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585results about How to "Increase polarity" patented technology

Modification method of PVDF (Polyvinylidene Fluoride) separation membrane

The invention discloses a modification method of a PVDF (Polyvinylidene Fluoride) separation membrane, and belongs to the technical field of water treatment. The modification method provided by the invention comprises the step of impacting the PVDF separation membrane by adopting high-pressure liquid, so that high-pressure micro-droplets are in high-speed friction with the surface of the PVDF separation membrane. According to the modification method provided by the invention, the hydrophilicity, the surface potential and the dye retention rate of the PVDF separation membrane can be effectively improved.
Owner:WUYI UNIV

Biodegradable hot melt adhesive based on castor oil and rosin resin and preparation process thereof

The invention relates to the field of hot melt adhesives, and discloses a biodegradable hot melt adhesive based on castor oil and rosin resin and a preparation process thereof, the biodegradable hot melt adhesive comprises EVA resin, modified castor oil, rosin resin, a modified additive, a lubricant and an antioxidant; the modified castor oil is prepared by crosslinking castor oil and isophorone diisocyanate and reacting lignin, 1, 4-butanediol and isocyanate groups; the modified castor oil and the modified additive are added, the modified castor oil and the modified additive are added, the modified castor oil and the modified additive are added, the modified castor oil and the modified additive are added, the modified castor oil and the modified additive are added, the modified castor oil and the modified additive are added, and the modified castor oil and the modified additive are added, so that the modified castor oil and the modified additive are added, and the modified castor oil and the modified additive are added; the tensile property and the adhesive property of the hot melt adhesive are improved, and meanwhile, the flame retardant property and the high and low temperature resistance of the hot melt adhesive can be improved.
Owner:FOSHAN BENJIA NEW MATERIAL TECH CO LTD

Anticorrosive Teflon coating as well as preparation method and application thereof

The invention provides an anti-corrosion Teflon coating as well as a preparation method and application thereof, and belongs to the technical field of coatings. The preparation method comprises the following steps: irradiating polytetrafluoroethylene micro-powder, performing graft modification on the irradiated polytetrafluoroethylene micro-powder and glycidyl methacrylate, reacting with phosphorus oxychloride and polydopamine modified graphene, adding into a Teflon primer, and uniformly stirring and mixing to obtain the anti-corrosion Teflon coating. The anti-corrosion Teflon coating prepared by the invention has good high-temperature resistance, corrosion resistance, rust resistance, mechanical properties, wear resistance, scratch resistance, medium resistance and the like, can effectively resist high-wear-resistance environments such as sliding friction, impact friction and cavitation friction and high-corrosion environments such as acid media and alkaline media, and has a wide application prospect.
Owner:SHANGHAI KIINERING IND & TRADE CO LTD

Ceramic tile with golden velvet texture and raw stone duplicating effect and preparation method of ceramic tile

The invention relates to the technical field of ceramics, and discloses a ceramic tile with a golden velvet texture and a recarved raw stone effect and a preparation method of the ceramic tile. The ceramic tile comprises a green body layer, a cover glaze layer, a pattern texture layer, a digital deep ink layer and a dry granular glaze layer which are sequentially arranged from bottom to top, the digital deep ink layer is composed of digital matte deep ink; the dry granular glaze layer is composed of dry granular glaze; a surface tension difference is formed between the digital matte deep ink and the dry granular glaze. By improving the digital matte deep ink, the digital matte deep ink can be combined with the dry granular glaze, and a matte three-dimensional non-collapse effect is formed on the glaze surface; the dry granular glaze is improved, so that the dry granular glaze has better physical properties; through the improvement of the suspending agent, the suspending agent can generate relatively strong combining capacity with dry particles, so that the dry particle glaze has relatively strong polarity, and can form enough repulsive force when being combined with digital matte deep ink with strong hydrophobicity, so as to form a finer and three-dimensional concave-convex fluctuating effect.
Owner:GUANGDONG NEWPEARL CERAMIC GRP CO LTD +2

Composite solid electrolyte diaphragm, preparation method and lithium ion battery

