7831 results about "Dispersity" patented technology

A cationic fluoric surfactant Gemini and its chemical structure are disclosed. Its advantages are lower critical micell concentration, less consumption, and high dispersity, foam stability, penetrability and wettability.

The invention discloses a method for using low-temperature plasma to prepare a supported metal sulfide catalyst and belongs to the technical field of material science. The method is characterized by including: allowing ionization of hydrogen sulfide gas or gas containing hydrogen sulfide through gas discharge to form the low-temperature plasma distributed evenly, and using the low-temperature plasma to interact with supported metal salt precursor to generate metal sulfide. Due to the fact that the catalyst is avoided from being exposed in excessively high temperature, the prepared catalyst is free of thermal agglomeration, so that the catalyst is smaller in particle size and higher in dispersity. The method is suitable for preparation of various sulfide catalysts, metal sulfide can be supported on different materials to prepare various supported catalysts. The method has the advantages of low reaction temperature, low energy consumption, short preparation time and the like. In addition, processing objects are common metal salt, wide involve range is achieved, and the prepared catalyst is applicable to various common heterogeneous reactions.

A pattern forming method comprising a step of applying a resist composition whose solubility in a negative tone developer decreases upon irradiation with an actinic ray or radiation and which contains a resin having an alicyclic hydrocarbon structure and a dispersity of 1.7 or less and being capable of increasing the polarity by the action of an acid, an exposure step, and a development step using a negative tone developer; a resist composition for use in the method; and a developer and a rinsing solution for use in the method, are provided, whereby a pattern with reduced line edge roughness and high dimensional uniformity can be formed.

The invention belongs to the technical field of molecular sieve preparation, and particularly relates to an in-situ preparation method for a microporous-mesoporous molecular sieve containing noble metal. The in-situ preparation method comprises the steps as follows: adding a coupling pore-forming agent, a silicon source, an aluminum source or a titanium source, and an alkali source into a water solution of noble metal nano particles in sequence under the water bath condition; and ageing, drying, crystallizing, drying and carrying out high-temperature calcination to obtain the microporous-mesoporous molecular sieve containing the noble metal. The prepared microporous-mesoporous molecular sieve is provided with a hierarchical pore structure; the noble metal nano particles with high dispersity are covered in situ while a mesoporous structure is generated; and a synthetic method is convenient and simple, saves energy and reduces emission. A multifunctional catalyst prepared with the method integrates the advantages of the microporous channels of the molecular sieve, the transgranular meso pores and the intergranular meso pores of the molecular sieve and the noble metal nano particles, and is more suitable for catalytic reactions of sulfur-containing large molecules such as hydrogen desulfurization and the like.

The invention relates to a novel preparing method for an in-situ nitrogen-doped porous carbon material, the application of the in-situ nitrogen-doped porous carbon material serving as a carrier of a load type catalyst, the load type catalyst comprising the in-situ nitrogen-doped porous carbon material, and the application of the load type catalyst in the water phase alcohol condensation reaction. Cheap micromolecule nitrogen substances serve as a nitrogen source of the in-situ nitrogen-doped porous carbon material, nitrogen atom in-situ doping is achieved in the carbon material preparing process, the doping content of the in-situ nitrogen-doped porous carbon material is controllable, the in-situ nitrogen-doped porous carbon material is distributed evenly, the dispersity of metal in the carrier and the combining strength with the carrier can be improved through doping of nitrogen atoms, and therefore the catalytic activity of the nitrogen-doped porous carbon material can be improved, and the service life of the nitrogen-doped porous carbon material can be prolonged.

A separation matrix comprises a porous surface layer; and a bulk porous support, wherein both the porous surface layer and the bulk porous support comprising a block copolymer. The block copolymer comprises A-B or A-B-A repeating units, wherein A and B at each occurrence are two different blocks of oligomer, or polymer. A structural unit of block A is derived from one or more atom transfer radical polymerization (ATRP)-active monomer or oligomer and a structural unit of block B is derived from a thermoplastic ATRP-active macro initiator. A poly dispersity index of the block copolymer is at least about 2.

