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1326 results about "Nanocrystal" patented technology

A nanocrystal is a material particle having at least one dimension smaller than 100 nanometres, based on quantum dots (a nanoparticle) and composed of atoms in either a single- or poly-crystalline arrangement.

Method for improving stability of perovskite nanocrystals and application

The invention provides a method for improving the stability of a perovskite nanocrystal, which comprises the following steps: S1, preparing the perovskite nanocrystal: mixing a perovskite nanocrystal precursor and a micro / mesoporous template to obtain a mixture; calcining the mixture under the condition that the collapse temperature of the micro / mesoporous template is lower than that of the micro / mesoporous template, so as to generate perovskite nanocrystals in the pore channels of the micro / mesoporous template; s2, post-treatment by a hydrothermal method; and S2, dispersing the perovskite nanocrystals obtained in the step S1 in a high-pressure reaction device filled with an inorganic fluoride solution, and treating the mixed solution through a hydrothermal method to obtain the perovskite illuminant. According to the method, the stability of the perovskite nanocrystals can be improved without collapsing the micro / mesoporous template.
Owner:WENZHOU XINXIN TAIJING TECH CO LTD

Uniform carbon-coated lithium iron phosphate positive electrode material and preparation method thereof

The invention discloses a uniform carbon-coated lithium iron phosphate positive electrode material and a preparation method thereof, and relates to the technical field of lithium iron phosphate positive electrode materials, the uniform carbon-coated lithium iron phosphate positive electrode material comprises lithium iron phosphate matrix particles, the lithium iron phosphate matrix particles are coated with a composite carbon layer, and the composite carbon layer is doped with cerium modified tantalum carbide nanocrystals; the preparation method of the cerium modified tantalum carbide nanocrystal comprises the following steps: dissolving pentaethoxy tantalum and cerous nitrate in ethylene glycol, adding urea as a precipitator, and synthesizing a Ta-Ce-O precursor through a microwave-assisted solvothermal method; the Ta-Ce-O precursor and phenolic resin are mixed and then subjected to ball milling and sintering, and the cerium modified tantalum carbide nanocrystal is obtained. By introducing a small amount of cerium modified tantalum carbide nanocrystals into the composite carbon layer for many times, uniform coating of the composite carbon layer can be realized, and the electrochemical performance of the lithium iron phosphate positive electrode material is enhanced.
Owner:HUNAN YUNENG NEW ENERGY BATTERY MATERIALS CO LTD

Composite optical film with polarization function, preparation method and application thereof

The invention discloses a composite optical film with a polarization function, a preparation method and application thereof. The composite optical film comprises a transparent substrate layer, and a buffer layer, an oriented calcite crystal layer and an anti-reflection layer which are laminated on one side of the transparent substrate layer. Wherein the oriented calcite crystal layer is obtained by coating a superparamagnetic modified calcite crystal composite material suspension on the surface of the buffer layer, inducing optical axis oriented arrangement through a magnetic field and performing UV curing; the buffer layer is obtained by co-extruding a cycloolefin polymer and a polyurethane acrylate mixture, and a thermal expansion coefficient transition system is formed; the anti-reflection layer is composed of nano-porous titanium dioxide with the refractive index changing from 1.8 to 2.3 in a gradient mode, and a refractive index gradient structure is formed. According to the composite optical film, the polarization efficiency and the light transmittance of the composite optical film are improved and the industrial stability is improved through the design of the polarization functional layer in which the calcite nanocrystals are directionally arranged under the induction of a magnetic field and in combination with the gradient refractive index scattering layer.
Owner:NINGBO CHANGYANG TECH

Aerogel reinforced composite electrolyte film for solid-state lithium battery and preparation method of aerogel reinforced composite electrolyte film