ActiveCN119542675AImprove liquid absorption capacityeffective migrationSecondary cellsCell component detailsSolid state electrolyteElectrical battery
The invention discloses a composite solid electrolyte diaphragm which comprises a bacterial cellulose membrane, fluorinated metal modified PEO electrolyte particles and functional group modified particles, and the fluorinated metal modified PEO electrolyte particles and the functional group modified particles are loaded in a three-dimensional network structure of the bacterial cellulose membrane. The functional group modified particles are functional group modified silicon dioxide particles and functional group modified LATP particles, the functional group modified silicon dioxide particles uniformly wrap the functional group modified LATP particles, and fluorinated metal of the fluorinated metal modified PEO electrolyte particles is combined with functional groups of the functional group modified particles through coordinate bonds. The invention also discloses a preparation method of the electrolyte diaphragm and a battery with the electrolyte diaphragm. The ionic conductivity of the electrolyte diaphragm is improved.
Owner:CHANGSHU INSTITUTE OF TECHNOLOGY

Mildew-proof modified starch-based super absorbent resin as well as preparation method and application thereof

The invention belongs to the technical field of materials, and discloses mildew-proof modified starch-based super absorbent resin as well as a preparation method and application thereof. The mildew-proof modified starch-based super absorbent resin is prepared from the following raw materials in parts by mass: 10 to 20 parts of modified carboxymethyl starch, 2 to 3 parts of quaternized carboxymethyl chitosan, 10 to 15 parts of 2-acrylamido-2-methylpropanesulfonic acid, 15 to 25 parts of acrylamide, 100 parts of acrylic acid, 0.4 to 0.7 part of a redox initiator and 0.05 to 0.15 part of a cross-linking agent. According to the invention, the inherent defects of low mechanical strength, poor salt tolerance, poor stability, easy decomposition, short service life and the like of the starch-based resin are obviously improved, so that the starch-based super absorbent resin with good mildew resistance and more excellent performance can be developed.
Owner:GUANGDONG UNIV OF TECH +1

Halogen-free flame-retardant environment-friendly heat-resistant cable and preparation method thereof

The invention discloses a halogen-free flame-retardant environment-friendly heat-resistant cable and a preparation method thereof, belongs to the technical field of cable material processing, and is used for solving the technical problem that the mechanical strength and heat resistance of a halogen-free flame-retardant environment-friendly cable in the prior art need to be further improved. The cable comprises a plurality of cable conductors, a wrapping layer and a sheath layer which are sequentially arranged from inside to outside, and the sheath layer comprises the following components in parts by weight: 70-80 parts of low-density polyethylene, 20-30 parts of modified polysiloxane, 10-16 parts of modified polyvinyl alcohol, 15-18 parts of modified kaolin, 2-3 parts of an initiator and 3-4 parts of an auxiliary additive. Low-density polyethylene is reinforced and modified through modified kaolin, modified polyvinyl alcohol and modified polysiloxane, so that not only are the mechanical strength and flame retardance of the environment-friendly heat-resistant cable effectively improved, but also the high-temperature resistance of the cable is improved, and the service life of the cable in a high-temperature environment is prolonged.
Owner:广东广缆电缆实业有限公司

Composite electrolyte, lithium metal battery and application of lithium metal battery

The invention relates to the technical field of batteries, in particular to a composite electrolyte, a lithium metal battery and application of the lithium metal battery. The invention relates to a composite electrolyte which comprises a fluorinated cyclic ether solvent, an alkane solvent, LiPF6 and LiTFSI, the carbon atom number Ra of the fluorinated cyclic ether solvent skeleton is more than or equal to 3 and less than or equal to 6; the volume ratio A of the fluorinated cyclic ether solvent is greater than or equal to 50% and smaller than or equal to Alt; 100%; the volume ratio B of the alkane solvent meets 0 lt; b < = 50%; the structural tortuosity Rb of the hydrocarbon solvent satisfies 1.5 < Rb < = 3; the ratio of the molar concentration Rc of LiPF6 to the molar concentration Rd of LiTFSI is more than 0 and less than or equal to 1. The composite electrolyte provided by the invention has excellent comprehensive physical and chemical properties, especially low-temperature performance, and can improve the cycle performance and rate capability of the battery.
Owner:SVOLT ENERGY TECHNOLOGY CO LTD

