1253results about How to "Reduce dosage" patented technology

The invention discloses a rare-earth metal arylamine group compound as well as preparation method and application thereof. The invention discloses the rare-earth metal arylamine group compound which is characterized in that a general formula of the rare-earth metal arylamine group compound is (2,6-R12PhNH)5LnLi2(THF)2, wherein Ln is a rear-earth metal selected from one of neodymium, samarium, ytterbium or yttrium; R1 is selected from one of hydrogen, methyl or isopropyl. The rare-earth metal arylamine group compound has the advantages that the rare-earth metal arylamine group compound has a definite structure; raw materials used in the preparation method are simple, easily obtained and cheap; the reaction process is simple and easily operated; the rare-earth metal arylamine group compound product is conveniently purified and the yield of the product is high; the rare-earth metal arylamine group compound has a high activity when acting as a single component catalyst to catalyze a hydrogen phosphine reaction of aldehyde or ketone and phosphite ester; the use amount of the catalyst is less; the yield is high; a substrate has wide universality; a new and simple method is provided for synthesis of a-hydroxyphosphonate.

The invention discloses an SNP (Single Nucleotide Polymorphism) molecular marker related to sheep fecundity and application of the SNP molecular marker. The SNP molecular marker comprises an SNP1 (Single Nucleotide Polymorphism) and / or an SNP2; the SNP1 is located at a base at the 115747587 site of a chromosome 6 of a sheep reference genome AR-UIRamV2.0 version, and the polymorphism of the SNP1 is T / G; the SNP2 is located at a basic group at the 41419566th site of a chromosome 22 of a sheep reference genome AR-UIRamV2.0 version, and the polymorphism of the SNP2 is A / G. According to the scheme, the SNP molecular marker related to sheep fecundity is provided, sheep with the high fecundity character can be efficiently and accurately identified and screened out, and the marker is high in typing quality, single in copy and high in polymorphism and can be used for sheep fecundity molecular marker assisted breeding.

The invention relates to a preparation method of soybean oil base polyhydric alcohol, in particular to a method for preparing soybean oil base polyhydric alcohol by directly using soybean oil. The soybean oil diluted by using a solvent reacts with hydrogen peroxide with the weight percentage being 30% for 2-5 hours at the temperature of 60-70 DEG C under catalysis of a catalyst with the weight percentage being 3-5%; vacuum distillation is conducted after the reaction is ended, and the solvent is evaporated; then low alcohol is added in a reactor to be subjected to a reaction for 4-6 hours under the pressure of 0.3-0.4 MPa and at the temperature of 70-80 DEG C, then the reaction is stopped, and the soybean oil base polyhydric alcohol is obtained. The method saves the using amount of hydrogen peroxide, reduces the post-treatment steps, and simplifies the production procedures, and accordingly the product cost is declined directly.

The utility model relates to a prefabricated middle partition wall structure of a tunnel ventilation inclined shaft. The prefabricated middle partition wall structure at least comprises a bottom supporting structure, a steel supporting assembly and a prefabricated modular wallboard. A positioning groove is formed in the top face of the bottom supporting structure, and the bottom of the steel supporting assembly is embedded into the positioning groove and fixed. The prefabricated modular wallboard is formed by splicing a plurality of prefabricated slabs, the adjacent prefabricated slabs are connected through tongue-and-groove structures which are matched in a concave-convex mode, and the tongue-and-groove joints are filled with sealing materials. The steel supporting assemblies are longitudinally arranged at intervals, and the tops of the steel supporting assemblies are fixed to a tunnel lining to form a steel-concrete combined structure for supporting the prefabricated modular wallboard. The steel supporting assembly and the prefabricated modular wall plate form a steel-concrete prefabricated structure, and the stability of the whole structure is enhanced. By adopting the autoclaved aerated concrete precast block material and the concave-convex groove embedded modular structure, the problems that the construction quality is difficult to control, the construction period is long, the on-way resistance of air flow is large and the like in the existing reinforced concrete mid-partition wall are solved.

