The invention discloses a treatment method of 2-acrylamido-2-methylpropanesulfonic acid
mother liquor, and relates to the technical field of
chemical engineering. Comprising the following steps: S1, adding water into the
mother liquor generated in the production process of 2-acrylamido-2-methylpropanesulfonic acid for extraction, and standing for layering to obtain an upper layer which is an
organic layer and a lower layer which is an
aqueous solution; s2, after extraction is completed, an upper
organic layer enters a
distillation kettle to be subjected to reduced pressure
distillation, and the distilled
solvent is recycled; distilling in the kettle until precipitates exist, cooling, carrying out
solid-liquid separation, and
drying to obtain N-tert-butyl
acrylamide; and adding an adsorbent into the
aqueous solution at the lower layer, filtering to obtain filtrate A, adding caustic soda liquid into the filtrate A until the pH value is 8-10, cooling, adding
seed crystal, standing, and carrying out
solid-liquid separation on the precipitate to obtain
solid sodium sulfate and a 2-acrylamido-2-methyl propanesulfonic acid
sodium salt solution. The treatment method is low in cost, simple to operate and high in
resource utilization rate, and the extracted product is high in purity.