Windproof breathable composite fabric and application thereof

The invention discloses a windproof and breathable composite fabric and application thereof. The windproof and breathable composite fabric is used for solving the technical problem that in the prior art, the windproof and breathable performance, the wear-resistant and antistatic performance and the washing resistance of a polyester fiber fabric need to be further improved. The preparation method comprises the following steps: putting a gray fabric into a pretreatment solution for pretreatment to obtain a pretreated gray fabric, taking modified quaternary ammonium salt as a cross-linking agent, promoting cross-linking of a polyurethane prepolymer co-blocked by modified polysiloxane and polyethylene glycol, preparing epoxy group-terminated modified polyurethane, and carrying out heat treatment to obtain the pretreated gray fabric. The modified polyurethane and the tetrabutyl titanate are dispersed and mixed in the alkaline emulsion, and the prepared finishing liquid is used for padding and modifying the pretreated gray fabric, so that the windproof and moisture-permeable performance of the composite fabric is effectively improved, and the antistatic performance, wear resistance and pilling resistance of the composite fabric are also improved.
Owner:BIEM L FDLKK GARMENT CO LTD

Primary amino modified solution polymerized styrene-butadiene rubber and preparation method thereof

The invention provides primary amino modified solution polymerized styrene-butadiene rubber and a preparation method thereof. The preparation method comprises the following steps: in a polymerization system, initiating polymerization of a butadiene monomer and a styrene monomer by taking n-butyllithium as an initiator and tetrahydrofuran as a polymerization activator to obtain a styrene butadiene rubber active chain; adding a diisocyanate compound into the polymerization system to terminate polymerization, and introducing an isocyanate group to the end part of a styrene butadiene rubber active chain to obtain a styrene butadiene rubber solution; and adding a terminator into the styrene-butadiene rubber solution, stirring, separating out precipitate, and drying to obtain the primary amino modified solution polymerized styrene-butadiene rubber. The primary amino modified solution polymerized styrene-butadiene rubber is prepared by the preparation method, has high polarity and strong binding force with silicon dioxide filler, promotes generation of a more stable filler-polymer network with a more perfect structure, and remarkably improves the dynamic performance of a rubber material.
Owner:ZHONGZHE (ZHEJIANG) POLYMER NEW MATERIALS CO LTD

Preparation method of high-concentration heteroatom-doped mesoporous carbon nanotube material and application of high-concentration heteroatom-doped mesoporous carbon nanotube material in lithium-sulfur battery

The invention provides a preparation method of a heteroatom-doped mesoporous carbon nanotube material and application of the heteroatom-doped mesoporous carbon nanotube material in a lithium-sulfur battery. The preparation method comprises the following steps: S1, preparing a polyphosphazene nanotube by utilizing a self-template method; s2, preparing PZS coated SiO2 by adopting a sol-gel method; s3, NPS-C coated SiO2 is prepared through carbonization; and S4, adding the NPS-C-coated SiO2 powder into an etching solution, stirring, centrifuging, washing, and finally performing vacuum drying at room temperature to obtain the NPS-C material. The NPS-C obtained by carbonizing the precursor prepared on the basis of a self-template method and a sol-gel method has excellent conductivity, the mesoporous hollow structure can be used as a sulfur species packaging framework to inhibit large volume fluctuation in the circulation process, heteroatoms can adsorb and fix polysulfide to effectively inhibit the shuttle effect, and the performance of the NPS-C is improved. And a new thought is opened up for exploration and design of the high-performance electrode material of the lithium-sulfur battery.
Owner:HARBIN INST OF TECH ZHENGZHOU RES INST

Method for preparing high-purity 2, 6-naphthalic acid by oxidizing 2, 6-diisopropylnaphthalene