The invention discloses recombinant escherichia coli with high yield of N-acetylneuraminic acid and application of the recombinant escherichia coli, and relates to the technical field of biological genetic engineering. The invention relates to a recombinant escherichia coli, which is characterized in that the escherichia coli is taken as a host, and free expression of an N-acetylmannosamine epimerase gene yihS from Streptomyces xiamenensis or an N-acetylmannosamine epimerase gene ce3 from Bacteroides polymorpha and an exogenous N-acetylneuraminic acid lyase gene nano A is carried out; and carrying out recombinant expression on N-acetyl hexosamine 1-kinase nahK, a UDP-N-acetyl glucosamine pyrophosphorylase gene glmU and a UDP-N-acetyl glucosamine-2-epimerase gene neuC in the other synthetic route of the ManNAc. According to the recombinant escherichia coli with high yield of N-acetylneuraminic acid, the yield of N-acetylneuraminic acid can reach 23.08 g / L under a shake flask fermentation condition; a two-stage batch feeding strategy is adopted, the yield of N-acetylneuraminic acid in a 5L fermentation tank reaches 71.25 g / L, the molar conversion rate of GlcNAc reaches up to 57.60%, and the method has the potential of industrial application.

The utility model discloses a permanent and temporary combined assembly type underground structure plate wall connecting node which comprises an assembly type underground diaphragm wall, a full-length steel plate is installed on the side wall of the assembly type underground diaphragm wall, and a prefabricated structure plate is hoisted on the full-length steel plate. The gap between the prefabricated structural slab and the fabricated underground diaphragm wall is filled with ultra-high-performance concrete, and a steel bar structure is arranged in the ultra-high-performance concrete. According to the utility model, the rigid connection between the two prefabricated parts is realized, the integrity of the structure is improved, and the safety and durability of the underground structure are fully ensured; an underground diaphragm wall which is usually used as a temporary structure is changed into a permanent structure, so that the construction period is shortened, and the investment is saved; the ultra-high performance concrete poured in the joint can greatly shorten the anchoring length of the steel bars, enlarge the arrangement distance of the steel bars, obviously reduce the using amount of the steel bars on site and the binding workload, is convenient to install and simple in process, obviously improves the construction efficiency, and has high popularization and application value.

The utility model provides a lamp holder light reflecting structure and a lamp. A pull aluminum profile of the device comprises a lamp plate clamping groove for clamping a light emitting unit, a light guide clamping groove for clamping a light guide plate, a radian shaping section for clamping a light reflecting plate and a second light reflecting clamping groove, the radian shaping section and the second light reflecting clamping groove are oppositely arranged at an angle, and the radian shaping section comprises a radian shaping section; when the reflecting plate is clamped and fixed in the radian shaping section and the second reflecting clamping groove, the overall radian is shaped through the arc-shaped shaping section. The lamp panel clamping groove, the light guide clamping groove and the light reflection clamping groove are integrally formed in the drawn aluminum profile, the core components of the lamp panel, the light reflection panel and the light guide plate are all integrated on the drawn aluminum profile made of the metal material, the working performance of the core components of the lamp is guaranteed, only two ends of the light reflection panel are clamped in the clamping grooves, and the bent appearance of the light reflection panel is limited by only one radian shaping section. The structure is simplified, the using amount of aluminum materials is reduced as much as possible, and light weight of the lamp is achieved to the maximum extent.