The invention provides an aerogel reinforced composite electrolyte thin film for a solid-state lithium battery and a preparation method of the aerogel reinforced composite electrolyte thin film, and belongs to the technical field of composite electrolytes.The thin film comprises a three-dimensional porous aerogel skeleton, a solid-state electrolyte compound and lithium salt nanocrystals; wherein the three-dimensional porous aerogel skeleton is prepared from inorganic oxide nanoparticles and a polymer precursor through a sol-gel method; pores of the three-dimensional porous aerogel skeleton are filled with the solid electrolyte compound, the solid electrolyte compound comprises lithium lanthanum zirconium oxide nanowires and a polyoxyethylene-lithium salt composite matrix, and the lithium lanthanum zirconium oxide nanowires are directionally arranged in the thickness direction of the film; the lithium salt nanocrystals grow on the surface of the pore wall of the three-dimensional porous aerogel in situ; the mass ratio of the aerogel skeleton to the solid electrolyte compound is (1: 3)-(1: 15). According to the thin film, the ionic conductivity, the mechanical strength and the interface stability of the electrolyte are remarkably improved.
Owner:YUNNAN YIOU LITHIUM ENERGY TECH CO LTD

Rare earth boride nanometer material and preparation method and application thereof

The invention discloses a rare earth boride nano material as well as a preparation method and application thereof. The phase state of the rare earth boride nano material is REB6 or REB4; the preparation method comprises the following steps: S1, respectively weighing a compound raw material containing an RE element and a compound raw material containing a B element; s2, adding an additive, and fully grinding; s3, reacting under the protection of inert gas; s4, after the reaction is finished, excessive methanol is added, centrifugal separation is performed after no bubbles emerge, and a precipitate A is reserved; s5, adding diluted hydrochloric acid for soaking, and performing centrifugal separation again to reserve a precipitate B; and S6, washing the precipitate B with deionized water, and drying to obtain the rare earth boride nano material. According to the preparation method disclosed by the invention, a normal-pressure and low-temperature preparation method is adopted, the pure-phase rare earth hexaboride nanocrystal can be obtained at normal pressure and the temperature as low as 300 DEG C, and no active metal elementary substance needs to be introduced in the preparation process.
Owner:XIZHIYUANDA (TIANJIN) NEW MATERIALS CO LTD

Application of microporous and mesoporous metal organic framework microsphere material in organic dye and heavy metal wastewater

The invention discloses an application of a microporous and mesoporous metal organic framework microsphere material in organic dye and heavy metal wastewater. According to the invention, mesoporous spheres formed by self-assembly of a block copolymer are used as objects, and regular and highly dense mesoporous micron-sized particles of a self-assembled amphiphilic block copolymer (PS-b-PAA) in a selective solvent mixture are used as a template; uiO-66-NH2 and ZIF-67 micron-sized microspheres which are formed by mutual growth of metal-organic framework nanocrystals and have two pore diameters of micropores and mesopores at the same time are produced, and larger carrying capacity is obtained, so that adsorption separation is more efficiently realized. The adsorbent is respectively used for dye adsorption and heavy metal ion adsorption, and the adsorption performance and mechanism of the adsorbent are explored. The metal organic framework microspheres with both micropores and mesopores are used as an adsorbent, and a simpler, more convenient and novel method is provided for adsorption.
Owner:NANJING TECH UNIV

Anti-sinking water-based acrylic resin coating and preparation method thereof

The invention belongs to the technical field of coatings, and discloses an anti-sinking water-based acrylic resin coating and a preparation method thereof.The anti-sinking water-based acrylic resin coating is prepared from, by weight, 110-130 parts of modified water-based acrylic resin, 10-25 parts of modified cellulose nanocrystals, 3-5 parts of a composite additive, 4-6 parts of a dispersing agent, 0.5-2 parts of a defoaming agent, 0.5-2 parts of a flatting agent and 10-20 parts of water; the acrylic resin is modified by using the organic silicon oligomer and the epoxy resin, the film hardness is high, the adhesive force is strong, and the film hardness, the impact resistance, the ultraviolet aging resistance and the flame retardant property of the material are improved by adding the modified cellulose nanocrystals and the composite additive.
Owner:DAYI (YUNFU) NEW MATERIAL TECH CO LTD