The invention relates to a method for preparing high-purity 2, 6-naphthalic acid by oxidizing 2, 6-diisopropyl naphthalene. The method comprises the following steps: adding 2, 6-diisopropylnaphthalene, a catalyst, a solvent and an additive into a titanium reaction kettle, uniformly mixing, introducing nitrogen to remove oxygen, raising the temperature in the titanium reaction kettle to 150-220 DEG C, and introducing nitrogen to ensure that the pressure in the titanium reaction kettle is 0.5-1 MPa; the solvent is a mixture containing acetic acid and water; pure oxygen is introduced into the titanium reaction kettle, so that the pressure in the titanium reaction kettle is increased to 2.4-3.2 MPa, the reaction system reacts for 1-3 h under the condition that the pure oxygen is continuously introduced, and 2, 6-naphthalic acid is prepared; the 2, 6-naphthalic acid prepared by the method has the advantage of high purity.
Owner:BEIJING UNIV OF CHEM TECH

Novel coronavirus SARS-CoV-2 mutant vaccine and application

The invention relates to a novel coronavirus SARS-CoV-2 mutant vaccine and application, the vaccine comprises a fusion protein, and the fusion protein comprises: (1) interferon or a functional fragment thereof; (2) a novel coronavirus SARS-CoV-2Omicron mutant strain S protein or a functional fragment of the novel coronavirus SARS-CoV-2Omicron mutant strain S protein; and (3) an immunoglobulin Fc region. Molecule and process optimization of the fusion protein comprises improvement of process developability and immunogenicity, and the vaccine can improve immunogenicity and antibody titer of a mutant new crown antigen through convergence mutation design, efficiently generate a neutralizing antibody, significantly improve defense ability to a variant strain, and can be massively and industrially produced.
Owner:LIVZON MABPHARM

Polytetrahydrofuran-nanocellulose toughened and reinforced epoxy resin and preparation method thereof

The invention relates to the technical field of epoxy resin, and discloses polytetrahydrofuran-nanocellulose toughened and reinforced epoxy resin, nanocellulose has a high length-diameter ratio and can play a stress transfer role in an epoxy resin matrix, and a polytetrahydrofuran molecular chain is introduced, so that the polarity of the nanocellulose is improved, and the toughness of the epoxy resin is improved. Compared with the prior art, the nano-crystalline cellulose has the same chain segment as carboxyl-terminated polytetrahydrofuran participating in curing, so that the nano-crystalline cellulose has better compatibility and can form good dispersity in a matrix, and an active carboxylic acid methyl ester group is introduced to a molecular chain of polytetrahydrofuran, so that the molecular chain of polytetrahydrofuran is introduced to the surface of the nano-crystalline cellulose, and the nano-crystalline cellulose is prepared. A polytetrahydrofuran molecular chain contains a flexible chain segment, so that the polytetrahydrofuran has a very good toughening effect, the rigidity of the epoxy resin is reduced, and the epoxy resin has more excellent mechanical properties under the synergistic toughening action of the nanocellulose and the polytetrahydrofuran.
Owner:LINZHANG COUNTY QIAOZHOU TECHNOLOGY CO LTD

Air-drying impact-resistant protective coating and preparation method thereof

The invention relates to the technical field of coating preparation, and discloses a self-drying impact-resistant protective coating and a preparation method thereof. The invention discloses a self-drying impact-resistant protective coating. Comprising the following components: acrylic resin, epoxy resin, modified polyurethane emulsion, glyceryl stearate, a styrene-butadiene-styrene block copolymer, modified tackifying resin, deionized water, ethylene glycol tert-butyl ether, ethanol, an organic silicon defoaming agent, an organic silicon flatting agent and an impact modifier methyl methacrylate-butadiene-styrene copolymer. The coating is prepared from polyurethane elastomer particles, organic bentonite, black paste and isocaprylic acid. The self-drying impact-resistant protective coating disclosed by the invention not only has excellent mechanical property, impact resistance, corrosion resistance, wear resistance and ultraviolet resistance, but also has self-healing property and antibacterial property.
Owner:YANCHENG TIANYI SEALING MATERIAL CO LTD

