismuth oxide is subjected to surface modification, and after surface grafting modification by the coupling agent, the surface of the bismuth oxide is changed from strong hydrophilicity to strong hydrophobicity, so that the dispersity and interfacial compatibility of the bismuth oxide in an organic medium are remarkably improved. Secondly, preparing the composite material from the modified bismuth oxide, epoxy resin and a curing agent through a mechanical blending-vacuum defoaming combined process. On one hand, bismuth oxide, epoxy resin and a curing agent are uniformly mixed through mechanical blending; on the other hand, bubbles generated in the blending process are removed through vacuum negative pressure. The bismuth oxide in the composite material is uniformly distributed, no bubble exists in the body, and the surface is smooth and complete, so that the composite material has excellent gamma-ray shielding performance and good mechanical property. The process is simple, the yield is high, the product property is stable, and good economic benefits and environmental benefits are achieved.

The invention belongs to the technical field of metal powder preparation, and discloses a method for preparing silver powder through reduction of hydrazine hydrate with the adjustable particle size. The preparation method comprises the following steps that a first dispersing agent is dissolved in deionized water, a silver-ammonia solution and a hydrazine hydrate solution are sequentially added, stirring reaction is conducted, and nano-silver seed crystal sol is obtained; uniformly mixing the obtained nano-silver seed crystal sol with a hydrazine hydrate solution and a second dispersing agent to obtain a reducing base solution; adding a surface modifier into absolute ethyl alcohol, and uniformly dissolving to obtain a surface modification coating solution; preparing a silver-ammonia solution, adding the prepared silver-ammonia solution into the reducing base solution, then adding the surface modification coating solution, and stirring for reaction to obtain silver powder slurry liquid; and after solid-liquid separation, a solid phase is taken, washed and dried, and silver powder is obtained. The preparation method is simple in process, the particle size of the silver powder can be adjusted through the adding amount of the seed crystal, and the prepared silver powder particles are uniform in particle size distribution, high in dispersity and suitable for the fields of conductive silver paste, electronic packaging and the like.

The utility model relates to the field of solar photovoltaic technology, in particular to a battery piece, a battery piece stacking structure and a solar battery assembly. In the battery piece, the plurality of first isolation bulges are arranged on the back surface of the battery piece body, and the first isolation bulges protrude out of the back surface of the battery piece body; the plurality of second isolation bulges are arranged on the front surface of the battery piece body and protrude out of the front surface of the battery piece body; the plurality of grid lines 40 are arranged on at least one surface of the battery piece body; in the thickness direction of the battery piece body, the height of at least one of the first isolation bulges and the second isolation bulges is greater than that of all the grid lines; and the plurality of second isolation bulges are projected on the back surface of the battery piece body, and the projection does not intersect with the first isolation bulges, or the projection partially intersects with the first isolation bulges. The arrangement of the first isolation protrusions and the second isolation protrusions effectively prevents the grid lines from making contact with the front face of the battery piece body.

The invention discloses a chemical adding control system for sewage treatment, which comprises a data acquisition module used for acquiring sewage inlet water quality data and inlet water flow, water quality data of each sewage treatment process and discharge water quality data in real time; the data acquisition module is used for acquiring dosing data and detection data; the data preprocessing module is used for assigning the partial water quality data Em based on a preset judgment threshold value; the dosing prediction module is used for inputting the real-time data into the self-attention dosing prediction model and outputting to obtain a next dosing strategy; the self-attention dosing prediction model corrects the attention score matrix based on the chemical reaction relation matrix E; and the dosing control module is used for dosing according to the output dosing strategy. The method can adapt to sewage component and concentration changes, and the dosing strategy of each process of sewage treatment is accurately predicted and obtained.

