1373 results about "Phosphorus" patented technology

A double cold rolled non-oriented electrical steel sheet having a composition including: 0.0001%≤Carbon≤0.007%, 0.1%≤Manganese≤0.2%, 3.1%≤Silicon≤3.6%, 0.8%≤Aluminum≤1.1%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements. The remainder composition being iron and unavoidable impurities caused by processing, the microstructure is made of ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, is from 35% to 45% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.64 T to 1.66 T.

A double cold rolled non-oriented electrical steel sheet having a composition including, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.15%≤Manganese≤0.3%, 3.2%≤Silicon≤3.8%, 0.8%≤Aluminum≤1.1%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements. The remainder composition being iron and unavoidable impurities caused by processing, the microstructure is made of ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, less than 30% when calculated in accordance of Bertotti method and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.66 T to 1.69 T.

A double cold rolled non-oriented electrical steel sheet having a composition including of the following elements, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.1%≤Manganese≤0.3%, 3.1%≤Silicon≤3.8%, 0.6%≤Aluminum≤0.8%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements. The remainder composition is iron and unavoidable impurities caused by processing. The microstructure ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, of 40 to 50% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.66T to 1.7T.

A non-oriented electrical steel sheet having a composition including of the following elements, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.21%≤Manganese≤0.7%, 3%≤Silicon≤3.6%, 0.7%≤Aluminum≤1.3%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, with 3.85%≤Si+Al+Mn≤5.5%, and can contain various optional elements. The remainder composition being composed of iron and unavoidable impurities. The microstructure is ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 35% to 45% and simultaneously having a magnetic polarization at 5000 A / m (J50) from 1.63T to 1.66T.

The invention relates to the technical field of sludge reduction and resource utilization, in particular to a method for resource utilization of sludge gasification slag. According to the method, municipal sludge gasification slag is smashed and then subjected to acid leaching, acid leaching liquid and acid leaching slag are obtained, iron in the acid leaching liquid is recycled, meanwhile, the acid leaching slag is subjected to alkaline leaching, under the strong alkaline condition, a calcium source is added into alkaline leaching liquid, then calcium phosphate sediment can be obtained, and iron in alkaline leaching separation liquid is recycled; a calcium ion solution can be generated in the processes of recovering iron in the pickle liquor and refining calcium phosphate, and the obtained calcium ion solution can be used as a calcium source for comprehensive utilization. The method disclosed by the invention can be used for realizing extraction and resource utilization of phosphorus, iron, aluminum and calcium in the sludge gasification slag, and has important significance on environmental protection and resource saving.

A kind of preparation method of high compaction lithium iron phosphate of multistage gradation, including step one: iron source, phosphorus source, lithium source, carbon source, dispersing agent, element dopant and solvent are dispersed according to proportion, slurry after dispersion is divided into A, B, C three slurry according to proportion, three slurry are grinded respectively, and then are respectively carried out spray drying;Step two: three spray materials are respectively pre-sintered at different temperatures, and pre-sintered material is respectively crushed;Step three: the material after pre-sintering is mixed to realize multistage particle gradation.Certain mass ratio of carbon source and pre-crushed material are dry mixed;Step four: after secondary sintering, crushing and magnetic removal process, the multistage gradation high compaction lithium iron phosphate positive material is obtained.The present application realizes particle gradation of once sintered material, secondary carbon coating and sintering strengthening by grading particle size design, and realizes the collaborative improvement of compaction density and specific capacity of lithium iron phosphate positive material.

The invention provides a preparation method of grain size grading iron phosphate and high compaction type lithium iron phosphate. Removing impurities from the titanium dioxide byproduct ferrous sulfate, and filtering to obtain a purified ferrous sulfate base solution; the method comprises the following steps: reacting phosphoric acid with ammonia water to prepare ammonium phosphate solutions with different reaction pH values and phosphorus molar concentrations, respectively mixing the ammonium phosphate solutions with a certain amount of hydrogen peroxide, and sequentially adding an iron source, a first phosphorus salt solution, a second phosphorus salt solution and a third phosphorus salt solution into a tubular reactor for reaction to obtain iron phosphate slurry; and sequentially converting, filtering, washing, drying and calcining the completely reacted slurry to finally prepare the anhydrous iron phosphate. According to the invention, a mode of controlling solution nucleation and growth is adopted, nucleation and growth rates are controlled by preparing phosphorus salt solutions with different concentrations, size grading of precursor particles is directly realized in a synthesis reaction section, and slurry grading uniformity is further realized through aging crystal transformation. Lithium iron phosphate prepared from the iron phosphate precursor has high compaction density.