Ketoxime ester photoinitiator, application thereof and photosensitive composition

The invention belongs to the technical field of photoinitiators, and particularly relates to a ketoxime ester photoinitiator as well as application and a photosensitive combination thereof. Compared with the prior art, the novel photoinitiator has the advantages that by introducing a sulfone phenyl specific structure to a ketoxime ester group and the like, excellent photosensitivity can be shown in the optical wavelength range of 280-400 nanometers, and compared with OXE-01 and OXE-02 commonly used in the market, the novel photoinitiator can show better photoinitiation efficiency under an ultraviolet visible (UV-Vi s) LED light source.
Owner:WUHAN SUNSHINE OPTOELECTRONICS TECH CO LTD

Base film for composite current collector and preparation method of base film

The invention discloses a base membrane for a composite current collector and a preparation method of the base membrane, and belongs to the technical field of current collectors for lithium batteries. Comprising two polymer polar material layers and a polymer reinforcing material layer located between the two polymer polar material layers. The polymer polar material layer comprises polyolefin, a polar polymer material, an amphoteric material and an antioxidant; the polymer reinforced material layer comprises polyolefin, a reinforced material and an antioxidant; the base film for the composite current collector is of a sandwich structure composed of the polymer polar material layer, the polymer reinforcing material layer and the polymer polar material layer, the performance of the edge layer and the performance of the core layer can be considered to the maximum extent, good temperature resistance, tensile strength and electrolyte resistance are achieved, the safety of a device is improved on the whole, and the service life of the device is prolonged. And the current collector development trend is met.
Owner:四川东方绝缘材料股份有限公司

A kind of polyurethane-polyurea aqueous dispersion and its preparation method and application

The present invention provides a highly elastic polyurethane-polyurea aqueous dispersion and a preparation method and application thereof, wherein the polyurethane-polyurea aqueous dispersion comprises a combination of chain extenders such as polyether polyol, polyester polyol and triazole. The soft elastic product prepared based on the polyurethane-polyurea aqueous dispersion provided by the present invention has elasticity and chemical resistance comparable to latex gloves.
Owner:WANHUA CHEM GRP CO LTD

Preparation method and application of bifunctional acrylate monomer modified polypropylene coarsening film for extremely cold-resistant oil-immersed capacitor

The invention discloses a preparation method and application of a bifunctional acrylate monomer modified polypropylene coarsening film for an extremely cold-resistant oil-immersed capacitor, and belongs to the technical field of manufacturing of electronic and electrical insulating materials. The invention relates to application of a bifunctional acrylate monomer modified polypropylene coarsened film in an extremely cold resistant oil-immersed capacitor or a thin film capacitor. The preparation method comprises the following steps: (1) respectively adding a polypropylene coarsened film, a monomer, an interface agent, a co-monomer, an initiator and deionized water in certain parts by weight into a reactor, and heating for swelling; (2) heating the reaction system to a certain temperature, and carrying out grafting reaction; and (3) washing, extracting and drying. According to the invention, the bifunctional acrylate is used as a monomer to carry out long-chain branching modification on the polypropylene coarsened film, so that the problem of poor performance of a capacitor in an extreme environment caused by low-temperature embrittlement and high-temperature insulation deterioration of the polypropylene coarsened film is solved. The method has the advantages of good effect, environmental protection, simple process, low cost and the like.
Owner:HARBIN UNIV OF SCI & TECH +6

Paraffin removing and inhibiting agent for oil well shaft and preparation process of paraffin removing and inhibiting agent