The invention discloses a porous substrate reinforced anion exchange membrane and a preparation method and application thereof, and relates to the technical field of anion exchange membranes. The porous substrate reinforced anion exchange membrane is prepared by the following steps: uniformly mixing a polyarylene alkylene type cationic polymer solution and a C1-C10 alcohol solvent, then coating two sides of a porous substrate with the mixture, and drying to obtain the porous substrate reinforced anion exchange membrane. And removing the solvent to obtain the product. According to the method, the porous substrate can be well infiltrated by the cationic polymer solution without pre-treating the porous substrate, so that the porous substrate reinforced anion exchange membrane with a sandwich-like structure is obtained. The film has outstanding swelling resistance and excellent mechanical properties, has good electrochemical properties, and has good application prospects in alkaline film energy conversion devices.

The remediation method for the moderately and severely cadmium-polluted rice field aims at strictly controlled cadmium-polluted rice fields, and is divided into two stages of strict control and safe utilization for remediation. In the strict management and control stage, an activating agent is applied to the soil in spring, then microalgae are inoculated, cadmium-enriched plants are planted, the plants are collected after being full of the microalgae, the plants are harvested when the plants grow to the enrichment extreme value, stubbles are reserved for growth, and the steps are repeated till winter; applying an activating agent in winter, planting green manure, and harvesting in spring in the next year; the process is cyclically carried out until the cadmium content of the soil is reduced to a safe utilization level. Entering a safe utilization stage, applying an activating agent in spring, inoculating nitrogen-fixing cyanobacteria, collecting the cyanobacteria after the cyanobacteria overgrow, and repeating the steps until the rice seedlings are transplanted; applying nitrogen-fixing blue-green algae, and planting rice; applying an activating agent after rice harvesting, planting winter green manure, and harvesting in next spring; the process is cyclically carried out until the cadmium content of the soil is reduced to a preferential protection level. The method is low in cost, high in remediation efficiency and good in effect, and a new way is provided for cadmium-polluted rice field remediation.

The invention discloses a compound microbial fertilizer and application thereof in field planting. The survival rate of the paenibacillus mucilaginosus HX-02 disclosed by the invention can be up to 62.8% after 170d under the condition of 38% of nitrogen, phosphorus and potassium. The strain is organically combined with bacillus velezensis RKN1111 and a nitrogen-phosphorus-potassium inorganic fertilizer (N + P2O5 + K2O = 38%), the compound microbial fertilizer is developed, the viable count of effective bacteria is not less than 1.5 billion / g, and the viable count of paenibacillus mucilaginosus is not less than 0.5 billion / g. The compound microbial fertilizer taking the strain as a main functional bacterium is applied to field corn planting, can replace part of chemical fertilizers and increase soil fertility, can reduce the use amount of the chemical fertilizers by 15.56%, and achieves the effects of promoting the growth of field crops and increasing the yield by 10.2%. The paenibacillus mucilaginosus HX-02 is separated from soil, is harmless to human, livestock and environment, and meets the requirements of green plant protection and agricultural sustainable development.

The invention discloses a rare-earth metal arylamine group compound as well as preparation method and application thereof. The invention discloses the rare-earth metal arylamine group compound which is characterized in that a general formula of the rare-earth metal arylamine group compound is (2,6-R12PhNH)5LnLi2(THF)2, wherein Ln is a rear-earth metal selected from one of neodymium, samarium, ytterbium or yttrium; R1 is selected from one of hydrogen, methyl or isopropyl. The rare-earth metal arylamine group compound has the advantages that the rare-earth metal arylamine group compound has a definite structure; raw materials used in the preparation method are simple, easily obtained and cheap; the reaction process is simple and easily operated; the rare-earth metal arylamine group compound product is conveniently purified and the yield of the product is high; the rare-earth metal arylamine group compound has a high activity when acting as a single component catalyst to catalyze a hydrogen phosphine reaction of aldehyde or ketone and phosphite ester; the use amount of the catalyst is less; the yield is high; a substrate has wide universality; a new and simple method is provided for synthesis of a-hydroxyphosphonate.