An oxygen evolution reaction electrocatalyst and methods for preparation and use thereof

PCT designated stage expiredWO2025043295A1CellsElectrodesPtru catalystPhysical chemistry
An oxygen evolution reaction electrocatalyst and a method for preparing said oxygen evolution reaction electrocatalyst are disclosed. The method comprises the steps of contacting a porous zeolite with a solution containing a noble metal precursor to form a noble metal doped zeolite, pyrolyzing the noble metal doped zeolite to form nanocrystals comprising at least the noble metal and a second metal, said nanocrystals being confined within a layer of carbon-based material, wherein the second metal and the carbon-based material are derived from the pyrolyzed zeolite, and annealing said layer of carbon-based material confined nanocrystals to form isolated noble metal atoms singly dispersed within a metal oxide lattice of the second metal as an oxygen evolution reaction electrocatalyst.
Owner:NEWSOUTH INNOVATIONS PTY LTD

Heat treatment process window widening method for nanocrystalline strip with high magnetic conductivity

The invention relates to the technical field of magnetic material preparation and heat treatment, in particular to a heat treatment process window widening method for a high-magnetic-conductivity nanocrystalline strip, which comprises the following steps of: by gradient component design and pulsed magnetic field coupling heat treatment, enabling the initial magnetic conductivity of the strip to exceed 22,000 and widening the heat treatment temperature interval to 400-600 DEG C; the alloy comprises 73.5% of Fe, 1% of Cu, 3% of Nb, 13.5% of Si, 8.5% of B and 0.5% of Co, during heat treatment, the temperature is increased to 450 DEG C at the speed of 15 DEG C / min, a 0.8 T pulsed magnetic field is applied for heat preservation, then the temperature is increased to 550 DEG C for heat preservation, alpha-Fe (Si) nanocrystalline and Co-B amorphous interface phases are generated through crystallization, and Co is distributed in a solid solution mode. The method widens the heat treatment temperature interval, improves the initial magnetic conductivity of the strip, improves the toughness, meets automatic production, and reduces the cost by using the existing equipment; and the prepared strip is high in magnetic conductivity, good in stability, suitable for various scenes and good in economic benefit and social benefit.
Owner:AT&M AMORPHOUS TECH CO LTD

High-strength, highly transparent nanocrystalline glass, preparation method therefor, and use thereof

PCT designated stage expiredWO2025138087A1High fractureCordierite
A high-strength, highly transparent nanocrystalline glass, a preparation method therefor, and a use thereof. The high-strength, highly transparent nanocrystalline glass uses precursor minerals mainly comprising synthetic aluminum-rich feldspar-like ceramic glass material, β-spodumene material, cordierite material, synthetic β-dicalcium silicate material, and magnesium aluminum spinel material for the main body of a feldspar-like matrix glass having a stable structure. Ultrafine zirconia powder having a particle size of less than 10 nm is used as a nucleating agent and microcrack damping and pinning agent, to control the formation of nanocrystals smaller than 100 nm in the glass body formed after melting. The volume percentage content of the nanocrystals is 50%-95%, and the nanocrystals together with the matrix glass form a high-strength, highly transparent nanocrystalline glass having a uniform microstructure. The obtained nanocrystalline glass has high hardness, high fracture toughness and high light transmittance, and is suitable for manufacturing various types of optical glass.
Owner:HUNAN JINGCI NEW MATERIALS CO LTD

Cerium oxide photo-thermal synergistic catalytic material loaded with metal cocatalyst and preparation method and application of cerium oxide photo-thermal synergistic catalytic material