The invention relates to the technical field of oil well paraffin removal and prevention, and discloses a paraffin removal and prevention agent for an oil well shaft and a preparation process. The paraffin remover and inhibitor for the oil well shaft comprises the following components in parts by weight: 10-25 parts of a compound surfactant, 15-30 parts of a mutual solvent, 5-10 parts of a stabilizer, 1-10 parts of a novel wax crystal improver, 0.2-0.5 part of a rapid penetrant, 0.5-1.5 parts of alkali and 25-70 parts of water, the novel wax crystal improver has a structure similar to that of paraffin, and wax crystals can be dissolved in the novel wax crystal improver, so that the wax crystals are not easy to gather and deposit on a pipe wall, and the dissolution rate of the wax crystals is further improved; sodium sulfonate in the structure has strong polarity and hydrophilicity, can adjust the crystallinity of paraffin inhibitor molecules, has a synergistic effect with asphalt, colloid and the like in crude oil, reduces the surface tension of water, has a good wetting effect, and improves the low-temperature fluidity of the crude oil.
Owner:XIAN HETAI CHEM CO LTD

Photopolymer system based on fluorine-containing liquid crystal, grating device and preparation method of grating device

According to the photopolymer system based on the fluorine-containing liquid crystal, the grating device and the preparation method of the grating device, the mixed liquid crystal containing the nematic liquid crystal and the fluorine-containing liquid crystal at the same time is adopted in the photopolymer system, and therefore the polarity and dielectric anisotropy of the mixed liquid crystal material are improved; the overall electro-optical performance, uniformity and stability of the photopolymer system are improved, so that a grating device prepared based on the photopolymer system has good optical characteristics of low haze while having relatively high diffraction efficiency. Specifically, fluorine-containing biphenyl liquid crystals, fluorine-containing alkyne liquid crystals and fluorine-containing difluoromethoxy liquid crystals of which the carbon atoms of flexible side chains are 2-5, and nematic liquid crystals of which the delta epsilon is not less than 10 are selected to jointly form mixed liquid crystals; and the balance and optimization between the diffraction efficiency and haze performance of the photopolymer system and the grating device prepared from the photopolymer system are realized.
Owner:NIKA OPTICS (TIANJIN) CO LTD

Integrally-formed multifunctional shoe sole and preparation method thereof

The invention discloses an integrally-formed multifunctional shoe sole and a preparation method thereof, and belongs to the field of shoe products, the method comprises the following steps: carrying out primary ejection on a first insole material and a second insole material by adopting double-color ejection equipment to obtain an insole parison; in the first insole material, an ethylene-vinyl acetate copolymer, an ethylene-butyl acrylate copolymer, random polyolefin, a styrene-butadiene-styrene block copolymer and an ethylene-butyl acrylate-maleic anhydride copolymer are used as matrix resin; carrying out molding and mold pressing on the insole blank and the laminated sheet rubber, so that the insole blank is foamed and crosslinked at a high temperature, and meanwhile, the sheet rubber is vulcanized and crosslinked at the same temperature; the coated raw rubber sheet is a mixed rubber sheet mainly taking rare earth butadiene rubber, natural rubber, polyacrylate rubber and brominated butyl rubber as main bodies. According to the invention, double-color sole foaming cross-linking and raw rubber vulcanization are integrally combined and molded, the process is simplified, the cost is reduced, and the production environment is improved.
Owner:ANTA (CHINA) CO LTD

Analysis method for measuring content of dihydroergoline mesylate bulk drug

The invention relates to the technical field of drug analysis, and particularly discloses an analysis method for measuring the content of a dihydroergoline mesylate bulk drug, which comprises the following steps: step S1, adding the dihydroergoline mesylate bulk drug into anhydrous acetonitrile to obtain a stock solution to be measured, precisely measuring 1mL of the stock solution, adding a cosolvent, uniformly shaking, and fixing the volume to obtain a solution to be measured; s2, taking a dihydroergoline mesylate raw material medicine, adding the dihydroergoline mesylate raw material medicine into anhydrous acetonitrile to obtain a control stock solution, precisely measuring 1mL of the control stock solution, adding a cosolvent, uniformly shaking, and fixing the volume to obtain a control solution; s3, measuring the content of the dihydroergoline mesylate raw material medicine by using a high performance liquid chromatography; according to the present invention, the cosolvent contains the 1-butyl-3-methylimidazole tosilate, the mobile phase of the high performance liquid chromatography contains the elution reinforcing agent, and through the reasonable ratio of the components, the solubility of the dihydroergoline mesylate can be improved, and the accuracy of the high performance liquid chromatography analysis can be improved.
Owner:宝利化(南京)制药有限公司