The invention belongs to the technical field of vanadium enrichment mechanisms of phosphorus vanadium ores, and discloses a research method of a vanadium enrichment mechanism in a diagenetic stage of phosphorus vanadium ores, which comprises the following steps: S1, sample collection and treatment; s2, rock ore identification and mineral composition analysis; s3, analyzing the occurrence state and microcell morphology of vanadium; s4, performing geochemical analysis on the whole rock; s5, in-situ microcell geochemical analysis is carried out; s6, phosphorus nodule analysis; s7, comprehensive analysis and mineralization model establishment; according to the method, mineralogy, total rock geochemistry, micro-area surface scanning and other multi-scale and multi-means research methods are comprehensively utilized, and the vanadium occurrence state, the ore-forming fluid evolution and the phosphorus-vanadium coupling relation are finely described; in-situ microcell geochemical analysis is introduced into phosphorus nodule analysis, the internal structure, the growth sequence and element distribution of the phosphorus nodule are directly revealed, obvious frontier and systematicness are achieved, and reliable theoretical support is provided for accurate exploration of vanadium ore resources and green and efficient dressing and smelting process research and development.

The invention discloses a phosphorus-nitrogen-silicon synergistic flame retardant containing a POSS (Polyhedral Oligomeric Silsesquioxane) structure and a preparation method of the phosphorus-nitrogen-silicon synergistic flame retardant. The flame retardant integrates three elements of phosphorus, nitrogen and silicon, and can generate a better flame-retardant synergistic effect; meanwhile, the POSS structure and the phenyl structure in the flame retardant endow the flame retardant with good heat resistance and good compatibility with a matrix material polycarbonate (PC), and the flame retardant is suitable for high-temperature processing conditions. In addition, the preparation method of the flame retardant is simple in process, the yield reaches up to 85% or above, and industrial production is easy to achieve.

The invention discloses an enhanced metal-based composite water purifying agent and a preparation method thereof, belongs to the technical field of preparation of water purifying agents, and aims to solve the technical problem that the flocculation capacity and the stability of a composite water purifying agent in the prior art need to be further improved. The preparation method specifically comprises the following steps: preparing a water purifying agent skeleton dispersion liquid by using chitosan and sodium alginate; chitosan-sodium alginate is used as a porous framework, a polyphenol-multi-metal complex is loaded, a structure is enhanced through Ca < 2 + > crosslinking, then SiO2 is used for coating to improve acid and alkali resistance and stability, and finally PAC is introduced to realize rapid flocculation. In the preparation process, the organic framework, the metal complex and the inorganic coating layer are fully compounded through pH control and step-by-step dropwise adding, and the obtained composite water purifying agent can efficiently remove phosphorus, chromium and suspended solids in water and shows a remarkable synergistic purification effect and storage stability.

The invention relates to the technical field of inorganic compound preparation, and particularly discloses a method for preparing high-purity iron phosphate through low-temperature acidolysis of phosphated residues, which comprises the following steps: washing, drying and crushing the phosphated residues to obtain phosphated residue powder; carrying out low-temperature acidolysis reaction on the phosphated residue powder and inorganic acid in an aqueous medium at 60-90 DEG C to obtain an acidolysis solution; adding an oxidizing agent into the acidolysis solution, adjusting the pH value of the system to 2.5-4.5 at 65-85 DEG C, carrying out oxidation impurity removal, and filtering to obtain an iron-containing phosphate solution; and selectively supplementing an iron source according to the molar ratio of iron to phosphorus in the solution, adjusting the pH value to 1.0-3.0, and carrying out precipitation reaction at 65-75 DEG C to generate iron phosphate. According to the method, low-energy-consumption resource utilization of the phosphated residues is achieved by combining low-temperature acidolysis with oxidation impurity removal and component regulation and control, the product purity meets the battery-grade requirement, and the method is suitable for preparing the lithium battery positive electrode material precursor.