The invention provides a cerium oxide photo-thermal synergistic catalytic material loaded with a metal promoter as well as a preparation method and application of the cerium oxide photo-thermal synergistic catalytic material. The cerium oxide photo-thermal synergistic catalytic material loaded with the metal promoter comprises a cerium oxide nanocrystal and the metal promoter loaded on the surface of the cerium oxide nanocrystal, the exposed crystal face of the cerium oxide nanocrystal comprises a {111} crystal face, and the area of the {111} crystal face accounts for more than 50% of the total area of the outer surface of the crystal face; the mass fraction of the metal cocatalyst is 0.1-2wt% of the mass of the cerium oxide. The catalytic material provided by the invention takes cerium oxide with a {111} crystal face as an exposed special crystal face as a carrier, photons can be captured and charges can be separated more efficiently, and phonons further promote deep trap state charge release. Meanwhile, the metal additive is added and cooperates with cerium oxide with exposed special crystal faces for catalysis, so that the catalytic effect is remarkably improved, and efficient catalytic combustion of methane is achieved under the mild condition.
Owner:TSINGHUA UNIVERSITY

Low-loss multiphase inductance material and inductance preparation method thereof

The invention relates to a low-loss multiphase inductance material which comprises a magnet and a winding, coils adjacent to the winding are wound in the reverse direction, meanwhile, the magnet extends out to form electrodes, and the magnet comprises Fe-based nanocrystalline and iron powder. The invention has the effect of reducing the loss of the inductance material.
Owner:SHENZHEN BEST ELECTRONICS CO LTD

Perovskite quantum dot with fluorine-containing passivation layer and construction method of fluorine-containing passivation layer

The invention provides a perovskite quantum dot with a fluorine-containing passivation layer, the perovskite quantum dot comprises a micro / mesoporous template with incompletely closed pores, perovskite nanocrystals and the fluorine-containing passivation layer grow in pores of the micro / mesoporous template, and the fluorine-containing passivation layer is used for passivating surface defects of the perovskite nanocrystals; and the fluorine-containing passivation layer comprises BaF2 (BaF2). According to the method, the surface of the perovskite nanocrystal can be passivated without collapsing the micro / mesoporous template, so that the stability is improved.
Owner:WENZHOU XINXIN TAIJING TECH CO LTD

Iron-based nanocrystalline soft magnetic alloy and preparation method thereof

The invention discloses an iron-based nanocrystalline soft magnetic alloy and a preparation method thereof. A magnetically soft alloy strip is prepared through smelting and a single-roller melt-spinning method, stress relief annealing is carried out on the magnetically soft alloy strip through assistance of a magnetic field, and then crystallization annealing treatment is carried out. Different from a traditional method for regulating and controlling the magnetic performance of the alloy through precipitation of a large number of nanocrystals, the method only induces precipitation of a very small number of nanocrystals, and high saturation flux density and low coercive force can be obtained while the toughness of the strip is ensured; the iron-based nanocrystalline soft magnetic alloy with high saturation flux density and low coercive force can be prepared by taking Fe as a main element, Co element with the atomic fraction lower than 8%, Cu element with the atomic fraction lower than 1% and at least one of oxygen, sulfur, phosphorus, carbon, silicon, boron and the like as other trace elements.
Owner:JIANGYIN KANGRUI MOLDING TECH CO LTD

Inhalable tanshinone IIA lipid nanocrystal as well as preparation method and application thereof

The invention provides an inhalable tanshinone IIA lipid nanocrystal as well as a preparation method and application thereof, and the inhalable tanshinone IIA lipid nanocrystal is mainly formed by entrapping tanshinone IIA by using dipalmitoyl phosphatidylcholine DPPC and dipalmitoyl phosphatidyl ethanolamine DPPE as mixed phospholipids in the presence of a stabilizer. Compared with the prior art, the inhalable tanshinone IIA lipid nanocrystal disclosed by the invention has the advantages that by improving the physicochemical property and drug release behavior of TA, the lung retention volume of TA after aerosol inhalation is obviously increased, the retention time of TA in the lung is prolonged, and the risk of toxic and side effects caused by whole-body escape of drugs is reduced; the treatment effect on idiopathic pulmonary fibrosis is improved, and the compliance of a patient is improved.
Owner:GUIZHOU MEDICAL UNIV

