The invention discloses a preparation method of
surface plasmon enhanced Mn < 4 + > doped
double perovskite fluorescent
powder, which comprises the following steps: S1, selecting specific A, B 'and B' 'source compounds, mixing according to a stoichiometric ratio, adding
zirconium oxide balls into a ball milling tank, carrying out planetary ball milling for 3-8 hours, putting into an
alumina crucible,
sintering at 900-1300 DEG C for 6-15 hours to obtain a substrate, cooling, carrying out particle size treatment, and carrying out XRD detection; s2, selecting a Mn < 4 + >-containing compound according to the concentration of 0.1-5 mol%, and carrying out ball milling on the Mn < 4 + >-containing compound and And S3, carrying out
metal nanometer treatment on a
metal salt solution and the material obtained in the previous step. The luminous efficiency of the fluorescent
powder is remarkably improved, the intensity can be improved by 30%-50% compared with that of traditional fluorescent
powder, color regulation and control are accurate, multicolor
fluorescence emission can be achieved, the
color saturation and luminous efficiency can be improved when the fluorescent powder is applied to a display technology, the
color rendering index and luminous efficiency can be improved when the fluorescent powder is used for illumination, and the anti-counterfeiting effect in the anti-counterfeiting field is enhanced; the
chemical stability is good, the preparation is easy to control, and industrial production and multi-field application expansion are facilitated.