The invention relates to a dephosphorization material, a preparation method thereof and a dephosphorization method, belongs to the field of water treatment, and solves at least one of the problems of contradiction between adsorption capacity and structural stability, fast capacity fading, short service life, difficult recovery, higher cost and the like of the existing lanthanum-based dephosphorization material. The phosphorus removal material is a nano-porous carbon-supported lanthanum composite material, and comprises an amorphous nano-porous carbon matrix, an amorphous nano-porous carbon carrier, an amorphous nano-porous carbon carrier, and an amorphous nano-porous carbon carrier, and an active component embedded in situ in the nanoporous carbon matrix; wherein the active component comprises lanthanum oxide and / or lanthanum hydroxide. According to the invention, the adsorption capacity is high, the structure is stable, the attenuation of the adsorption capacity is delayed, the service life is prolonged, the cost is reduced, and the adsorbent can be recycled.

The invention provides a sulfide solid electrolyte and a preparation method of the sulfide solid electrolyte. The sulfide solid electrolyte is a phosphorus-free solid electrolyte, and has a chemical general formula as shown in a formula I: Li < 7-m > MS < 6-m-n > OnXm, wherein M comprises at least one of As, Sb and Bi, and X comprises at least one of F, Cl, Br and I and 1lt; mlt; mlt; 2, 0.5 < = nlt; and 3, the sulfur-oxygen ratio S / O in the formula I is greater than 1. The sulfide solid electrolyte has excellent ionic conductivity and air stability.

The invention relates to the technical field of iron phosphate preparation, in particular to a preparation method of low-impurity iron phosphate with a high iron-phosphorus ratio, which at least comprises the following steps: preparing an iron source solution and a phosphorus source solution; mixing an oxidizing agent and a phosphorus source solution as a phosphorus source mixed solution; adding the phosphorus source mixed solution into the iron source solution, and controlling the molar ratio of iron to phosphorus to be 1: (1.1-1.3) to prepare slurry; dividing the slurry into two parts, respectively adding an impurity removal agent, and then carrying out segmented aging at 90 DEG C to prepare crystallized slurry; and filtering, washing, drying and calcining the crystallized slurry to obtain a target product iron phosphate finished product. The impurity removal agent is selected from one or more of ferrous sulfate, ferrous chloride, ferrous nitrate and ferrous oxalate. Seed crystals are formed through segmented aging crystal transformation to promote crystal growth, and autonomous grain size distribution is achieved; an impurity removing agent is added in the aging stage, impurities are reduced by using the same ion effect, the iron-phosphorus ratio is increased, and the compaction density and the electrical property of the prepared lithium iron phosphate are remarkably improved.

A non-oriented electrical steel sheet having a composition of the following elements, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.09%≤Manganese≤0.15%, 2.5%≤Silicon≤3%, 0.1% ≤ Aluminum≤0.5%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, and can contain various optional elements, the remainder composition being composed of iron and unavoidable impurities caused by processing, the microstructure of the steel sheet being made of ferrite and including in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and having a percentage of eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, from 35% to 45% when calculated in accordance of Bertotti method.

The invention belongs to the technical field of preparation of phosphorus removal agents, and particularly relates to a composite phosphorus removal agent and a preparation method and application thereof. The composite phosphorus removal agent comprises a honeycomb carrier and microspheres, the microspheres are loaded on the honeycomb carrier; the microspheres are prepared from the following raw materials: polyvinylidene fluoride particles, graphene oxide, ZrOCl2 and phosphorus-accumulating bacteria. The composite phosphorus removal agent comprises a honeycomb carrier, microspheres and microcapsules, wherein the microspheres and the microcapsules are loaded on the honeycomb carrier; capturing phosphate radicals in a water body by the microspheres and carrying out biological phosphorus removal and adsorption phosphorus removal; the honeycomb carrier also has the effect of adsorbing phosphate; and the two synergistically remove phosphate in the water body, so that the phosphorus removal effect of the phosphorus removal agent is improved, and the burden of the water body is not increased.

The invention discloses a moss ecological brick and a preparation method thereof, and relates to the technical field of ecological restoration, the moss ecological brick comprises a moss gametophyte matrix and a brick body, the brick body comprises the following raw materials: a tailing composite material, metakaolin, an acid activator and water, and the tailing composite material comprises phosphate tailings and iron tailings. The phosphate tailings and the iron tailings can provide necessary phosphorus elements, other trace elements and the like for the growth of the moss, and the acid activator in the brick body not only can provide a weak acid environment to facilitate the good growth of the moss, but also can solve the problem of saltpetering of the brick body in the environment; the growth of the moss can effectively relieve sulfate erosion of the acid-activated material, and a good curing environment is provided for the acid-activated concrete brick body. Therefore, in the moss ecological brick provided by the invention, the acid-activated concrete brick body can supplement and promote the growth of moss.