Smooth-surface diamond composite film

The diamond coated glass structure may include a glass substrate in which the deposited nanocrystal diamond is coated on the glass substrate. A layer of ultra-nanocrystalline diamond may be deposited on the deposited nanocrystalline diamond. The combination of the deposited nanocrystal diamond and ultra-nanocrystal diamond may have a surface roughness of less than 9 nanometers RMS.
Owner:AKHAN SEMICONDUCTOR INC

Corrosion-resistant protective sleeve for aluminum alloy cable and preparation method of corrosion-resistant protective sleeve

The invention discloses a corrosion-resistant protective sleeve for an aluminum alloy cable and a preparation method of the corrosion-resistant protective sleeve, and belongs to the field of cable protective sleeves. The corrosion-resistant protective sleeve for the aluminum alloy cable is prepared from the following raw materials in parts by mass: 40 to 50 parts of ethylene propylene diene monomer, 15 to 25 parts of fluorinated silicone rubber, 5 to 10 parts of modified thiolated ethylene-vinyl alcohol copolymer, 8 to 15 parts of metal fluoride nanocrystal, 4 to 8 parts of vulcanizing agent, 3 to 8 parts of plasticizer and 3 to 5 parts of flame retardant. The two rubber matrixes are compounded to form a physical barrier layer to prevent corrosion media and water molecules from permeating, material pores can be filled with the metal fluoride nanocrystals, diffusion channels of the corrosion media are reduced, and hydrophobicity and corrosion resistance are improved through cooperation of the metal fluoride nanocrystals and the fluorinated silicone rubber. The modified thiolated ethylene-vinyl alcohol copolymer can improve the compatibility between rubber matrixes and form coordination with metal ions of the metal fluoride nanocrystals, so that the diffusion path of a corrosive medium is prolonged, and the corrosion of the corrosive medium is synergistically blocked.
Owner:HUBEI HONGLE CABLE HLDG

Planarized crystalline films for diffractive optics

Optical device films and methods of forming optical device films having a RMS surface roughness less than about 2.2 μin and a refractive index greater than 2.0 are provided. In one embodiment, an optical device film is provided and includes a crystalline or nano-crystalline material having a refractive index greater than 2.0. A top surface of the optical device film has a root-mean-square (RMS) surface roughness less than about 2.2 microinches (μin).
Owner:APPLIED MATERIALS INC

Preparation method of high-strength, high-hardness and ablation-resistant CuWTaTeAl gradient nano composite material

The invention discloses a preparation method of a high-strength, high-hardness and ablation-resistant CuWTaTeAl gradient nano composite material. The method comprises the following steps: 1, mechanically mixing Cu80Al20 spherical coated powder, Cu90W10 spherical coated powder, WTe2 alloy powder, Ta powder and Cu powder, and then carrying out ball milling and mixing; 2, performing SPS (spark plasma sintering); thirdly, after soaking treatment, multi-pass hot rolling deformation is carried out, and then quenching treatment is carried out; and 4, annealing heat treatment. The binary spherical coating powder, the alloy powder and the elementary substance powder are subjected to ball milling and mixing to achieve uniform distribution of all elements, high-melting-point W and Ta are added to improve the ablation-resistant temperature of the composite material, large-scale copper dendrite powder is added to form gradient distribution nanocrystals, the proportion of all the elements is controlled, the lattice distortion degree is increased, and the ablation-resistant temperature of the composite material is improved. The high-strength, high-hardness and ablation-resistant CuWTaTeAl gradient nano composite material is suitable for the fields of contacts, switches, electrical connectors, resistance welding electrodes and the like.
Owner:NORTHWEST INSTITUTE FOR NONFERROUS METAL RESEARCH

Normal-temperature preparation method of ultra-narrow emission spectrum perovskite quantum dot composite material