The invention discloses a Ca / Mg-based modified biochar material and a preparation method and application thereof, and the preparation method comprises the following steps: pretreatment: drying a biomass material shaddock peel, crushing, sieving, washing and drying, then carrying out acid leaching activation, washing again and drying to obtain high-activity biomass powder for later use; dipping modification: fully mixing the high-activity biomass powder obtained in the pretreatment step with CaO and MgO, adding distilled water, dipping under heating and stirring conditions, then carrying out solid-liquid separation, washing a filter cake for multiple times, freeze-drying, and sieving to obtain an intermediate product; the intermediate product is calcined, naturally cooled, washed and dried, and the Ca / Mg-based modified bimetallic modified charcoal material is obtained and can be applied to adsorption of phosphate in a wastewater solution as an adsorbent. The preparation method is simple, the raw materials are easy to obtain, the cost is low, the material stability is good, the pH adaptability is good, the adsorption effect is good, and the method is suitable for water environments with more complex pollution factors.

A solar cell includes a cell substrate, a plurality of collector electrodes, a plurality of bus electrode segments, and a plurality of columns of interconnects. The battery substrate has a target surface. The current collection electrodes are arranged on the target surface, extend in the first direction and are distributed at intervals in the second direction intersecting with the first direction. The bus electrode section is located on the target surface and extends in the second direction. And each row of interconnection parts extend along a second direction, and the interconnection parts are arranged on the current collection electrodes. The bus electrode section extends in the second direction and is located in the upper end edge area and / or the lower end edge area of the target surface. On the target surface, the number of the bus electrode sections is smaller than two times of the column number of the interconnection parts, and / or the length of at least one bus electrode section is smaller than or equal to 5.3 mm, and / or the weighted average width of at least one bus electrode section is smaller than or equal to 0.29 mm. And by reducing the number of the bus electrode sections, the current collection electrode can collect current carriers to the maximum extent, and the conversion efficiency of the battery is improved. The utility model also provides a photovoltaic module comprising the solar cell.

The invention belongs to the field of vanadium metallurgy, and particularly relates to a method for preparing metal vanadium through aluminothermy in cooperation with molten salt electrolysis so as to solve the problem that in the prior art, the production cost of the metal vanadium is high due to the fact that high-temperature and high-vacuum refining is used for removing impurity aluminum. The method comprises the following steps: uniformly mixing a vanadium-containing raw material, metal aluminum and an additive according to a weight ratio of 100: (25-35): (4-8), igniting to carry out aluminothermic reduction reaction, and removing upper smelting slag after a reaction product is cooled to obtain primary metal vanadium; and the primary metal vanadium is subjected to molten salt electrolytic refining in the protective gas atmosphere, and refined metal vanadium is obtained. According to the method, high-temperature or high-vacuum refining is not needed, the high-purity metal vanadium can be prepared only through the two-step operation of aluminothermic reduction and molten salt electrolysis, and compared with an existing vanadium preparation process adopting high-temperature and high-vacuum refining, the energy consumption and the production cost are remarkably reduced.

The invention relates to the technical field of sulfur-iodine circulating hydrogen production, in particular to a thermochemical iodine-sulfur-barium circulating hydrogen production process and a thermochemical iodine-sulfur-barium circulating hydrogen production system, which comprises the following steps: reacting excessive Ba < 2 + > with sulfuric acid in a Bunsen reaction product to obtain barium sulfate so as to obtain a first reaction mixed solution containing HI, BaSO4, H2O, BaI2 and a small amount of unreacted I2; sequentially carrying out cyclone separation, liquid removal and filter pressing to obtain a barium sulfate filter cake and a second mixed solution containing HI, H2O and BaI2; the method comprises the following steps: crushing a barium sulfate filter cake, performing high-temperature decomposition, returning gas generated by decomposition to participate in Bunsen reaction, and dissolving BaO generated by decomposition into Ba < 2 + >; and reboiling the second mixed solution to obtain hydrogen iodide steam, cooling a product obtained by decomposing the hydrogen iodide steam, carrying out gas-liquid separation to obtain hydrogen, and returning liquid obtained by gas-liquid separation to participate in the Bunsen reaction of the next cycle. Barium circulation is introduced, the process is simplified, the dosage of elemental iodine is reduced, and the cost is low.