Preparation process of modified non-woven fabric produced by recycled PP meal box broken pieces

The invention discloses a preparation process of a modified non-woven fabric produced by utilizing recycled PP meal box broken pieces, and belongs to the technical field of non-woven fabrics, the process comprises the following steps: firstly, sorting, cleaning and screening the recycled PP meal box broken pieces, and then mixing the recycled PP meal box broken pieces with a modification enhancer for later use; conveying the prepared raw materials to a screw extruder by adopting a spiral feeder, and carrying out melt extrusion; extruding the melt through a spinneret plate, carrying out spinning molding, cooling and solidifying the fiber through a cooling device, and laying to form a continuous fiber net; finally, the fiber net is reinforced in a drafting and heat bonding mode, the non-woven fabric with the needed physical performance is formed after net laying, and heat treatment and calendaring treatment are conducted. According to the preparation process, the waste PP meal box is effectively utilized, the use of original PP is reduced, the production cost is reduced, meanwhile, the environmental pollution is reduced, and the preparation process has remarkable economic and social benefits.
Owner:SHANGHAI RE-POLY ENVIRONMENTAL PROTECTION TECH CO LTD

Method for synthesizing and purifying electronic-grade diborane

The invention discloses a synthesis and purification method of electronic-grade diborane, and relates to the technical field of diborane synthesis, and the synthesis and purification method has the advantages that cation 1-ethyl-3-methylimidazole in ionic liquid has a relatively large volume and a specific spatial configuration; the ionic liquid can be close to reactants sodium borohydride and hydrogen through intermolecular force, meanwhile, the anion bis (trifluoromethanesulfonyl) imide salt has high polarity and can attract reactant molecules with opposite charges, so that the ionic liquid makes full contact with the reactants, sulfolane has high dissolving capacity and can well dissolve sodium borohydride and hydrogen, and the ionic liquid can be separated from the reactants. Sodium borohydride and hydrogen are uniformly distributed in a mixed solvent, the sodium borohydride and hydrogen are efficiently reacted at proper temperature and pressure to generate high-purity diborane under the synergistic effect of the sodium borohydride and the hydrogen, sufficient contact of reactants is ensured by timely stirring in the reaction process, the reaction efficiency and the diborane yield are greatly improved, and the yield of the diborane is increased. And favorable conditions are created for subsequent preparation of electronic-grade diborane.
Owner:HEFEI XIANWEI SEMICON MATERIAL CO LTD

Method for removing trace acetone in high-purity isopropanol

The invention provides a method for removing acetone in isopropanol. The method comprises the following steps: S1, converting acetone in isopropanol into acetoxime; and S2, rectifying the product obtained in the step S1. According to the method disclosed by the invention, the acetone is removed by innovatively converting the acetone in the isopropanol into acetoxime which is greatly different from the isopropanol in boiling point, the ppm-level acetone in the isopropanol can be effectively removed, the removal rate can reach 100%, and the content of the acetone is as low as 0 ppm through gas chromatography detection. Acetone oxime and other impurities can be almost completely removed in a conventional rectification, ion exchange or adsorption mode, so that the high-purity electronic-grade isopropyl alcohol is obtained.
Owner:SHENZHEN CAPCHEM TECH CO LTD

Compound corrosion inhibitor for gathering pipeline of oil and gas field and preparation method of compound corrosion inhibitor