The invention relates to a normal-temperature preparation method of an ultra-narrow emission spectrum perovskite quantum dot composite material. The method comprises the following steps: firstly, mixing wide bandgap nanocrystals with a high-polarity solvent (such as N, N-dimethylformamide and the like) to prepare a wide bandgap nanocrystal solution; respectively mixing with perovskite quantum dot reaction precursors (such as CsBr, PbBr2 powder and the like) to prepare a reaction precursor solution; and mixing the reaction precursor solution, organic acid, organic amine and the like, and then adding a reverse polar solvent to form a precipitate, thereby preparing the perovskite quantum dot composite material with the ultra-narrow emission spectrum. The perovskite quantum dot composite material with the full width at half maximum of 15 nanometers or below can be prepared at normal temperature, and the minimum full width at half maximum can reach 14.4 nanometers.
Owner:TIANJIN UNIVERSITY OF TECHNOLOGY

High-toughness biaxially oriented nylon film and production method thereof

The invention discloses a high-toughness biaxially oriented nylon film and a production method thereof. Comprising the following raw materials in parts by weight: 40-50 parts of copolymerized nylon resin, 10-20 parts of nylon 12, 15-25 parts of thermoplastic polyamide elastomer, 3-6 parts of nanofiller, 1-3 parts of coupling agent, 10-20 parts of reinforced fiber, 5-8 parts of additive, 3-7 parts of ethylene-methyl acrylate-glycidyl methacrylate terpolymer and 6-10 parts of modified cellulose nanocrystal. The invention relates to a flame-retardant polyamide resin, which is prepared from the following components in parts by weight: 2-4 parts of amino-terminated hyperbranched polyamide and 1-3 parts of 3, 3 '-diamino-4, 4'-difluorodiphenyl sulfone. The film is high in tensile strength, good in tear resistance and excellent in barrier property and low-temperature impact resistance.
Owner:NINGBO RUICHENG PACKING MATERIAL CO LTD +1

Coil module and electronic equipment

The invention provides a coil module and electronic equipment. Relates to the technical field of circuit boards. A high-speed signal line and a wireless charging coil are integrated in the same coil module. The coil module can comprise a substrate and a metal layer formed on one side of the substrate, the metal layer comprises a thick metal area, a thin metal area and a transition area located in a junction area of the thick metal area and the thin metal area, a wireless charging coil is arranged in the thick metal area, and a high-speed signal line is arranged in the thin metal area. The first nanocrystal and the second nanocrystal are oppositely arranged on the two sides of the substrate, at least part of the periphery of the wireless charging coil is covered with the first nanocrystal, the first nanocrystal extends to the position above the transition area, and at least part of the wireless charging coil is covered with the second nanocrystal. The integration level can be improved, space resources are saved, and the high-speed signal line and the wireless charging coil are pulled away through the transition area without affecting the signal quality of the high-speed signal line and the wireless charging coil.
Owner:HUAWEI TECH CO LTD

An air filtration membrane based on nano-hybrid modified polylactic acid fiber and its preparation method

The present invention discloses an air filtration membrane based on nanohybrid-modified polylactic acid fiber and a preparation method thereof. The present invention adopts a microwave-assisted in-situ synthesis method to directly induce the in-situ growth of ZIF-8 nanocrystals on the surface of CNTs to obtain CNT@ZIF-8 nanohybrids. Through coaxial electrospinning technology, an air filtration membrane with CNT@ZIF-8 uniformly embedded in polylactic acid fibers is obtained. The preparation method of the present invention is simple and the conditions are controllable. The prepared air filtration fiber membrane has the advantages of high surface potential, large specific surface area, good air permeability, long-term filtration, etc., and is an air filtration material with broad application prospects.
Owner:CHINA UNIV OF MINING & TECH

Environment-friendly flame-retardant polyvinyl alcohol film and preparation method thereof