The invention belongs to the technical field of organic synthesis, and particularly relates to a catalyst-free continuous production method of chlorotert-butane, which comprises the following steps: adding diluted hydrochloric acid as a starting solution into the tower kettle of a reactive distillation tower, and heating the tower kettle to boil until reflux exists at the tower top; the method comprises the following steps: adding tert-butyl alcohol and concentrated hydrochloric acid into a mixing preheater for preheating, then continuously feeding from a feed port of a reactive distillation tower until the tower top temperature is 45-48 DEG C, the side discharge port temperature is 50-52 DEG C and the tower kettle temperature is 96-105 DEG C, and carrying out reflux according to a reflux ratio of (1.5-3): 1; and continuously extracting crude chlorinated tert-butane from a side discharge port of the tower, cooling, neutralizing, drying and filtering to obtain the chlorinated tert-butane. According to the invention, through the integrated design of the mixing preheater and the reactive distillation column, especially by utilizing the reactive distillation technology to continuously remove the product, the chemical equilibrium limitation of the traditional intermittent process is successfully broken, the raw material conversion rate is obviously improved, and meanwhile, the green production targets of flow simplification, energy consumption reduction and three-waste emission reduction are realized.

The present application aims at the problems of excessive consumption of traditional cement limestone resources, excessive energy consumption and high carbon emission, and provides a carbonated hardened low-calcium cement and a preparation and hardening method thereof, which is a hardening method for curing low-calcium cement by CO2 carbonation. The mass percentage composition of cement raw material components is: limestone: 60-70%, sandstone or clay or silica ash: 15-25%, phosphogypsum, fluorogypsum or desulfurization gypsum: 5-25%, component A: 0.5-2%. Component A is composed of the following raw material components in mass percentage: fluorite 0-50%, barium slag: 0-50%, lithium slag 0-50%, wood ash 0-50%, industrial sodium carbonate 0-30%. The composition design of carbonated hardened cement clinker minerals is C2S: 10-90%, C5S2$: 10-90%, C$: 0-5%, C4A3$: 0-10%, etc. In the present application, the limestone required for the cement clinker is lower than that of ordinary Portland cement clinker, the calcination temperature is reduced by 200-350 DEG C than that of ordinary Portland cement clinker, and the energy consumption and carbon emission are significantly lower than those of Portland cement; the low-calcium cement is hardened by CO2 carbonation curing, which can make the cement obtain excellent mechanical properties within 2 hours.

The invention is applicable to the technical field of hemodialyzers, and provides a hollow fiber membrane hemodialyzer with a gradient aperture structure, which comprises a shell, a hollow fiber membrane bundle packaged in the shell, an end cover and a sealing component, the hollow fiber membrane bundle is composed of a plurality of gradient aperture hollow fiber membranes; the hollow fiber membrane is of a two-way gradient aperture structure along the membrane thickness direction; a compact screening layer and a loose transition layer are sequentially arranged on the inner wall of the hollow fiber membrane; a loose diffusion layer and a compact protective layer are sequentially arranged on the outer side of the hollow fiber membrane; the pore diameter of the compact protective layer is not greater than 30nm; the porosity of the hollow fiber membrane is synchronously and progressively increased along with the aperture gradient, the porosity range is 40%-80%, the dialyzer has the characteristics of bidirectional gradient aperture optimization design, gradient functional coating protection, modular adaptation, special-shaped section synergy and the like, and the technical problems that an existing dialyzer is incomplete in toxin removal, insufficient in safety and the like are solved.

The invention belongs to the technical field of high-voltage electric appliance material preparation, and particularly relates to a zinc oxide resistor disc and a preparation method and application thereof. The preparation method comprises the following steps: (1) pre-sintering zinc oxide powder; (2) mixing the zinc oxide powder obtained in the step (1), an auxiliary agent and a dispersion liquid, and carrying out ball milling to obtain slurry; the particle size D50 of the slurry is 0.8-1.2 [mu] m, and the dispersity is greater than or equal to 95%; (3) performing spray drying and granulation on the slurry to obtain granulation powder; (4) carrying out molding and first sintering on the granulated powder to obtain a resistor disc semi-finished product; the first sintering adopts sectional sintering; and (5) forming an electrode layer on at least one surface of the resistor disc semi-finished product by adopting a vacuum sputtering and / or electrophoretic deposition process, and performing secondary sintering and annealing. The contact resistance of the zinc oxide resistor disc is less than or equal to 5m omega; and after 1000 hours of aging in a 85 DEG C + 85% RH environment, the leakage current increase is less than or equal to 2 [mu] A, and the performance degradation rate is less than or equal to 5%.