The application discloses a kind of synchronous denitrification and phosphorus removal light materials and its preparation and application method, belong to environmental functional materials and sewage treatment technical field.The application is obtained by fully melting and dispersing sulfur and iron-based component, and the iron-based component is a mixture of pyrite and calcium-magnesium carbonate.The molten mixture is foamed to form a synchronous denitrification and phosphorus removal light material.The synchronous denitrification and phosphorus removal light material has high porosity, large specific surface area, light weight and high reactivity.The light material is used as a microbial carrier and an electron donor for biochemical reactions, and is applied to fixed bed, fluidized bed and other reactors for sewage treatment.The light material has good microbial adhesion performance, high denitrification rate and good phosphorus removal effect.

The invention relates to a process for preparing a phosphor copper rod by using a phosphonate-amide composite purifying agent as a quenching aid, and belongs to the technical field of non-ferrous metallurgy. Phosphorus pentoxide and sodium carbonate are mixed and decocted into fused salt, the fused salt is cooled and ground and then added into a corundum crucible together with scrap copper to be rapidly heated, compressed air is blown in, and slagging-off is conducted after heat preservation and standing; blowing mixed gas into the melt for reduction refining; adding calcium boride into the melt for refining; the refined copper liquid is subjected to continuous casting and continuous rolling; rapidly immersing the phosphorus copper rod subjected to continuous casting and rolling into a quenching aid solution, and carrying out quenching treatment; and the quenched phosphor copper rod is blow-dried and dried, and the high-conductivity phosphor copper rod is obtained. The high-purity phosphorus copper rod prepared by the method is excellent in key indexes of copper content, phosphorus content and conductivity, and meets the expected requirements of high purity and high conductivity.

The invention relates to the technical field of wet-process phosphoric acid, and discloses a wet-process phosphoric acid grading and arsenic removal treatment method and system, and the system can be switched between a parallel grading treatment mode and a series depth treatment mode through flow control; in the parallel mode, the two arsenic removal reaction tanks operate independently to respectively treat different raw materials and produce desulfurized acid for industrial monoammonium and low-arsenic dilute phosphoric acid for high-phosphorus compound fertilizer, the low-arsenic dilute phosphoric acid is mixed and blended with untreated dilute acid and then concentrated, qualified products are obtained with the minimum treatment capacity, and the cost is remarkably reduced; in the series connection mode, raw materials sequentially flow through the two tanks to be deeply purified, and single high-quality phosphoric acid is produced; the two modes are both integrated with efficient filter pressing units, solid-liquid separation is carried out on arsenic-containing thick slurry generated by arsenic removal, and phosphorus resource recovery and arsenic pollution control are achieved; the device has production flexibility and deep purification capacity, perfectly meets the requirements of raw material fluctuation and multiple products, and thoroughly solves the problem of arsenic slag disposal.

The invention discloses a phosphorus slag ceramsite lightweight thermal insulation concrete structure preparation control system and method, and particularly relates to the technical field of building material preparation, and the method comprises the following steps: collecting ceramsite physical information, establishing a multi-dimensional parameter set, and setting a component mapping rule; ceramsite space configuration is completed according to mapping; the prepared ceramsite is subjected to surface pretreatment and mixed to form preformed concrete, and the preformed concrete is cured after performance evaluation; maintenance is controlled according to a multi-section temperature and humidity linkage path, and whether the next section is entered or not is judged by the trained machine learning model; when the conditions are not met, the control conditions are updated through optimization steps, and judgment is executed again until all the curing processes are completed; according to the invention, the performance matching configuration of the phosphorus slag ceramsite in the structure is realized, and the preformed concrete is maintained after the performance of the preformed concrete reaches the standard; and through path analysis and state judgment, the multi-section curing process is dynamically regulated and controlled, and the performance consistency and control precision of the concrete structure are improved.