The invention discloses an environment-friendly flame-retardant polyvinyl alcohol film and a preparation method thereof, and relates to the technical field of polyvinyl alcohol films. The polyvinyl alcohol film is prepared from the following components in parts by weight: 90 to 110 parts of polyvinyl alcohol, 0.4 to 1.2 parts of polydopamine modified cellulose nanocrystals, 8 to 15 parts of chitosan / phytic acid / boron nitride composite flame retardant and 0.6 to 0.9 part of plasticizer. The preparation method comprises the following steps: adding polyvinyl alcohol into deionized water, dissolving and mixing to obtain a polyvinyl alcohol aqueous solution, adding glycerol, continuously stirring for 1-2 hours, sequentially adding a chitosan / phytic acid / boron nitride composite flame retardant and polydopamine modified cellulose nanocrystals, and uniformly stirring and mixing at 50-70 DEG C to obtain a blended solution; and carrying out film casting on the blended solution. The limit oxygen index of the film is greater than or equal to 30%, the vertical combustion grade is V-0, the tensile strength is greater than or equal to 40%, the elongation at break is greater than or equal to 140%, and the light transmittance is greater than or equal to 85%.
Owner:ANHUI RUIHONG NEW MATERIAL TECH CO LTD

Degradable environment-friendly electric insulation plastic packaging bag and preparation method thereof

The invention relates to the field of packaging materials, and particularly discloses a degradable environment-friendly electric insulation plastic packaging bag and a preparation method thereof. The degradable environment-friendly electric insulation plastic packaging bag is prepared from the following raw materials in parts by weight: 100 parts of polylactic acid, 1-4 parts of organic zirconium phosphate, 2-5 parts of hydrophobic modified cellulose nanocrystals, 4-10 parts of polyimide / aluminum fluoride composite nanofibers, 1-3 parts of a dispersing agent, 1-4 parts of an antioxidant, 3-5 parts of inorganic filler, 1-3 parts of a slipping agent, 1-3 parts of an antistatic agent and 3-5 parts of a flame retardant. The packaging bag can be used for objects with high requirements for electrical insulation, has high electrical insulation capacity at high temperature, and is high in transparency and mechanical property.
Owner:QINGDAO ZHOUSHI PLASTIC PACKAGE

Method and system for dynamically monitoring molecular interaction in situ based on UCNPs probe

The invention relates to a UCNPs probe-based in-situ dynamic monitoring molecular interaction method, which comprises: S1, providing a UCNPs probe, the core layer of the UCNPs probe being a rare earth up-conversion nanocrystal, the shell layer of the UCNPs probe being an anti-quenching inert material, and the anti-quenching inert material coating the surface of the rare earth up-conversion nanocrystal; the surface of the anti-quenching inert material is modified with ligand molecules, and the ligand molecules are used for being specifically combined with target molecules in a to-be-detected sample; s2, mixing or contacting the UCNPs probe with a to-be-detected sample containing target molecules to construct a to-be-analyzed molecular interaction system; s3, irradiating the molecular interaction system by adopting near-infrared pulse laser, and collecting the change of the fluorescence lifetime tau of the UCNPs along with the time t and the change of the fluorescence intensity I along with the time t in real time to obtain a tau-t curve and an I-t curve; and S4, according to the tau-t curve and the I-t curve, realizing in-situ dynamic monitoring on the molecular interaction state. According to the method, a molecular binding / dissociation event is directly converted into a quantifiable and anti-interference optical signal, and the technical defect that in-situ dynamic monitoring of molecular interaction cannot be achieved in a traditional technology is overcome.
Owner:SHANGHAI LEIMENGKE TECHNOLOGIES CO LTD

Aluminum-manganese composite nanocrystal, and preparation method therefor and use thereof

An aluminum-manganese composite nanocrystal, and a preparation method therefor and the use thereof. The method for preparing the aluminum-manganese composite nanocrystal comprises: step 1, mixing an aluminum salt solution, a manganese salt solution and an anionic adjuvant solution to obtain a mixture, and adjusting the pH value of the mixture to 5.5-8.5; and step 2, heating the mixture for a reaction, and washing the obtained solid reactant to obtain the aluminum-manganese composite nanocrystal. According to the aluminum-manganese composite nanocrystal prepared using the preparation method and the use thereof in the preparation of a vaccine adjuvant, a pharmaceutical composition, a drug delivery carrier or an immunogenic composition, the technical problem that an existing aluminum adjuvant cannot activate humoral immunity and cell immunity at the same time can be effectively solved.
Owner:THE GBA NAT INST FOR NANOTECHNOLOGY INNOVATION