The application relates to the technical field of tunnel construction, and discloses a combined segment structure, which comprises a UHPC segment and concrete test blocks, a plurality of concrete test blocks are arranged on the outer side surface of the UHPC segment in sequence along the curvature direction of the UHPC segment, the UHPC segment is provided with main reinforcement and stirrups, the main reinforcement is provided with a plurality of strips along the curvature direction of the UHPC segment, a plurality of stirrups are sequentially sleeved on the plurality of main reinforcement and are connected with the main reinforcement through binding, the concrete test blocks are provided with transverse steel bars and longitudinal steel bars, the transverse steel bars extend to the outside of the concrete test blocks and are overlapped with the stirrups, and the longitudinal steel bars extend to the outside of the concrete test blocks and are overlapped with the main reinforcement. Compared with the prior art, the structure design realizes optimal control of material cost by filling the concrete test blocks in the non-key stress area under the premise of hardly sacrificing the core performance of UHPC materials such as strength, durability and stress condition, and effectively eliminates the core economic obstacle in the popularization process of the UHPC shield segment.

This invention discloses a method for installing a grating sensor for wind turbine blade testing, comprising: positioning, marking, surface grinding, cleaning of the bonding surface, ablation treatment of the bonding surface, ablation cleaning of the bonding surface, ablation treatment of the sensor, ablation cleaning of the sensor, surface treatment of the bonding surface, bonding of the sensor, cleaning after bonding, installation of the outer surface protective layer, and fixing and protecting the connecting optical cable. Compared with existing processes, the sensor installed using the method of this invention has a longer service life, shorter installation time, and lower auxiliary material consumption, thereby improving the efficiency of wind turbine blade testing preparation and reducing labor and material costs.

The present application mainly relates to a kind of preparation of sulfur-rich amino acid protein CMd-copper nanoclusters and its detection mercury ion method, comprising: a) by prokaryotic expression obtains CMd protein, and the protein concentration of 5 mg / mL-25 mg / mL CMd protein solution is obtained by purification.b) CMd is reacted with reducing agent TCEP after opening protein disulfide bond.c) the protein solution after reduction is reacted with anhydrous copper sulfate, and preparation high fluorescence CMd-copper nanocluster.d) CMd-copper nanocluster is applied to detect heavy metal mercury ion.The application method can be synthesized under mild aqueous conditions by "one-step method" structure controllable, stable CMd-copper nanocluster, widens the raw material of copper nanocluster synthesized with protein as template, avoids the use of organic solvent and strong reducing agent, and reduces the cost and environmental burden brought by noble metal raw material, and also has higher selectivity to mercury ion.

This invention discloses a support structure and construction method for high-stress tunnels in Class II-III hard rock in the field of initial support technology for tunnel engineering. The tunnel is divided into multiple sections based on each cycle of excavation. These sections include steel-framed sections, which contain steel frames and anchor bolts, and are sealed with shotcrete. There are also non-steel-framed sections, which do not contain steel frames or anchor bolts, but are sealed with shotcrete. The steel-framed and non-steel-framed sections are arranged cyclically along the excavation direction. Multiple anchor bolts in the steel-framed sections are configured obliquely, so that the surrounding rock of the non-steel-framed section corresponds to the anchor bolts of two adjacent steel-framed sections. This changes the traditional steel-frame, full-anchor bolt support mode per cycle to "steel frame, anchor bolts across two cycles," reducing the amount of steel frames and anchor bolts by approximately 50%. The surrounding rock arch effect is fully utilized, using the rigid support points formed by adjacent supported sections to transfer the stress on the middle section of the surrounding rock to both sides, achieving overall stability.