The invention discloses a preparation method of a hydrocracking catalyst. The method comprises the steps of preparing an acidic mixed solution A containing hydrogenation reactive metals and silicon, preparing a sodium metaaluminate alkaline solution B, and then adding the acidic mixed solution A, the alkaline solution B and CO2 to a reaction tank filled with clear water in parallel to prepare gel; and then adding turbid liquid of a Y type molecular sieve, mixing the substances uniformly, filtering, drying and forming the mixture, and then washing, drying and roasting the product, thus preparing the hydrocracking catalyst. The method has the beneficial effects that a clean preparation method is adopted, so not only can the catalyst be easily formed and the strength of the catalyst be improved, but also the pore volume and specific surface area of the catalyst can be increased and the dispersity of metals in the catalyst can be improved, thus the catalyst has higher hydrocracking activity, middle oil selectivity and stability; and the catalyst prepared by the method can be used for a single-section hydrocracking process of a non-refining section or a one-section serial hydrocracking process of a refining section.

The invention belongs to the field of adsorbing materials, and relates to an inorganic-inorganic hybrid material, particularly a graphene/clay composite material. The composite material is powdery, is compounded from porous graphene and clay, and has a porous structure; the porous graphene is inserted among clay layers through intercalation reaction; the mass ratio of the porous graphene to the clay is 1:(0.1-10); the specific area of the graphene/clay composite material is 200-250 m<2>/g, and the weight loss within 900 DEG C is 3-6 wt%; and the clay is montmorillonite, vermiculite, illite, kaolin or rectorite. The graphene/clay composite material can be easily dispersed, can be used for comprehensively and efficiently adsorbing heavy metals and organic substances, and has the characteristics of high dispersity and efficient and selective adsorbability for heavy metals and organic substances; the maximum comprehensive removal rate can reach 99%; and thus, the invention has wide prospects in industrialized application.

The invention discloses a preparation method of a double-layer coated water-based aluminum pigment, which comprises the following steps: coating ethyl orthosilicate on lamellar aluminum powder to form a single-layer coated aluminum pigment; and under the action of an azo initiator, coating a hydrophilic ester monomer on the single-layer coated aluminum pigment to form the double-layer coated water-based aluminum pigment. The double-layer coated water-based aluminum pigment prepared by the method provided by the invention has the advantages of high coating tightness and favorable water resistance, and the coating layer can not be easily damaged. The organic layer on the outer layer is easily compatible with high-molecular rein in the paint, has favorable dispersity in the paint, and is mainly used in various water-based paints and water-based inks.

The invention discloses a preparation method and application of a supported metal catalyst. The supported metal catalyst comprises carrier framework materials and nano particles, loaded on the surfaces of the carrier framework materials, of metal or metal oxide, or metal ions chelated on the surfaces of the carrier framework materials, wherein the metal ions and nano particles of the metal or metal oxide are loaded on the surfaces of the carrier framework materials through the polymerization layers, adhered to the surfaces of the carrier framework materials, of catechol derivatives. The preparation method of the supported metal catalyst has the advantages that the method is simple, various carrier framework materials are used, one or more metal ions or nano particles can be loaded, and universality is achieved; the supported metal catalyst is good in active metal dispersity, large in carrier specific surface area, low in use amount, low in cost, and the like; the catalyst loaded with noble metal is catalyst material which is widely used and environmental friendly and is efficiently applicable to environmental chemical engineering fields such as dye wastewater decoloring, wastewater organic pollutant removing, car tail gas treatment, air purification, hydrogenation and reforming catalytic reaction, gas sensors and fuel cells.

The invention discloses a lithium ion battery silicon carbide composite anode material and a preparation method thereof and aims to solve the technical problem of improving the cycling stability of a silicon carbide cathode. The lithium ion battery silicon carbide composite anode material consists of the following components in percentage by mass: 85 to 75 percent of graphite and 15 to 25 percent of silica particles, wherein the nano silica particles are dispersed on a graphite carrier to form a nuclear shell structure and are 5 to 16 mum in granularity. The preparation method comprises the following steps of: preparing a graphite dispersing agent and a silicon grinding dispersing agent; adding the silicon grinding dispersing agent into the graphite dispersing agent; and performing thermal treatment. When the method is compared with the prior art, silicon atoms are dispersed on a graphite atomic nucleus by a cation-anion charge absorption method, so that the silicon atoms can uniformly wrap the surface of the graphite, the dispersity of silicon is effectively improved in a silicon carbide composite material preparing process, the initial efficiency and the cycling stability of the silicon carbide composite anode material are improved, and a battery using the material as an anode material has relatively high safety, multiplying power performance and cycle performance.