Felodipine sustained release tablet and preparation method thereof

The invention relates to the field of pharmacy, and discloses a felodipine sustained release tablet and a preparation method thereof.The felodipine sustained release tablet comprises a tablet core and a film coating layer wrapped outside the tablet core, and the tablet core comprises the following components in parts by mass: 3.5-5.0 parts of felodipine nanocrystals; 50 to 65 parts of modified hydroxypropyl methylcellulose; the preparation method comprises the following steps: S1, preparing felodipine nanocrystals: dissolving felodipine in an organic solvent, and carrying out anti-solvent precipitation and high-pressure homogenization treatment, so as to obtain a nanocrystal suspension; drug nanocrystals are embedded between silicate layers through an ultrasonic embedding technology, and burst release is inhibited by combining physical confinement and electrostatic adsorption; the gradient pore skeleton constructs a pore layer-by-layer decreasing structure through fluidized bed multi-temperature zone deposition, the release rate is accurately regulated and controlled, and collapse is avoided; the ionic liquid stabilizer is introduced, and the problems of nanocrystal aggregation and degradation are synchronously solved through hydrogen bond anchoring and an antioxidant function.
Owner:JIANGSU LIANHUAN PHARMA

High-strength anti-freezing vegetable protein adhesive based on multi-scale structure regulation and control and preparation method of high-strength anti-freezing vegetable protein adhesive

PendingCN120383909AProtein adhesivesCellulose derivative adhesivesPolymer scienceAdhesive
The invention discloses a high-strength anti-freezing vegetable protein adhesive based on multi-scale structure regulation and a preparation method thereof. The vegetable protein adhesive is mainly prepared from the following raw materials: vegetable protein meal, an anti-freezing modifier, modified cellulose nanocrystals, a chemical cross-linking agent and a dispersion medium. Wherein the components comprise 30 parts of vegetable protein meal, 10-15 parts of an anti-freezing modifier, 0.5-1.2 parts of modified cellulose nanocrystals, 4-6 parts of a chemical cross-linking agent and 70 parts of a dispersion medium. The invention provides a high-strength anti-freezing vegetable protein adhesive based on multi-scale structure regulation and control, which breaks through the bottleneck of low-temperature freezing and brittleness of the traditional adhesive, effectively solves the problem of poor performance of the vegetable protein adhesive in a low-temperature environment, fills up the blank of a bio-based adhesive in the low-temperature field, and has a wide application prospect. The anti-freezing performance, the bonding strength, the environment-friendly performance and the sustainability are excellent.
Owner:BEIJING FORESTRY UNIVERSITY

Solid waste-based low-carbon gel material and preparation method thereof

ActiveCN121063892ASlurryNanocrystal
The invention discloses a solid waste-based low-carbon gel material and a preparation method thereof. The material comprises the following components in percentage by mass: 40%-60% of high-activity slag, 20%-35% of tower bottom ash subjected to stage treatment, 3%-8% of a pH sensitive composite exciting agent, 0.5%-2% of nano C-S-H seed crystal, 0.1%-1% of modified cellulose nanocrystals and 15%-25% of water, and the water-solid ratio is controlled to be 0.15-0.28. The preparation method comprises the steps of tower bottom ash grading pretreatment, nano C-S-H seed crystal preparation and dispersion, pH sensitive composite exciting agent preparation, mixing and slurry preparation. Sulfate release is optimized through staged treatment, alkalinity is dynamically regulated and controlled through a pH sensitive exciting agent, ordered hydration and a multi-stage pore structure are induced through nano C-S-H seed crystals and modified cellulose nanocrystals, and the compressive strength, the impermeability and the low expansion rate are remarkably improved. Industrial solid waste is effectively utilized, energy consumption and carbon emission are reduced, the problems of non-uniform hydration and expansion cracking are solved, and the method is suitable for the fields of green buildings and resource recycling.
Owner:POLYMER ECOLOGICAL TECHNOLOGY (JIANGSU) CO LTD