This invention relates to an integrated demolition and construction method for rebuilding a suspension bridge on the same site after demolishing an old rigid frame bridge. The method involves first demolishing the old bridge, then constructing the anchorages, main towers, and side spans of the new suspension bridge, installing the main cables and cable-mounted cranes, and using the cable-mounted cranes to dismantle the closure section of the middle span, the side spans, and the cantilever of the main beam of the middle span of the old bridge, and hoisting the steel box girder of the new suspension bridge. Simultaneously, crawler cranes are used to sequentially dismantle the closure section of the side spans, the cast-in-place section of the side spans, and the side piers of the old bridge. This invention allows for overlapping and simultaneous demolition and construction, which helps shorten the construction period. Utilizing the old bridge deck as a traction platform for the pilot cable of the new suspension bridge across the river does not affect navigation and saves costs. Using the cable-mounted cranes from the new suspension bridge construction for demolition ensures high construction efficiency and safety.

This invention relates to a prefabricated 3D-printed box-type concrete retaining wall and retaining wall system. The prefabricated 3D-printed box-type concrete retaining wall is assembled from 3D-printed concrete retaining wall units. Each 3D-printed concrete retaining wall unit is an integrated 3D-printed concrete structure, consisting of an arched outer wall panel, a concave inner wall panel, and concave side wall panels, which enclose a cavity. A transverse keyway is formed between the concave side wall panels of adjacent 3D-printed concrete box-type retaining wall units. Shear keys are formed by casting cement-based material within the transverse keyway, enabling the combined load-bearing capacity of the 3D-printed concrete retaining wall units. Under the same loading conditions, the peak bearing capacity of the structure of this invention is significantly improved compared to traditional vertical box-type retaining walls, and the bearing performance is further enhanced under simulated backfill conditions, demonstrating good engineering applicability and green construction value.

The present application relates to an antifungal microneedle patch and its preparation method and application, the antifungal microneedle patch includes backing layer and the needle head arranged on the surface of the backing layer;The needle head constitutes n×n array on the surface of the backing layer;The surface of the needle head includes fatty acid coating containing antibacterial drug;The inside of the needle head includes photosensitizer;The n is selected from integer.The antibacterial drug is lipophilic triazole antifungal drug.The fatty acid is selected from saturated fatty acid containing 6-12 carbon atoms.The present application innovatively combines antifungal drug itraconazole and photo-thermal agent / photosensitizer indocyanine green, loads in microneedle, can carry out painless minimally invasive local administration, through the antibacterial action, photo-thermal effect and photodynamic effect of antifungal drug released under the excitation of near-infrared light, realize the effective killing to fungi, and will not cause irreversible damage to normal tissue.

This invention discloses a four-armed star-shaped polymer containing a polyoxyethylene structure, its preparation method, composition, and applications. The polymer is prepared by mixing an unsaturated organic carboxylic acid compound, an unsaturated sulfonic acid compound, and water, stirring to obtain a reaction solution, and continuously stirring and heating the reaction solution. An aqueous solution of a polyether macromonomer compound and the initiator aqueous solution are added to the heated reaction solution, followed by polymerization and purification. The polymer structure contains a large number of carboxyl groups, sulfonic acid groups, and ether groups, as well as abundant polyoxyethylene groups and alkyl chains, giving the polymer good water solubility and excellent chelating properties for metal ions. The polymer prepared by this method shows good effects in cleaning, defoaming, and scale inhibition. Furthermore, compositions formed by combining the polymer with other corrosion and scale inhibitors exhibit good compatibility and can be used for scale inhibition in high-hardness water.

The utility model discloses a kind of multi-pass solenoid valve with power connection plate, comprising: multiple valve bodies and power connection plate, each valve body has a pair of same direction projecting insert, the power connection plate includes: multiple metal sheets for the conductive connection of the insert and power supply, and plastic layer covering the metal sheet, the metal sheet has wiring end connected with power supply and insert connection plug-in end, the plastic layer exposes the wiring end and the plug-in end, characterized in that, between adjacent two metal sheets, there is the bending part formed by punching cutting, the plastic layer is provided with at least part recess of covering the bending part, to prevent the rebound of bending part, thereby avoid the short circuit problem that multi-pass solenoid valve appears when working.