The invention discloses a method for degrading dioxin in fly ash and stabilizing heavy metals, which comprises the following steps: carrying out water washing treatment on the fly ash, and carrying out solid-liquid separation to obtain water washing slag; mixing the washed slag with water, adding zero-valent iron and sulfite, carrying out hydrothermal treatment, and carrying out solid-liquid separation to obtain hydrothermal slag and hydrothermal liquid; according to the method for degradation of dioxin in fly ash and stabilization of heavy metal in cooperation with degradation of dioxin in fly ash, under the combined action of zero-valent iron, chlorite and a hydrothermal environment, efficient degradation of dioxin in fly ash can be rapidly achieved under the lower reaction condition, stabilization of heavy metal in fly ash can be synchronously achieved, and the method is suitable for industrial production. The method has the advantages of being low in cost, mild in reaction condition, high in treatment efficiency, good in treatment effect, environmentally friendly and the like, can effectively solve the problems existing in the prior art, provides powerful support for harmless treatment and resource utilization of the waste incineration fly ash, and has wide engineering application prospects.

The utility model relates to a floating type offshore wind power suction anchor foundation mooring lifting lug structure which comprises a suction anchor cylinder body, a main eye plate and a cylinder body thickening plate, the cylinder body thickening plate is fixed on the inner side wall of the suction anchor cylinder body, the main eye plate is fixed on the outer side surface of the suction anchor cylinder body, and the cylinder body thickening plate is fixed on the inner side wall of the suction anchor cylinder body. The main eye plate penetrates through the side wall of the suction anchor cylinder and the cylinder thickening plate and is fixedly connected with a first connecting plate, a second connecting plate is fixed to the other side of the first connecting plate, and the second connecting plate is fixed to the inner side wall of the other side of the suction anchor cylinder. According to the utility model, the suction anchor cylinder body can form a whole with a stable structure.

The invention discloses a hybrid sturgeon feed and a preparation method thereof, and relates to the technical field of sturgeon feeds, and the key point of the technical scheme is that methionine and lysine are supplemented in a feed in which soybean protein concentrate replaces fish meal, so that the influence of methionine and lysine on the growth performance, liver and intestinal health and muscle quality of hybrid sturgeons is improved. The soybean protein concentrate is used for replacing the fish meal, so that the dosage and production cost of the fish meal are greatly reduced, and meanwhile, the methionine and the amino acid are added, so that the negative influence caused by replacing the fish meal with the soybean protein concentrate is avoided.

The invention belongs to the field of pesticides, and relates to a composition containing a biological source pesticide. The composition contains an active component A and an active component B, the component A is selected from a compound I-72, and the component B is selected from biological source insecticides and acaricides; the weight part ratio of the component A to the component B is (1: 99)-(99: 1); wherein the structural formula of the compound I-72 is shown in the specification, and the composition disclosed by the invention has an obvious synergistic effect and can be used for preventing and treating various pests and pest mites. # imgabs0 #

The invention provides a method for preparing a high-coercivity sintered neodymium-iron-boron magnet, and belongs to the technical field of rare earth permanent magnet material preparation, and the method comprises the following steps: 1, taking the sintered neodymium-iron-boron magnet as a base material, and removing an oxide layer through alkali washing deoiling, ultrasonic water washing and acid pickling cleaning; 2, taking the Pr-Dy-Cu-Ga quaternary alloy as a diffusion source, and cutting the Pr-Dy-Cu-Ga quaternary alloy into slices; 3, attaching the thin sheet to the surface of a base material for diffusion heat treatment; fourthly, low-temperature tempering is conducted; 5, testing a room temperature demagnetization curve of the sample; light rare earth Pr replaces a part of heavy rare earth Dy and is matched with Cu and Ga elements in a certain proportion to be smelted to obtain quaternary alloy, the quaternary alloy with low heavy rare earth serves as a diffusion source, the microscopic characteristics of the magnet are improved, grain boundary phase distribution is optimized, and under the condition that residual magnetism and the maximum magnetic energy product are slightly reduced, the coercive force of the sintered neodymium-iron-boron magnet is improved; and terbium and dysprosium are not used, so that the use amount of heavy rare earth elements and the production cost are reduced.