The invention provides a low-expansion coefficient polyvinyl chloride alloy material and a manufacturing method thereof. The ingredients of raw materials of the alloy material comprise a polyvinyl chloride substrate, a heat-resistant modifier, a heat stabilizer, a lubricator, a filler and a processing agent, and the alloy material is manufactured by a melt blending technique. The processing agent and the filler in the ingredients of the raw materials of the invention are the processing agent that is subjected to modification by a new method and the filler that is subjected to organic treatment, and by means of a mechanochemical reaction, self-plastification, toughening and reinforcement of the PVC can be combined organically to improve compatibility and dispersity of the polyvinyl chloride, the filler and heat-resistant resin, thus settling the problem about the contraction between the improvement of heat expansion performance and heat resistance of the PVC, and processing performance, strength and toughness of the PVC; the polyvinyl chloride engineering plastic with low expansion coefficient, high heat resistance, high strength, high toughness, excellent aging resistance and outstanding processing performance is manufactured; the invention has extensive industrial market prospect and the manufacturing method thereof is simple in technology, convenient in operation and control, stable in quality and high in production efficiency.

A pattern forming method comprising a step of applying a resist composition whose solubility in a negative tone developer decreases upon irradiation with an actinic ray or radiation and which contains a resin having an alicyclic hydrocarbon structure and a dispersity of 1.7 or less and being capable of increasing the polarity by the action of an acid, an exposure step, and a development step using a negative tone developer; a resist composition for use in the method; and a developer and a rinsing solution for use in the method, are provided, whereby a pattern with reduced line edge roughness and high dimensional uniformity can be formed.

The invention provides a method for preparing active porous graphene. The method comprises the following steps: 1) bleaching cellulose by use of hydrogen peroxide to obtain a first intermediate product; 2) activating the first intermediate product by use of an activating agent to obtain a second intermediate product; 3) performing carbonization treatment on the second intermediate product at 600-1100 DEG C to obtain the active porous graphene. The invention aims to provide a method for preparing active porous graphene, and the active porous graphene prepared from the method provided by the invention has better conductivity and has better dispersity.

The invention provides a ZSM-5 type molecular sieve for a catalyst for a reaction for preparing propylene from methanol and/or dimethyl ether, which has a silica alumina ratio of 250-1,150 and a grain diameter of 65-250nm. A preparation method of the molecular sieve comprises the following steps: (1) mixing an aluminum source and an organic directing agent and stirring an obtained mixture at constant temperature of 0-30 DEG C for 2-24 hours; (2) adding a silicon source and an organic addition agent to the mixed solution obtained in the step (1) and continuing stirring the mixed solution to obtain gel; (3) stirring the gel obtained in the step (2) at 35-95 DEG C and then carrying out a crystallization reaction for 24-240 hours at 60-200 DEG C, wherein in the raw materials for synthesizing the molecular sieve, and the molar ratio of OH<-1> to SO2 to AL2O3 to H2O to the organic directing agent to the organic directing agent is (0.1-0.35):1:(0.0005-0.01):(10-25):(0.1-0.6):(0.5-8). The ZSM-5 type catalyst has the characteristics of controllable grain size, adjustable silica alumina ratio, high dispersity, and the like and has higher propylene selectivity and P/E ratio in the reaction for preparing low carbon olefin from the methanol and/or the dimethyl ether.

The invention discloses graphene based conductive ink, comprising 2-25 wt% of conductive component, 5-25 wt% of bonding agent, 0.1-5 wt% of additive, 0.1-2 wt% of pH (Potential of Hydrogen) adjusting agent and the balance of solvent. A preparation method comprises the following steps of: dispersing the pH adjusting agent into the solvent to obtain a uniform first mixed liquid; mixing the first mixed liquid with the bonding agent to obtain a second mixed liquid; and mixing the second mixed liquid with the conductive component and the additive to obtain the graphene based conductive ink. The invention further provides a flexible conductive thin film prepared from the conductive ink. The conductive ink disclosed by the invention has the advantages of good dispersity, good conductive effect, easiness for printing, and cheap price. Furthermore, the flexible conductive thin film prepared from the conductive ink disclosed by the invention has good conductive performance.