The invention relates to a high-impact PC-elastomer composite battery shell and a preparation method thereof, and belongs to the technical field of battery shell manufacturing. The shell adopts a three-layer composite structure design and comprises an outer polycarbonate layer of which the end group is grafted with a hindered amine light stabilizer, a middle thermoplastic polyurethane layer containing a double-crosslinking network and an inner glass fiber reinforced polycarbonate layer. Through material modification, uniform distribution and dense combination of all layers of materials are realized, the impact resistance and the weather resistance of the battery shell are remarkably improved, and the excellent bonding property of an interface is ensured.

This utility model discloses an integrated transition yaw connection system for wind turbines, belonging to the technical field of wind power generation equipment. The system includes a wind turbine tower, a slewing bearing, a short-section cylinder, and a lower platform. The wind turbine tower has a truss-type hollow structure. The short-section cylinder is vertically arranged and its top is welded to the lower platform as a whole. Its bottom is connected to the top of the tower through the slewing bearing. This utility model uses a hierarchical structure of truss tower-slewing bearing-short-section cylinder-platform. It utilizes the short-section cylinder to distribute the nacelle load and compensate for installation errors. Combined with the slewing bearing, it achieves low-friction and stable yaw. This structure effectively solves the problems of heavy self-weight, obvious yaw vibration, complex assembly, and easy wear of connection parts of traditional wind turbine towers. It has the advantages of lightweight, stable yaw, convenient installation, and long service life.

The application relates to a motor rotor, comprising a rotor support and a plurality of magnet units, the rotor support comprising a support ring, the support ring having a first ring surface and a second ring surface in the thickness direction, the plurality of magnet units being arranged at intervals along the circumferential direction of the first ring surface, the first ring surface being provided with a first annular taper surface, each magnet unit having a first magnetic surface and a second magnetic surface in the thickness direction, the first magnetic surface being provided with a first magnetic taper surface, the first magnetic taper surface being matched with the first annular taper surface, wherein the thickness of the support ring at the first annular taper surface part gradually decreases in the direction from the ring center to the ring outer edge, and the thickness of the magnet unit at the first magnetic taper surface part gradually increases in the direction from the ring center to the ring outer edge. The application also relates to an axial motor. The use amount of permanent magnet material is reduced, and cost is saved.

The application provides an asynchronous flotation enrichment method and application based on quartz and feldspar. The asynchronous flotation enrichment method comprises the following steps: S1, providing a to-be-processed ore material containing quartz and feldspar; S2, adding a tertiary amine cationic collector and then adding an anionic collector in the presence of a feldspar depressant, and then performing quartz flotation on the ore material to obtain a first feldspar and quartz rough concentrate; and S3, performing feldspar flotation on the quartz rough concentrate by using a feldspar combined collector in the presence of a feldspar activator and a quartz depressant to obtain a second feldspar and quartz concentrate. In the quartz flotation, the combination of the tertiary amine cationic collector and the anionic collector can realize the pre-enrichment of the quartz under neutral conditions; meanwhile, the pre-enrichment of the quartz reduces the feldspar content of the to-be-processed ore slurry in the feldspar flotation, and the use amount of the feldspar activator can be effectively reduced, so that the feldspar flotation under weakly acidic or neutral conditions is realized.

The application discloses a comb-shaped long-chain alkyl copolymer asphalt inhibitor and a preparation method and application thereof. First, octadecyl methacrylate, maleic anhydride and styrene are used for copolymerization, and then an amide reaction of the copolymer and tetradecylamine or octadecylamine is carried out to obtain the comb-shaped long-chain alkyl copolymer asphalt inhibitor. The inhibitor has an inhibition rate of greater than 95%, raw materials are easy to obtain, reaction conditions are mild, and the inhibitor is suitable for large-scale production. The preparation method only needs two-step conventional reactions, and high pressure and special purification equipment are not needed.