The invention discloses a method for preparing a battery-grade vanadyl sulfate electrolyte by using a vanadium leachate, which comprises the following steps: S1, carrying out anion resin adsorption-desorption treatment and reduction treatment by using the vanadium leachate with the vanadium ion concentration of 1.0-20g / L as a stock solution and using a sulfurous acid solution or a saturated SO2 solution as a desorption solution to obtain a vanadyl sulfate solution with the vanadium ion concentration of 20-40g / L; the method comprises the following steps: sequentially performing extraction and back extraction on a vanadyl sulfate solution with the vanadium ion concentration of 20-40g / L to obtain a vanadyl sulfate electrolyte with the vanadium ion concentration of 80-160g / L; and S3, adsorbing the vanadyl sulfate electrolyte with the vanadium ion concentration of 80-160g / L by using an adsorbent, and filtering to obtain the battery-grade vanadyl sulfate electrolyte. According to the method, the removal of impurities in the vanadium leachate and the efficient reduction conversion and enrichment purification of vanadium ions can be simultaneously / synchronously realized, and the technical effects of improving the product quality, shortening the process flow, improving the production efficiency and reducing the production cost are achieved.

The present invention provides a preparation method of 4,6-dihydroxypyrimidine, and the preparation method comprises the following steps: adding a mixed solution of malonate and formamide to an alkali metal alcoholate / solvent containing a catalyst, and then keeping the mixture warm for reaction after the addition is completed. After the reaction is completed, the solvent is evaporated to dryness, and after being dissolved in water, the mixture is acidified to a pH of 2-3, filtered, washed with water, and dried to obtain 4,6-dihydroxypyrimidine. The present invention utilizes a catalyst to catalyze the reaction, thereby improving the reaction yield, having a high atomic economy, and reducing the amount of raw materials used, reducing the generation of saline wastewater, and alleviating environmental pressure.

The invention relates to the technical field of perovskite quantum dots, in particular to a method for preparing perovskite quantum dots through a normal-temperature solution reaction method. The preparation method comprises the following steps: dissolving a first ligand and a cation precursor in a first solvent, and then diluting with a second solvent to prepare a cation-ligand solution; dissolving a second ligand and lead salt in a first solvent, and then diluting by using a second solvent to prepare a lead salt-ligand solution; and mixing the lead salt-ligand solution with a second solvent, adding the cation-ligand solution under the condition of violent stirring to obtain a reaction system, and then reacting under the condition of normal temperature to obtain the perovskite quantum dots. The perovskite quantum dots can be prepared through a solution reaction method under a normal temperature condition, harsh conditions of a hot injection method and use of a large amount of an anti-solvent of a ligand-assisted precipitation method are avoided, rapid cooling from a high temperature is not needed, the quantum dots can be synthesized without using the anti-solvent, and the preparation method is simple and convenient. The defect that large-scale and large-batch production of the perovskite quantum dots is difficult to realize by the existing synthesis method can be overcome.