The invention relates to the field of ecological environment and digital simulation, in particular to a phosphorus pollution risk evaluation method and system based on a migration and transformation mechanism. A phosphorus pollution risk evaluation method based on a migration and transformation mechanism comprises the following steps that S10, at a preset sampling point position of a preset drainage basin, various data are collected according to preset parameter types, and the parameter types comprise various parameter types needed by a preset mechanism model and a preset output coefficient model; sorting the collected data according to a collection time sequence, and establishing a space-time matching database; and S20: extracting parameter types in the database, defining a cross-medium migration relationship of phosphorus based on physical parameters, constructing a conversion relationship of a corresponding form in combination with parameters of chemical and biological types, and dividing factor types. According to the scheme, the problem of low evaluation accuracy caused by insufficient sensitivity of analysis results of a static evaluation method and a dynamic evaluation method based on a simplified model in phosphorus pollution risk evaluation is solved.

The invention discloses a refining calcium-free treatment process, and belongs to the technical field of refining and smelting of high-carbon aluminum-containing steel. According to the method, various smelting parameters of the whole steelmaking process are adjusted, sulfur entering a converter is guaranteed in a desulfurization area, tapping carbon, tapping temperature, in-place refining component hit rate, deoxidation degree and tapping phosphorus difference are guaranteed in a converter area, refining treatment time, white slag protection time and soft blowing time are guaranteed in a refining area, the content of Al2O3 in molten steel is reduced, the purity of the molten steel is guaranteed, and the quality of the molten steel is improved. Molten steel calcium-free treatment is achieved, and the quality of molten steel is improved.

A non-oriented electrical steel sheet having a composition including of the following elements, expressed in percentage by weight: 0.0001%≤Carbon≤0.007%, 0.15%≤Manganese≤0.2%, 3%≤Silicon≤3.6%, 0.7%≤Aluminum≤1.3%, Phosphorus≤0.15%, Sulfur≤0.006%, Nitrogen≤0.09%, with 3.85%≤Si+Al+Mn≤5.5%, various optional elements. The remainder composition is iron and unavoidable impurities caused by processing. The microstructure is made of ferrite and has in area fraction, 80% to 100% recrystallized microstructure, 0% to 20% non-recrystallized microstructure wherein the average grain size of recrystallized microstructure is from 20 microns to 110 microns and eddy current losses in total iron losses, measured at 1 T and 400 Hz according to IEC 60404-2 standards, of 35 to 55% when calculated in accordance with Bertotti method and simultaneously having a magnetic polarization at 5000A / m (J50) from 1.635T to 1.670T.

The invention relates to a recycling method of chemical polishing waste liquid, which comprises the following steps: (1) carrying out first pH regulation treatment on the chemical polishing waste liquid containing phosphate radicals, sulfate radicals, aluminum ions and + 3 valent iron ions to obtain aluminum mud and aluminum-removed liquid; (2) sequentially carrying out second pH regulation treatment, third pH regulation treatment and dealumination treatment on the aluminum mud to obtain a hydrated calcium aluminate product; (3) the aluminum-removed liquid is subjected to phosphorus removal treatment, and first phosphorus mud and phosphorus-removed liquid are obtained; sequentially carrying out fourth pH regulation treatment and first evaporative crystallization treatment on the first phosphorus sludge to obtain a sodium phosphate product; and sequentially carrying out fifth pH regulation treatment and second evaporative crystallization treatment on the dephosphorized liquid to obtain a sodium sulfate product. According to the method disclosed by the invention, phosphorus, sulfur and aluminum in the chemical polishing waste liquid are completely separated by utilizing different solubility of different substances in the solution when the pH value is the same, and a sodium phosphate product, a sodium sulfate product and a hydrated calcium aluminate product are respectively obtained, so that complete recycling of elements in the chemical polishing waste liquid is realized, and no byproduct waste is produced.

The invention relates to the technical field of sewage treatment, in particular to an intelligent adaptive phosphorus removal adding method and system based on deep learning, and the method comprises the steps: obtaining a historical sewage information set based on original historical sewage data, dividing the historical sewage information set through a cloud intelligent center, and carrying out the training, verification and testing of a deep learning framework, and obtaining a deep learning phosphorus removal model; the method comprises the following steps: acquiring real-time water inlet information, predicting phosphorus removal agent adding information by using a deep learning model, acquiring empirical adding information based on the real-time water inlet information and an empirical formula, comprehensively predicting the phosphorus removal agent adding information, the empirical adding information and actual reserve information, controlling the actual adding operation of a phosphorus removal agent, and acquiring real-time water outlet information. The historical sewage information set is updated, if a preset retraining condition is met, the updated historical sewage information set is used for retraining the model, and continuous optimization and self-adaptive adjustment of the model are achieved. According to the invention, the accuracy and economical efficiency of adding the dephosphorization agent in the sewage treatment process can be improved.