The application belongs to the technical field of proton exchange membrane fuel cell, and relates to a hydrophobicity-adjustable alloy nanotube array electrode for fuel cell and preparation and application thereof. Specifically, the application comprises preparation of metal nanotube array, alloying and hydrophobization of the metal nanotube array, and assembly of the membrane electrode. First, a metal nanotube array is constructed on a substrate surface through a two-step hydrothermal method; then, a hydrophobic substance is introduced into the metal nanotube array by means of immersion or ultrasonic spraying; then, pyrolysis is performed to realize alloying and hydrophobization of the nanotube array; finally, the nanotube array is transferred to a proton membrane, and the membrane electrode is cleaned. The membrane electrode can be applied to a proton exchange membrane fuel cell. The hydrophobicity-adjustable nanotube array electrode prepared by the application has the advantages of high catalyst activity and stability, low platinum loading, good water management, and easy scaling-up.

The application discloses a method for preparing non-spherical nano-silica particles by self-assembly induction, which comprises synthesis of silica particle seeds and further growth of the seeds: by preparing monodispersed seed particles, trace amounts of amphoteric electrolytes are added into the seed growth solution to induce anisotropic growth of the seeds, the types and proportions of the electrolytes are adjusted to make the monodispersed seeds generate silica sol of non-spherical silica particles with different morphologies, and then a series of post-treatments such as water replacement solvent, filtration and concentration are conducted to obtain non-spherical ultra-high-purity silica sol with a mass fraction of more than 18%, a primary particle size of 40-80 nm and a morphology of peanut-shaped, short-chain-shaped and long-chain-shaped, etc. The application also relates to the non-spherical ultra-high-purity silica sol and application thereof in CMP. The preparation method of the application adopts a self-assembly mode of monodispersed seeds to prepare non-spherical particles, and the particle morphology can be further adjusted by adjusting the dosage or types of the self-assembly induction agent.

The application relates to the field of thermal catalysis, and discloses a method for preparing 1-cyclohexylbenzene hydrogen peroxide by solvent-free thermal catalytic selective oxidation of cyclohexylbenzene with molecular oxygen. The method uses a metal bromide as a catalyst, azobisisobutyronitrile or t-butyl hydroperoxide as an initiator, and pure oxygen as an oxidant, and can effectively selectively oxidize cyclohexylbenzene (CHB) into 1-cyclohexylbenzene hydrogen peroxide under normal pressure, solvent-free conditions and at a temperature above 90 DEG C. The catalytic system has the advantages of low cost, simple operation process, high catalytic oxidation efficiency and high selectivity of the target oxidation product.

The application discloses a composite catalyst for chemical flow casting preparation of a polyimide film and a method for preparing the polyimide film. After a polyamide acid composition is flow cast on a support to form a gel film, the polyimide film is prepared through high-temperature curing. The polyamide acid composition is uniformly mixed at normal temperature from a polyamide acid solution, a polar aprotic solvent, an imidization composite catalyst, a thermal latent catalytic type blocking agent and a dehydrating agent. The imidization composite catalyst is compounded from two types of imidization catalysts with high activity and low activity respectively. The application develops a normal-temperature (16 DEG C to 35 DEG C) chemical flow casting preparation method of a PI film by adopting the imidization catalysts with high catalytic activity and low activity to prepare the composite catalyst. Compared with a traditional low-temperature chemical flow casting method, the manufacturing energy consumption and manufacturing cost are greatly reduced.

The utility model provides a kind of immersion battery pack and cooling system belong to new energy battery field.The battery pack includes battery module and box, multiple flow channel plates are provided in the box, multiple flow channel plates are arranged at intervals, one end of flow channel plate is in abutment with the inner wall of box, and the other end is provided with electric core insulation sealing plate, battery module is arranged between two adjacent flow channel plates, one end of battery module is in abutment with the inner wall of box, and the other end is in abutment with electric core insulation sealing plate.A kind of immersion battery pack and cooling system provided by the utility model embodiment can solve the problem of large amount of immersion liquid and inconvenient installation in the prior art.