The invention relates to the technical field of shearing devices for unmanned aerial vehicle production, in particular to a cutting device and method for unmanned aerial vehicle production. The device comprises a workbench, a cutting disc cutting device body is arranged on the workbench, and a cutting disc is arranged below the cutting disc cutting device body and used for cutting an unmanned aerial vehicle; a water adding device is arranged on the cutting disc cutting device body, a mounting cylinder is further arranged on the workbench and close to the cutting disc, the two sides in the mounting cylinder communicate with a dust suction pipe and an air blowing pipe correspondingly, a second negative pressure fan is arranged at the position, located at the communicating position of the dust suction pipe, in the mounting cylinder, and a water adding pipe communicates with the position, located above the second negative pressure fan, of the mounting cylinder. The water adding pipe is communicated with the water adding device, the second negative pressure fan is used for scattering water sprayed into the mounting cylinder by the water adding pipe, positive pressure generated by the dust suction pipe blows the water to the back of the rotating direction during cutting of the cutting disc, and the temperature of the cutting disc and the cutting position is rapidly reduced through cooperation of the water adding device, the air blowing nozzle and the dust suction cover.

The invention discloses a mine filling cementing material and a preparation method thereof. The mine filling cementing material comprises the following components in percentage by mass: 3-8 wt% of high belite sulphoaluminate cement clinker; 1-3 wt% of high free calcium silicate cement clinker; 74 to 85 wt% of granulated blast furnace slag powder or granulated blast furnace slag; and 10 to 18 wt% of gypsum. Compared with other paste filling materials with the same strength, the cementing material solves the problems that in the prior art, a mine filling cementing material is poor in excitation effect and poor in mechanical property, so that the mine filling effect is affected, and the cost is high due to the fact that the using amount of the cementing material is large, and meanwhile the using proportion is reduced; and the use of mine backfill engineering is fully met.

The invention relates to the field of scavengers, in particular to a copper-based urea crystal scavenger for a vehicle and a preparation method of the copper-based urea crystal scavenger. The automotive copper-based urea crystal scavenger provided by the invention is prepared from the following raw materials: a copper-based catalyst, a surfactant, a foaming agent, a dispersing agent, a reducing pigment and deionized water, wherein the copper-based catalyst comprises copper acetate, the surfactant comprises AEO-10 and MOA-3PK, and the reducing pigment comprises methylene blue; the prepared automotive copper-based urea crystal scavenger is convenient to use, excellent in urea crystal melting effect and short in effective mileage, the environmental protection property of automobile running can be obviously improved after the automotive copper-based urea crystal scavenger is used, and meanwhile the effect of reducing the use cost of an automobile is remarkable.

The invention discloses a supported iron-molybdenum catalyst for formaldehyde production and a preparation method and application thereof, and belongs to the field of catalysts.The catalyst comprises a core-shell structure, the core of the catalyst is a carrier, molybdenum trioxide is supported on the carrier, and the shell of the catalyst is iron molybdate. The carrier is selected from at least one of silicon dioxide, aluminum oxide, titanium oxide, magnesium oxide, magnesium silicate, a molecular sieve, white carbon black and hydroxyapatite; the preparation method comprises the following steps: firstly, loading molybdenum trioxide on a carrier, then dispersing the carrier in deionized water, dropwise adding a molybdenum source solution and an iron source solution in a parallel flow manner under stirring to perform deposition loading of iron molybdate, and performing aging, drying, forming and calcining to obtain the catalyst. The catalyst is used for preparing formaldehyde by oxidizing methanol, dimethyl ether and methylal; according to the catalyst disclosed by the invention, the raw material cost and the pollutant treatment capacity are obviously reduced due to the reduction of the dosage of molybdenum and iron components, and the catalyst has relatively good activity and stability.

The utility model discloses a multi-pass falling film evaporator. An upper port of a barrel is hinged with an upper tube box, and the lower end of the barrel is connected with a lower tube box; a plurality of heat exchange tubes are connected between an upper tube plate and a lower tube plate of the barrel; a plurality of liquid distribution discs which are isolated from one another and integrally spliced into a circle are arranged above the upper tube plate, and liquid distribution holes of each liquid distribution disc are distributed in the periphery of a tube opening of each heat exchange tube below in a regular triangle shape; a plurality of tube pass material inlet tubes are inserted into the dome of the upper tube box, and the lower ends of the tube pass material inlet tubes point to the centers of the corresponding liquid distribution discs respectively; the bottom of the lower tube box is divided into a plurality of liquid collection spaces by partition plates, each pass liquid collection space corresponds to each pass liquid distribution disc, and the lowest part of each pass liquid collection space is connected with a tube pass material outlet tube; an expanding section is arranged on the upper portion of the barrel, a shell pass steam inlet is formed in the circumference of the expanding section, a condensate water outlet is formed in the side wall of the lower portion of the barrel, and a secondary steam outlet is formed in the side wall of the middle section of the lower tube box. The evaporator is small in occupied area, convenient to overhaul, convenient to adjust and good in evaporation quality of thermosensitive media.