The invention discloses a compound corrosion inhibitor for gathering and transportation pipelines of oil and gas fields and a preparation method, and relates to the field of corrosion and protection of petroleum pipeline steel, and the compound corrosion inhibitor comprises 59-64% of a compound corrosion inhibitor, 30-33% of an auxiliary material and 3-11% of a filler. The main materials comprise fluorine-containing oleic acid imidazoline, quinoline quaternary ammonium salt and carbon quantum dots; auxiliary materials: a surfactant, a complexing agent and an antioxidant; the filler is nano mesoporous silica. The corrosion inhibitor disclosed by the invention can be used for effectively protecting gathering and transportation pipelines of oil and gas fields in neutral or acidic corrosive media and high-temperature environments. The corrosion inhibitor has the advantages of being environmentally friendly, small in dosage and low in cost.
Owner:JIANGXI POYANG LAKE LNG CO LTD

A bamboo hard carbon material and preparation method thereof

The invention discloses a bamboo hard carbon material, comprising the following components in parts by weight: 65-70 parts of bamboo powder, 6-8 parts of phosphoric acid, 5-7 parts of ethylenediamine, 4-6 parts of N-hydroxysuccinimide, 3-6 parts of 2,5-furan dimethanol, and 80-90 parts of deionized water. The bamboo hard carbon material is prepared by the following method: bamboo is pre-treated and carbonized, ball-milled to obtain 500-mesh bamboo powder, then mixed with phosphoric acid, ethylenediamine, N-hydroxysuccinimide, 2,5-furan dimethanol, deionized, dried, filtered to obtain modified bamboo powder, and then the modified bamboo powder is carbonized at high temperature and plasma treated to obtain the bamboo hard carbon material. The bamboo hard carbon material prepared by the present invention can be used as a negative electrode material of an ion battery, which can effectively improve the specific capacity, initial coulomb efficiency, and rate performance of the ion battery, and enhance its cycle stability, prolong service life, and the production process is simple and easy to promote.
Owner:SHAANXI PUSTAR ENVIRONMENTAL PROTECTION TECH CO LTD

Epigallocatechin gallate starch nanoparticles as well as preparation method and application thereof

The invention discloses epigallocatechin gallate starch nanoparticles as well as a preparation method and application thereof, and belongs to the technical field of medicinal chemistry. According to the method, high-proportion branched-chain cassava starch is used as a raw material, ultrasonic microwave assistance is adopted, in the nanometer starch alcohol precipitation process, epigallocatechin gallate is synchronously packaged to form nanometer-level epigallocatechin gallate starch nanometer particles, and embedding of epigallocatechin gallate is completed. The embedding rate of the epigallocatechin gallate starch nanoparticles can reach 50.20%, the drug loading capacity can reach 311mg / g, the drug slow release performance is obvious in the process of simulating gastrointestinal digestion, the sustained release time can be 20 hours, the drug release capacity can reach 72.33% and 90.10% respectively, and the preparation process is simple, easy to operate, low in preparation cost and suitable for large-scale production and application.
Owner:GUANGXI UNIV FOR NATITIES

Non-polar thermoplastic material with polar surface coating as well as preparation method and application of non-polar thermoplastic material

The invention relates to a non-polar thermoplastic plate with a polar surface coating as well as a preparation method and application of the non-polar thermoplastic plate, and belongs to the technical field of automobile coatings. The problems that in the prior art, in the process of attaching a paint film to the surface of a non-polar thermoplastic plate, a base material is prone to thermal stress or deformation, the paint film is uneven in attachment and prone to falling off or peeling off, cost is high, process time is long, and industrialization is difficult to achieve are solved. According to the method, low-cost polyphenol and amine substances are used for spraying codeposition, and a particle coating with a certain thickness and roughness is formed on the surface of the non-polar thermoplastic plate by regulating and controlling the condition parameters of the spraying process, so that the adhesion capacity of the surface of a matrix is enhanced; the introduced active groups increase the surface polarity of the matrix and enhance the interface bonding between the matrix and the paint film; the particle coating is prepared at normal temperature, so that thermal stress or deformation caused by heating of a matrix is avoided; and by adopting the processes of adding a strong oxidant and spraying and codepositing, the modification time is greatly shortened, the working efficiency is improved, and the industrial production of the modified non-polar thermoplastic plate is promoted.
Owner:BEIJING NAT INNOVATION INST OF LIGHTWEIGHT LTD +1