The invention belongs to the technical field of microorganisms, and discloses a novel Burkholderia cepacia HSP-21 capable of dissolving phosphorus and solidifying heavy metals and an application of the novel Burkholderia cepacia HSP-21. The novel burkholderia cepacia disclosed by the invention is Burkholderia cepacia HSP-21, and the preservation number of the novel burkholderia cepacia is CCTCC (China Center for Type Culture Collection) NO: M 20251344; the strain is preserved in China Center for Type Culture Collection on June 12, 2025, and the preservation address is Wuhan University, Wuhan, Hubei, China. The strain disclosed by the invention has relatively strong phosphorus dissolving activity, heavy metal removal capacity and curing effect, and can effectively inhibit migration and transformation of heavy metals, so that long-term stabilization of the heavy metals is realized. The strain can be applied to environmental remediation and heavy metal pollution treatment.

The application discloses a high-phosphorus molten iron extremely-low-sulfur and low-phosphorus hydrogen-doped pipeline steel steelmaking process control method, which reduces the burden of LF desulfurization through post-furnace slag system treatment, effectively improves the refining rate, improves the production efficiency and guarantees continuous casting through over-treatment or re-treatment of LF refining; compared with conventional production, the desulfurization efficiency is improved through converter slag system and LF refining slagging process, the cleanliness of the steel is also greatly improved, and the final total oxygen content can be stably controlled within 0.0015%. The application aims to provide a steelmaking process control method for realizing low-phosphorus and extremely-low-sulfur chemical composition in the process of smelting hydrogen-doped pipeline steel from high-phosphorus molten iron, especially for smelting low-phosphorus steel and extremely-low-sulfur steel from high-phosphorus molten iron, the cleanliness of the steel is also greatly improved, and the final total oxygen content can be stably controlled within 0.0015%.

The invention relates to the technical field of preparation of battery materials, and discloses a method for synthesizing iron phosphate through continuous oxidation, which comprises the following steps: oxidation: oxidizing a ferrous solution by adopting oxygen-containing gas to obtain a ferric iron solution; synthesizing iron phosphate: reacting the ferric iron solution with a phosphorus source to obtain amorphous iron phosphate; and crystal transformation and roasting: carrying out crystal transformation and roasting on the amorphous iron phosphate to obtain the iron phosphate. The iron phosphate material prepared by the invention is oxidized by adopting the oxygen-containing gas, so that compared with hydrogen peroxide adopted in the prior art, the cost is lower, and the specific surface area and the tap density of the prepared iron phosphate material are higher.

The building block is prepared from the following raw materials in parts by weight: 30 to 60 parts of ardealite, 0.5 to 2 parts of lime, 10 to 30 parts of slag, 0 to 2.5 parts of silica fume, 0 to 2.5 parts of fly ash, 1 to 5 parts of cement, a water reducing agent with the mass ratio of 0.5 to 1.5 percent of ardealite, 8 to 12 parts of water, 10 to 20 parts of an acrylic acid metal salt mixed solution, 0.5 to 2.5 parts of a water repellent agent and 15 to 50 parts of aggregate, the acrylic acid metal salt mixed solution contains calcium ions or / and magnesium ions; through the in-situ polymerization synergistic effect among the cement, the lime, the inorganic active material and the acrylic acid metal salt solution, the inorganic-organic hybrid gel efficiently and stably solidifies the phosphogypsum, harmful ions are converted into insoluble and thermodynamically stable forms, and efficient and stable phosphorus, fluorine and heavy metal immobilization is achieved. The mixing amount of the phosphogypsum is as high as 30-60%, the building block has good mechanical properties, the 28-day compressive strength of the building block is greater than or equal to 30 MPa, and the breaking strength is greater than or equal to 3.5 MPa; and through surface modification treatment of the hydrophobic agent, a hydrophobic film is formed on the surface of the ardealite, the hydrophobic performance of the surface of the ardealite is enhanced, the water resistance of the ardealite is improved, and the water absorption rate of the building block is less than or equal to 5.0%. And the preparation process has the advantages of low cost, simplicity and convenience in operation, environment friendliness and the like.