The invention discloses a NiCrAl structured catalyst as well as a preparation method and an application method thereof. The catalyst contains NiCrAl layered double hydroxides (NiCrAl-LDHs) and a metal substrate, the NiCrAl-LDHs vertically grow on the surface of the metal substrate in situ, nickel ions, chromium ions and aluminum ions in the NiCrAl-LDHs structure come from the metal substrate, and the preparation method comprises the following steps: dissolving urea in water to prepare a urea aqueous solution; and putting the metal substrate into the urea aqueous solution, and carrying out hydrothermal reaction to obtain the composite material. The application method of the catalyst comprises the following steps: introducing current into the catalyst in a reaction atmosphere, and driving the catalytic reaction by using Joule heat generated by the current. The NiCrAl structured catalyst provided by the invention has the characteristics of simple preparation method, less chemical reagent dosage, excellent catalytic performance, easiness in batch production and the like, and is very suitable for application of electrothermal catalysis.

The invention discloses a method for synthesizing a CHA molecular sieve from coal gangue, and belongs to the technical field of coal chemical materials. The method comprises the following steps: S1, mixing a silicon source, an aluminum source, a template agent I and water to obtain mixed gel I; s2, heating and crystallizing the mixed gel I in the step S1 under a closed condition to obtain a high-activity crystal nucleus II; s3, mixing the high-activity crystal nucleus II in the step S2 with coal gangue, water, a template agent II and an alkali metal source to obtain gel III; s4, heating and pre-crystallizing the gel III in the step S3 under a closed condition to obtain a pre-crystallized product I; and S5, heating and crystallizing the product I in the step S4 under a closed condition to obtain the CHA powder sieve material. According to the method for synthesizing the CHA molecular sieve from the coal gangue, disclosed by the invention, the CHA molecular sieve product can be rapidly synthesized at high yield by using the low-activity coal gangue as a raw material under the condition of low template agent dosage.

The present invention provides the use of organic materials in the preparation of color-changeable polymer materials, and also provides color-changeable polymer materials prepared based on such organic materials and a preparation method thereof, belonging to the technical field of polymer laser processing. The present invention adds a specific organic material as an additive to a polymer to obtain a color-changeable polymer material, and the polymer material has an excellent color-change effect. Under the action of a laser, various color marks can be formed on the polymer material, and the obtained color marks are clear and flat with high contrast. At the same time, the polymer material is light in color, and color marks on light-colored, white or transparent polymer substrates can be realized, expanding the application range of laser color marks. In addition, the amount of organic material used in the color-changeable polymer material of the present invention is small, and the preparation method is simple, easy to operate, safe, and low in energy consumption, which is very suitable for large-scale industrial production.

The invention relates to a migration-resistant anti-aging agent as well as a preparation method and application thereof, the method comprises the following steps: taking a substance as shown in a formula I and nitric acid as reactants, condensing H in an amino para-position group-CH-H and nitryl to obtain a nitrated substance, and carrying out hydrogenation reduction on the nitryl of the nitrated substance under the action of a catalyst to obtain an intermediate product. And carrying out hydrogenation on the intermediate product and ketone under the action of a catalyst to obtain a final product, namely the migration-resistant anti-aging agent II. The raw materials are convenient to purchase and transport, the product yield is high, the cost is low, the operation is simple, and the environmental pollution is small, so that the method has an industrial development prospect. # imgabs0 #