The invention discloses an efficient silicone defoaming agent, which mainly comprises a silicone grease mixture, a synergistic agent, a polyether silicone oil emulsifier, an assistant emulsifier, a thickening agent, preservative and water, wherein in an emulsifier emulsion, the silicone grease mixture and the polyether silicone oil emulsifier account for 70-90 percent of the amount of active matters; the active matters account for 5-30 percent of the amount of the emulsion; and water serves as another medium. In the efficient silicone defoaming agent, the foam inhibiting performance is enhanced by using the silicone grease mixture, the defoaming performance and dispersity are improved by using the polyether silicone oil emulsifier, and the silicone grease viscosity and compatibility are lowered and the emulsifying effect is improved by adding the synergistic agent. The efficient silicone defoaming agent has the characteristics of application to waterborne systems, high defoaming speed, good foam inhibiting effect, low using dosage, high chemical inertness, nontoxicity, capability of acting under severe conditions and low cost.

An object of the present invention is to provide a conjugated polymer which has a high hole transportability and is excellent in solubility and depositability. Another object of the present invention is to provide an organic electroluminescence element which is capable of low voltage driving and has a high luminous efficiency and drive stability. The conjugated polymer of the present invention is a conjugated polymer containing a specific structure as the repeating unit, where the conjugated polymer contains an insolubilizing group as a substituent, the weight average molecular weight (Mw) is 20,000 or more and the dispersity (Mw/Mn) is 2.40 or less.

The invention provides a high-scratch-resistance abrasion-resistant coating material and a preparation method thereof. The preparation method comprises the following steps: modifying the graphene surface by using active groups by a chemical modification technique to obtain modified graphene, and blending the modified graphene with polysiloxane to obtain the high-scratch-resistance abrasion-resistant nano composite coating material. The surface modification is carried out to enhance the dispersity of the graphene and the interactions between the graphene and polysiloxane matrix, thereby enhancing the mechanical properties of the coating. No pigment or filler is added. The scratch resistance of the transparent graphene/polysiloxane composite coating is enhanced by 140% or above, and the abrasion loss is reduced by 60% or above. The transparent graphene/polysiloxane composite coating has excellent adhesion, heat resistance, weather resistance, flame retardancy and corrosion resistance. The graphene/polysiloxane composite coating can be used for surface protection and shielding of various metals, plastics, wood, concrete, glass and other substrates, and is applicable to the fields of automobile paints, photoelectric materials, precision instruments, marine heavy-corrosion protection, buildings and the like.

The invention belongs to the technical field of composite materials, and discloses a carbon fiber composite material fatigue life estimating method based on stress ratio influences. Structural response calculation is carried out by means of a finite element technology. A finite element model is based on a classical laminate plate theory, and a umat subprogram taking tension and compression asymmetry into consideration is built. By carrying out constant-amplitude fatigue tests under different stress ratios, an equation of an influence mechanism of average stress on prediction of the service life of a carbon fiber composite material structure is built and is popularized to a block load and a spectrum load. A service life estimating model built through the method is based on the classical laminate plate theory and takes influences of the average stress and a variable-amplitude load into consideration, dispersity of a prediction result is little, accuracy is high, theoretical guidance is provided for reliability design of parts made of carbon fiber composite materials, and the technical problems that existing carbon fiber composite material structure fatigue life is only estimated through a test method, and accordingly cost is high and consumed time is long are solved.

The invention belongs to the technical field of synthesis of lithium ion battery ternary anode material precursors, and particularly relates to a preparation method of a nickel-cobalt-manganese hydroxide. The method comprises the following steps: preparing a small-particle-size nickel-cobalt-manganese hydroxide by a nucleation/crystallization isolation method: introducing a nickel-cobalt-manganese mixed metal solution, sodium hydroxide and ammonia water under the condition of a high pH value at the same time for nucleation, adding a certain amount of additive at the end of nucleation to help a crystal nucleus to be dispersed rapidly, and entering a crystal nucleus growing stage to obtain a spherical particular nickel-cobalt-manganese hydroxide with D50 being equal to 2 to 3 mum, high dispersity and high degree of sphericity; controlling the washing condition, so that the sulfur content of the nickel-cobalt-manganese hydroxide is as low as 1,500ppm. The method has the advantages of easiness and convenience in operation, high flexibility, no need of modifying a reaction kettle, easiness for expanded production and the like.